Allylbenzene by Asch

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eMolecules

Reactions (440)

Yield

LabNetwork

Substances (2)

Citations (416)

Conditions

References

199

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Rx-ID: 6330291 Find similar reactions

With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in tetrahydrofuran

T=120°C; 24 h; in sealed ampoule;

200

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Rx-ID: 17632183

Kosugi, Masanori; Tanji, Tadatoshi; Tanaka, Yukio; Yoshida, Atsushi; Fugami, Keigo; Kameyama, Masayuki; Migita, Toshihiko

Journal of Organometallic Chemistry, 1996 , vol. 508, # 1-2 p. 255 - 257 Title/Abstract Full Text View citing articles Show Details

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Multi-step reaction with 2 steps 1: sodium metaperiodate / methanol; H2O 2: 92 percent / various solvent(s) / 0.02 h / Irradiation; other sulfoxides, thermal elimination View Scheme

Matloubi Moghaddam, Firouz; Ghaffarzadeh, Mohammad

Tetrahedron Letters, 1996 , vol. 37, # 11 p. 1855 - 1858 Title/Abstract Full Text View citing articles Show Details

201

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Rx-ID: 17632796 Find similar reactions

Multi-step reaction with 2 steps 1: sodium metaperiodate / methanol; H2O 2: 90 percent / various solvent(s) / 0.02 h / Irradiation View Scheme

Matloubi Moghaddam, Firouz; Ghaffarzadeh, Mohammad

Tetrahedron Letters, 1996 , vol. 37, # 11 p. 1855 - 1858 Title/Abstract Full Text View citing articles Show Details

202

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Rx-ID: 3858621 Find similar reactions

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61%

With boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride in dichloromethane

-78 deg C -> r.t.;

Matano, Yoshihiro; Yoshimune, Masanori; Suzuki, Hitomi

Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7475 - 7478 Title/Abstract Full Text View citing articles Show Details

56%

With other arenes and other allyl compounds investigated; thallic(III) trifluoroacetate in dichloromethane

T=0°C; 5 h;

Ochiai, Masahito; Arimoto, Masao; Fujita, Eiichi

Tetrahedron Letters, 1981 , vol. 22, # 45 p. 4491 - 4494 Title/Abstract Full Text View citing articles Show Details

56%

With thallic(III) trifluoroacetate in dichloromethane

0.5 h; Ambient temperature;

Ochiai, Masahito; Arimoto, Masao; Fujita, Eiichi

Tetrahedron Letters, 1981 , vol. 22, # 45 p. 4491 - 4494 Title/Abstract Full Text View citing articles Show Details

56%

With thallic(III) trifluoroacetate in dichloromethane

1.) 0 deg C, 5 h., 2.) room temp., 30 min.;

Ochial; Fujita; Arimoto; Yamaguchi

Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 1 p. 86 - 93 Title/Abstract Full Text View citing articles Show Details

With iodosylbenzene; boron trifluoride diethyl etherate

Ochiai, Masahito; Fujita, Eiichi; Arimoto, Masao; Yamaguchi, Hideo

T=-20°C; 1 h; other temp.; other react. time; Product distribution;

Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 1 p. 41 - 47 Title/Abstract Full Text Show Details

64 % Chromat.

With phenylthalium(III) di(trifluoroacetate)

2.5 h; Ambient temperaturevariation of ratio of reactants and time; Product distribution;

Ochiai, Masahito; Fujita, Eiichi; Arimoto, Masao; Yamaguchi, Hideo

Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 11 p. 3994 - 3999 Title/Abstract Full Text Show Details

73 % Chromat.

With diethyl ether; iodosylbenzene; boron trifluoride

T=-20°C; 1 h;

Ochiai, Masahito; Fujita, Eiichi; Arimoto, Masao; Yamaguchi, Hideo

Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 1 p. 41 - 47 Title/Abstract Full Text Show Details

88 % Chromat.

With 2,5-dimethylphenylthallium bis(trifluoroacetate)

2.5 h; Ambient temperature;

Ochiai, Masahito; Fujita, Eiichi; Arimoto, Masao; Yamaguchi, Hideo

Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 11 p. 3994 - 3999 Title/Abstract Full Text Show Details

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203

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Rx-ID: 4159408 Find similar reactions

A: 1% B: 1% C: 95%

With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in toluene

T=60°C; P=45600 Torr; 15 h;

Yamamoto, Akio

Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 2 p. 433 - 446 Title/Abstract Full Text Show Details

With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in toluene

P=15200 Torr; 96 h; Ambient temperatureother reagents, other solvents, var. temp., pressure, time; Product distribution;

Yamamoto, Akio

Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 2 p. 433 - 446 Title/Abstract Full Text Show Details

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204

Synthesize Find similar Rx-ID: 4164194 Find similar reactions

A: 56% B: 43%

With palladium tetrakis (triphenyl-phosphine) palladium; carbon monoxide in toluene

T=50°C; P=760 Torr; 4 h;

Yamamoto, Akio

Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 2 p. 433 - 446 Title/Abstract Full Text Show Details

A: 56% B: 43%

With palladium tetrakis (triphenyl-phosphine) palladium; carbon monoxide in toluene

T=50°C; P=760 Torr; 4 h;

Yamamoto, Akio

Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 2 p. 433 - 446 Title/Abstract Full Text Show Details

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205

Synthesize Find similar Rx-ID: 4179826 Find similar reactions

With boron trifluoride diethyl etherate; sodium cyanoborohydride

Ambient temperature;

Srikrishna, Adusumilli; Viswajanani, Ranganathan; Sattigeri, Jitendra A.; Yelamaggad, Channabasaveshwar V.

Tetrahedron Letters, 1995 , vol. 36, # 13 p. 2347 - 2350 Title/Abstract Full Text View citing articles Show Details

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206

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Rx-ID: 4272001 Find similar reactions

207

A: 70% B: 15%

With aluminum oxide; silica gel; potassium carbonate; zinc(II) chloride

T=30°C; 1 h; var. of reagents; Product distribution;

Kodomari, Mitsuo; Nawa, Satoru; Miyoshi, Tadahiro

Journal of the Chemical Society, Chemical Communications, 1995 , # 18 p. 1895 - 1896 Title/Abstract Full Text View citing articles Show Details

A: 70% B: 15%

With aluminum oxide; silica gel; potassium carbonate; zinc(II) chloride

T=30°C; 1 h;

Kodomari, Mitsuo; Nawa, Satoru; Miyoshi, Tadahiro

Journal of the Chemical Society, Chemical Communications, 1995 , # 18 p. 1895 - 1896 Title/Abstract Full Text View citing articles Show Details

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Rx-ID: 4380361 Find similar reactions

45 % Chromat.

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With boron trifluoride diethyl etherate in dichloromethane

T=-78°C;

Matano, Yoshihiro; Yoshimune, Masanori; Suzuki, Hitomi

Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7475 - 7478 Title/Abstract Full Text View citing articles Show Details

208

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Rx-ID: 4381581 Find similar reactions

80%

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With triethylaluminum; triphenylphosphine; bis(acetylacetonate)nickel(II) in hexane; toluene

T=120°C; 5 h;

Trost, Barry M.; Spagnol, Michel D.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 17 p. 2083 - 2096 Title/Abstract Full Text View citing articles Show Details

209

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Rx-ID: 4381582 Find similar reactions

62%

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With Ni(PPh3)4 in benzene

T=100°C; 7 h;

Trost, Barry M.; Spagnol, Michel D.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 17 p. 2083 - 2096 Title/Abstract Full Text View citing articles Show Details

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210

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Rx-ID: 4470645 Find similar reactions

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Wagner, Peter J.; Frerking, Harlan W. Jr.

Canadian Journal of Chemistry, 1995 , vol. 73, p. 2047 - 2061 Title/Abstract Full Text Show Details

in benzene

6 h; Irradiationstudy the triplet state; Product distribution;

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211

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Rx-ID: 1934897 Find similar reactions

A: 6 % Chromat. B: 5 % Chromat.

With palladium diacetate; sodium acetate in acetic acid

T=25°C; 24 h;

Cho, Chan Sik; Uemura, Sakae

Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 85 - 92 Title/Abstract Full Text View citing articles Show Details

A: 6 % Chromat. B: 5 % Chromat.

With palladium diacetate; sodium acetate in acetic acid

T=25°C; 24 h;

Cho, Chan Sik; Uemura, Sakae

Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 85 - 92 Title/Abstract Full Text View citing articles Show Details

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212

Synthesize Find similar Rx-ID: 2478759 Find similar reactions

With 9,10-dihydroanthracene in various solvent(s) T=259°C; 1.5 h; var. reaction times; Product distribution;

Doering; Birladeanu, Ludmila; Sarma, Keshab; Teles, Joaquim Henrique; Klaerner; Gehrke, Jan-Stephan

Journal of the American Chemical Society, 1994 , vol. 116, # 10 p. 4289 - 4297 Title/Abstract Full Text View citing articles Show Details

213

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Rx-ID: 3382274 Find similar reactions

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With ammonium chloride; zinc in tetrahydrofuran

other ketones and aldehydes; Mechanism;

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Sjoeholm, Rainer; Rairama, Riitta; Ahonen, Matthias

Journal of the Chemical Society, Chemical Communications, 1994 , # 10 p. 1217 - 1218 Title/Abstract Full Text View citing articles Show Details

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214

Synthesize Find similar Rx-ID: 3710418 Find similar reactions

A: 18% B: 8% C: 12% D: 8% E: 2% F: 3%

Aitken, R. Alan; Armstrong, David P.; Mesher, Shaun T. E.; Galt, Ronald H. B.

Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6143 - 6146 Title/Abstract Full Text View citing articles Show Details

T=650°C; flash vacuum pyrolysis;

215

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Rx-ID: 3952136 Find similar reactions

61 % Chromat.

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With copper(l) iodide; triphenyl-arsane; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide

T=60°C; 6 h;

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Farina, Vittorio; Kapadia, Suresh; Krishnan, Bala; Wang, Chenjie; Liebeskind, Lanny S.

Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 5905 - 5911 Title/Abstract Full Text View citing articles Show Details

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216

Synthesize Find similar Rx-ID: 2139423 Find similar reactions

A: 17.4 % Chromat. B: 75.1 % Chromat. C: 7.2 % Chromat.

With sodium methylate in methanol

48 h; Ambient temperatureother 1-phenyl-2-alkyl tosylates; Rate constantProduct distributionMechanism;

Cho, Bong Rae; Han, Man So

Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 105 - 108 Title/Abstract Full Text View citing articles Show Details

217

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40 % Chromat.

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Rx-ID: 2751551 Find similar reactions

With triethylamine; 3-chloro-benzenecarboperoxoic acid in diethyl ether

T=25°C; 2 h;

Nishibayashi, Yoshiaki; Komatsu, Naoki; Ohe, Kouichi; Uemura, Sakae

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1133 - 1138 Title/Abstract Full Text View citing articles Show Details

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218

Synthesize Find similar Rx-ID: 3323761 Find similar reactions

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A: 45% B: 20%

With HUSY26

T=149.9°C;

Espeel, P. H.; Janssens, B.; Jacobs, P. A.

Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7688 - 7693 Title/Abstract Full Text View citing articles Show Details

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219

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Rx-ID: 3327523 Find similar reactions

A: 42 % Chromat.

With silver(I) acetate; palladium diacetate in acetic acid

T=25°C; 5 h;

Cho, Chan Sik; Itotani, Koichi; Uemura, Sakae

Journal of Organometallic Chemistry, 1993 , vol. 443, # 2 p. 253 - 259 Title/Abstract Full Text View citing articles Show Details

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220

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With sodium tetrahydroborate in dichloromethane

5 h; Ambient temperature; Yield given. Yields of byproduct given;

Hendrickson, James B.; Singer, Michael; Hussoin, Md. Sajjat

Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6913 - 6914 Title/Abstract Full Text View citing articles Show Details

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221

With water in benzene-d6

Rx-ID: 6674705 Find similar reactions

Mashima, Kazushi; Yamanaka, Yoshimichi; Gohro, Yoshihiko; Nakamura, Akira

Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Journal of Organometallic Chemistry, 1993 , vol. 455, # 1-2 p. C6 - C8 Title/Abstract Full Text View citing articles Show Details

222

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Rx-ID: 18604298 Find similar reactions

Multi-step reaction with 2 steps 1: CH2Cl2

2: NaBH4 / CH2Cl2 / 5 h / Ambient temperature View Scheme

Hendrickson, James B.; Singer, Michael; Hussoin, Md. Sajjat

Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6913 - 6914 Title/Abstract Full Text View citing articles Show Details

223

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Rx-ID: 19272077 Find similar reactions

Multi-step reaction with 2 steps 1: 83 percent / NaBH4 / ethanol / 3 h / 20 - 25 °C 2: 40 percent Chromat. / m-chloroperbenzoic acid, Et3N / diethyl ether / 2 h / 25 °C View Scheme

Nishibayashi, Yoshiaki; Komatsu, Naoki; Ohe, Kouichi; Uemura, Sakae

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1133 - 1138 Title/Abstract Full Text View citing articles Show Details

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224

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A: 20.1% B: 2% C: 0.8%

With nichrome wire

T=830°C; 2 h; also other alkanes and alkines, var. wire metals and wire temperatures; Product distribution;

Takagi, Yuzuru; Aoyagi, Toshiaki; Yoshida, Takeo; Yada, Satoru; Yamaguchi, Tatsuaki; et al

Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 1 p. 274 - 279 Title/Abstract Full Text Show Details

D: 10.8% E: 3.5% F: 4.6%

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225

Synthesize Find similar Rx-ID: 3067536 Find similar reactions

Lewis-Bevan, Wyn; Gaston, Rick D.; Tyrrell, James; Stork, Wilmer D.; Salmon, Gary L.

Journal of the American Chemical Society, 1992 , vol. 114, # 6 p. 1933 - 1935 Title/Abstract Full Text View citing articles Show Details

T=450 - 800°C; P=0.01 Torr;

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226

Synthesize Find similar Rx-ID: 3076533 Find similar reactions

Jongh, Connie P. de; Modro, Tomasz A.

Journal of the Chemical Society, Chemical Communications, 1992 , # 14 p. 1003 - 1004 Title/Abstract Full Text View citing articles Show Details

in sulfolane

T=195°C; other 2-acyloxyalkylphosphonates; entropy of activation; Rate constantThermodynamic dataMechanism;

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227

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Jongh, Connie P. de; Modro, Tomasz A.

Journal of the Chemical Society, Chemical Communications, 1992 , # 14 p. 1003 - 1004 Title/Abstract Full Text View citing articles Show Details

in sulfolane

T=195°C; Rate constant;

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228

Synthesize Find similar Rx-ID: 3097484 Find similar reactions

Jongh, Connie P. de; Modro, Tomasz A.

Journal of the Chemical Society, Chemical Communications, 1992 , # 14 p. 1003 - 1004 Title/Abstract Full Text View citing articles Show Details

in sulfolane

T=195°C; Rate constant;

229

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Rx-ID: 20383408 Find similar reactions

Multi-step reaction with 4 steps 1: 1.) Ac2O, 2.) aq. LiOH / 1.) AcOH, RT, 2.) MeOH, THF 2: 77 percent / m-chloroperbenzoic acid / CH2Cl2 / -78 °C 3: 26 percent / ZnI2 / Ambient temperature 4: 450 - 800 °C / 0.01 Torr View Scheme

Lewis-Bevan, Wyn; Gaston, Rick D.; Tyrrell, James; Stork, Wilmer D.; Salmon, Gary L.

Journal of the American Chemical Society, 1992 , vol. 114, # 6 p. 1933 - 1935 Title/Abstract Full Text View citing articles Show Details

230

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Rx-ID: 20413732 Find similar reactions

Multi-step reaction with 3 steps 1: 77 percent / m-chloroperbenzoic acid / CH2Cl2 / -78 °C 2: 26 percent / ZnI2 / Ambient temperature 3: 450 - 800 °C / 0.01 Torr View Scheme

Lewis-Bevan, Wyn; Gaston, Rick D.; Tyrrell, James; Stork, Wilmer D.; Salmon, Gary L.

Journal of the American Chemical Society, 1992 , vol. 114, # 6 p. 1933 - 1935 Title/Abstract Full Text View citing articles Show Details

231

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Rx-ID: 20413895 Find similar reactions

Multi-step reaction with 2 steps 1: 26 percent / ZnI2 / Ambient temperature 2: 450 - 800 °C / 0.01 Torr View Scheme

Lewis-Bevan, Wyn; Gaston, Rick D.; Tyrrell, James; Stork, Wilmer D.; Salmon, Gary L.

Journal of the American Chemical Society, 1992 , vol. 114, # 6 p. 1933 - 1935 Title/Abstract Full Text View citing articles Show Details

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232

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With triphenylphosphine; nickel dichloride; zinc in N,N-dimethyl-formamide

T=23°C; 1.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Wenkert, Ernest; Chianelli, Donatella

Journal of the Chemical Society, Chemical Communications, 1991 , # 9 p. 627 - 628 Title/Abstract Full Text View citing articles Show Details

233

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With methanol; 9-borabicyclo[3.3.1]nonane dimer

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Rx-ID: 2505458 Find similar reactions

Singaram, Bakthan; Rangaishenvi, Milind V.; Brown, Herbert C.; Goralski, Christian G.; Hasha, Dennis L.

heating, 1h; Yield given. Multistep reaction;

Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1543 - 1549 Title/Abstract Full Text View citing articles Show Details

With methanol; 9-borabicyclo[3.3.1]nonane dimer

1.) THF, 25 deg C, 3 h; Yield given. Multistep reaction;

Singaram, Bakthan; Goralski, Christian T.; Rangaishenvi, Milind V.; Brown, Herbert C.

Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 384 - 386 Title/Abstract Full Text View citing articles Show Details

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234

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With silica gel

multistep reaction: 1) condensation with the surface OH-groups of silica, 2) thermolysis at 400 deg C; MechanismProduct distributionRate constant;

Britt, Phillip F.; Buchanan, A. C.

Journal of Organic Chemistry, 1991 , vol. 56, # 21 p. 6132 - 6140 Title/Abstract Full Text View citing articles Show Details

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235

Synthesize Find similar Rx-ID: 26847240 Find similar reactions

A: 1% B: 8% C: 6% D: 25% E: 2%

236

With methanol in tetrahydrofuran

Irradiation (UV/VIS); Further Products. Purging of a THF soln. of Cs-salt with N2, addn. of MeOH in THF, irradn. at 254 nm.; Monitored by (11)B-NMR and GC.;

Kropp, Michael A.; Baillargeon, Michelle; Park, Kyung Mi; Bhamidapaty, Kaumudi; Schuster, Gary B.

Journal of the American Chemical Society, 1991 , vol. 113, # 6 p. 2155 - 2163 Title/Abstract Full Text View citing articles Show Details

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Rx-ID: 1934896 Find similar reactions

60%

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Legros, Jean-Yves; Fiaud, Jean-Claude

Tetrahedron Letters, 1990 , vol. 31, # 51 p. 7453 - 7456 Title/Abstract Full Text View citing articles Show Details

With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran

T=60°C; 24 h;

237

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Rx-ID: 2292464 Find similar reactions

With boron trifluoride diethyl etherate; acetic acid; isopentyl nitrite

1.) 70 deg C, 35 min 2.) 70 deg C, 8 min; Yield given. Multistep reaction;

Cunico, Robert F.

Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4474 - 4478 Title/Abstract Full Text View citing articles Show Details

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238

Synthesize Find similar Rx-ID: 2294513 Find similar reactions

A: 88.7 % Chromat. B: 4.4 % Chromat. C: 5.9 % Chromat.

239

T=321°C; P=64.5 Torr; other temperatures; other pressures; Arrhenius parameters (Ea, log A); MechanismKineticsThermodynamic data;

Chuchani, Gabriel; Dominguez, Rosa M.; Rotinov, Alexandra; Martin, Ignacio; Alvarez, G. Jaime

Journal of Physical Chemistry, 1990 , vol. 94, # 8 p. 3341 - 3343 Title/Abstract Full Text View citing articles Show Details

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Rx-ID: 2925648 Find similar reactions

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Brown, Herbert C.; Rangaishenvi, Milind V.

Tetrahedron Letters, 1990 , vol. 31, # 45 p. 7115 - 7118 Title/Abstract Full Text View citing articles Show Details

Yield given. Multistep reaction;

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240

Synthesize Find similar Rx-ID: 3745479 Find similar reactions

A: 10% B: 90%

With lithium formate; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; Ph2P(CH2)3SO3Li-Pd(II)-complex in n-heptane; water

T=90°C; other Pd(II)-phosphine complexes, other polyether detergents, other formates, Na, K, NH4; Product distribution;

Paetzold, E.; Oehme, G.

Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 51/52, p. 829 Title/Abstract Full Text Show Details

A: 61% B: 28%

With lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran

T=-50°C; 0.25 h;

Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho

Chemistry Letters, 1983 , p. 1877 - 1878 Title/Abstract Full Text Show Details

With formates; palladium in n-heptane; water

T=90°C;

Paetzold, E.; Oehme, G.

Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 51/52, p. 829 Title/Abstract Full Text Show Details

Hide Details

With lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran

T=-20°C; 6 h; Yield given. Yields of byproduct given;

Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho

Chemistry Letters, 1983 , p. 1877 - 1878 Title/Abstract Full Text Show Details

241

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With n-butyllithium

1.) THF, hexane, 0 deg C, 0.5 h, 2.) 0 deg C, 1 h; Yield given. Multistep reaction;

Rx-ID: 6330295 Find similar reactions

Kuchin, A. V.; Markova, S. A.; Gorobets, E. V.; Tolstikov, G. A.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 5.2 p. 1034 - 1037 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 5 p. 1151 - 1154

Title/Abstract Full Text View citing articles Show Details

242

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Rx-ID: 21869236 Find similar reactions

Multi-step reaction with 2 steps 1: 27 percent / LiAlH4 / tetrahydrofuran / 2.5 h / Heating 2: 1.) glacial acetic acid, iAmONO 2.) BF3.Et2O / 1.) 70 deg C, 35 min 2.) 70 deg C, 8 min View Scheme

Cunico, Robert F.

Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4474 - 4478 Title/Abstract Full Text View citing articles Show Details

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243

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Rx-ID: 26565393 Find similar reactions

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A: >95 B: 70-80

in 1,2-dichloro-ethane

react. of Pd-complex with BPh4(1-) at 25°C in sovent in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in methanol; water

Kinetics; react. of Pd-complex with BPh4(1-) at 25°C in aq. CH3OH in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in dichloromethane

react. of Pd-complex with BPh4(1-) at 25°C in CH2Cl2 in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

Hide Details

A: >95 B: 70-80

in acetone

react. of Pd-complex with BPh4(1-) at 25°C in acetone in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in acetonitrile

react. of Pd-complex with BPh4(1-) at 25°C in CH3CN in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

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244

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Rx-ID: 26565394 Find similar reactions

A: >95 B: 70-80

in methanol; water

Kinetics; react. of Pd-complex with BPh4(1-) at 25°C in aq. CH3OH in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in dichloromethane

react. of Pd-complex with BPh4(1-) at 25°C in solvent in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in 1,2-dichloro-ethane

react. of Pd-complex with BPh4(1-) at 25°C in solvent in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

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A: >95 B: 70-80

in acetone

react. of Pd-complex with BPh4(1-) at 25°C in acetone in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in acetonitrile

react. of Pd-complex with BPh4(1-) at 25°C in CH3CN in presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

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245

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Rx-ID: 26565396 Find similar reactions

B: 0%

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Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

in methanol; water

Kinetics; react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

246

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Rx-ID: 26565397 Find similar reactions

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A: >95 B: 70-80

in methanol; water

Kinetics; react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in dichloromethane

react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in 1,2-dichloro-ethane

react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

Hide Details

A: >95 B: 70-80

in acetone

react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

A: >95 B: 70-80

in acetonitrile

react. of Pd-compex with BPh4(1-) at 25°C in solvent in the presence of dimethylfumarate;

Crociani, Bruno; Bianca, Francesca Di; Canovese, Luciano; Uguagliati, Paolo

Journal of Organometallic Chemistry, 1990 , vol. 381, # 1 p. C17 - C20 Title/Abstract Full Text View citing articles Show Details

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247

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Rx-ID: 1616984 Find similar reactions

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A: 9% C: 47%

With tetrakis(triphenylphosphine) palladium(0) in benzene

T=100°C; 20 h;

Kosugi, Masanori; Tamura, Hiroyuki; Sano, Hiroshi; Migita, Toshihiko

Tetrahedron, 1989 , vol. 45, # 4 p. 961 - 968 Title/Abstract Full Text View citing articles Show Details

A: 9% C: 47%

With tetrakis(triphenylphosphine) palladium(0) in benzene

T=100°C; 20 h;

Kosugi, Masanori; Tamura, Hiroyuki; Sano, Hiroshi; Migita, Toshihiko

Tetrahedron, 1989 , vol. 45, # 4 p. 961 - 968 Title/Abstract Full Text View citing articles Show Details

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248

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Rx-ID: 1939872 Find similar reactions

With (C5H5)Fe(C5H5) in water; acetone

1) 45 deg C, 2) 50 - 60 deg C, 1 h; Yield given. Yields of byproduct given;

Yashkina, L. V.; Kopylova, B. V.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 4.2 p. 863 - 865 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 4 p. 957 - 959 Title/Abstract Full Text View citing articles Show Details

With (C5H5)Fe(C5H5) in water; acetone

1) 45 deg C, 2) 50 - 60 deg C, 1 h; other aryldiazonium chlorides; Product distribution;

Yashkina, L. V.; Kopylova, B. V.

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249

Synthesize Find similar Rx-ID: 1983180 Find similar reactions

A: 15 % Chromat.

With sodium hydrogen sulphate; silica gel in 1,1,2,2-tetrachloroethylene

0.666667 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;

Nishiguchi, Takeshi; Kamio, Chizuko

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 707 - 710 Title/Abstract Full Text View citing articles Show Details

A: 15 % Chromat.

With sodium hydrogen sulphate; silica gel in 1,1,2,2-tetrachloroethylene

0.666667 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Nishiguchi, Takeshi; Kamio, Chizuko

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 707 - 710 Title/Abstract Full Text View citing articles Show Details

A: 15 % Chromat.

With sodium hydrogen sulphate; silica gel in 1,1,2,2-tetrachloroethylene

0.666667 h; Heatingother solvents, catalysts, different time; Product distributionMechanism;

Nishiguchi, Takeshi; Kamio, Chizuko

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 707 - 710 Title/Abstract Full Text View citing articles Show Details

250

Synthesize Find similar Rx-ID: 2007665 Find similar reactions

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Kopinke, Frank-Dieter; Zimmermann, Gerhard; Aust, Janette; Scherzer, Klaus

Chemische Berichte, 1989 , vol. 122, p. 721 - 726 Title/Abstract Full Text Show Details

T=600°C; further temp.; Product distributionMechanismRate constant;

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251

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Rx-ID: 1580254 Find similar reactions

With C3H8 bulk gas; oxygen

T=37.5°C; Irradiation0.5 Torr substrate, 690 Torr bulk gas, 4 Torr O2 and 2.4 Torr methanol partial pressures; Product distribution;

Fornarini, Simonetta; Sparapani, Cinzia; Speranza, Maurizio

Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 34 - 41 Title/Abstract Full Text View citing articles Show Details

With methane; oxygen

T=37.5°C; Irradiationdifferent partial pressures of components and in the given case: in the presence of 4 Torr NMe3 partial pressure; Product distribution;

Fornarini, Simonetta; Sparapani, Cinzia; Speranza, Maurizio

Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 34 - 41 Title/Abstract Full Text View citing articles Show Details

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252

Synthesize Find similar Rx-ID: 1580742 Find similar reactions

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With monofluoromethane; oxygen

T=37.5°C; Irradiation0.6 Torr substrate, 700 Torr bulk gas, 4 Torr O2 and 1.9 Torr methanol partial pressures; Product distribution;

Fornarini, Simonetta; Sparapani, Cinzia; Speranza, Maurizio

Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 34 - 41 Title/Abstract Full Text View citing articles Show Details

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253

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Rx-ID: 1580743 Find similar reactions

With C3H8 bulk gas; oxygen

T=37.5°C; Irradiation0.5 Torr substrate, 700 Torr bulk gas, 4 Torr O2 and 2.0 Torr methanol partial pressures; Product distribution;

Fornarini, Simonetta; Sparapani, Cinzia; Speranza, Maurizio

Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 34 - 41 Title/Abstract Full Text View citing articles Show Details

254

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Rx-ID: 1934949 Find similar reactions

70 % Chromat.

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1939 - 1945 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 9 p. 2159 - 2166 Title/Abstract Full Text View citing articles Show Details

With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether

T=20°C; 6 h; Product distribution;

255

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Rx-ID: 1944816 Find similar reactions

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With bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; diethyl ether

T=20°C; 0.5 h; other solvent; Product distribution;

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

256

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Rx-ID: 1986751 Find similar reactions

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99 % Chromat.

With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether

T=20°C; 18 h;

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

55 % Chromat.

With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether

T=20°C; 4 h; other reaction time; Product distribution;

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

257

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Rx-ID: 2013172 Find similar reactions

95 % Chromat.

258

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With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether

T=20°C; 4 h; other reaction time, temperature; Product distribution;

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

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Rx-ID: 2106821 Find similar reactions

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With maleic anhydride; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; diethyl ether

T=20°C; 100 h; other solvent, reaction time, also in the absence of one or both reagents; Product distribution;

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.

259

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85%

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Rx-ID: 2582914 Find similar reactions

With tetrabutyl ammonium fluoride in tetrahydrofuran

0.666667 h; Heating;

Hsiao, C.-N.; Shechter, H.

Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2688 - 2699 Title/Abstract Full Text View citing articles Show Details

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260

Synthesize Find similar Rx-ID: 2736531 Find similar reactions

A: 75% B: 25%

With 3-chloroprop-1-ene

MechanismProduct distribution;

Cheng, Jya-Wei; Luo, Fen-Tair

Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1293 - 1294 Title/Abstract Full Text View citing articles Show Details

261

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Rx-ID: 3530244 Find similar reactions

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With 2,3-dichloro-prop-1-ene; magnesium

1.) THF, 2.) THF, rt.; Multistep reaction. Yields of byproduct given;

Cheng, Jya-Wei; Luo, Fen-Tair

Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1293 - 1294 Title/Abstract Full Text View citing articles Show Details

With 2,3-dichloro-prop-1-ene; magnesium

1.) THF, 2.) THF, rt.; Yield given. Multistep reaction. Yields of byproduct given;

Cheng, Jya-Wei; Luo, Fen-Tair

Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1293 - 1294 Title/Abstract Full Text View citing articles Show Details

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262

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Rx-ID: 3858622 Find similar reactions

A: 75%

With iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane

T=0°C; 3 h;

Lee, Kilsung; Kim, Dae Young; Oh, Dong Young

Tetrahedron Letters, 1988 , vol. 29, # 6 p. 667 - 668 Title/Abstract Full Text View citing articles Show Details

263

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Rx-ID: 20433854 Find similar reactions

Multi-step reaction with 2 steps 1: 1.) n-butyllithium / 1.) hexane, diethyl ether, -70 deg C, 25 min, 2.) hexane, diethyl, RT, overnight 2: 85 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.67 h / Heating View Scheme

Hsiao, C.-N.; Shechter, H.

Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2688 - 2699 Title/Abstract Full Text View citing articles Show Details

264

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Rx-ID: 1710462 Find similar reactions

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A: 9 % Chromat. B: 47%

With tetrakis(triphenylphosphine) palladium(0) in benzene

T=100°C; 20 h;

Kosugi, Masanori; Tamura, Hiroyuki; Sano, Hiroshi; Migita, Toshihiko

Chemistry Letters, 1987 , p. 193 - 194 Title/Abstract Full Text Show Details

A: 9% B: 47%

With tetrakis(triphenylphosphine) palladium(0) in benzene

T=100°C; 20 h;

Kosugi, Masanori; Tamura, Hiroyuki; Sano, Hiroshi; Migita, Toshihiko

Chemistry Letters, 1987 , p. 193 - 194 Title/Abstract Full Text Show Details

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265

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Rx-ID: 1793049 Find similar reactions

A: 10 % Chromat. B: 7 % Chromat. C: 7 % Chromat. D: 20 % Chromat. E: 10 % Chromat.

With 2,3-dimethyl-naphthalene; palladium diacetate; triethylamine; triphenylphosphine in acetonitrile

T=100°C; 25 h; influence of nature of catalyst, further boronates; Product distribution;

Nilsson, Kristina; Hallberg, Anders

Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 8 p. 569 - 576 Title/Abstract Full Text Show Details

266

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Rx-ID: 1793386 Find similar reactions

A: 15 % Chromat. B: 4 % Chromat. C: 4 % Chromat. D: 15 % Chromat. E: 25 % Chromat.

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With 2,3-dimethyl-naphthalene; palladium diacetate; triethylamine; triphenylphosphine in acetonitrile

T=100°C; 25 h; influence of nature of catalyst, further boronates; Product distribution;

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Nilsson, Kristina; Hallberg, Anders

Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 8 p. 569 - 576 Title/Abstract Full Text Show Details

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267

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Rx-ID: 1793598 Find similar reactions

A: 12 % Chromat. B: 3 % Chromat. C: 4 % Chromat. D: 2 % Chromat. E: 30 % Chromat.

With 2,3-dimethyl-naphthalene; palladium diacetate; triethylamine; triphenylphosphine in acetonitrile

T=100°C; 18 h; influence of catalyst, further boronates; Product distribution;

Nilsson, Kristina; Hallberg, Anders

Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 8 p. 569 - 576 Title/Abstract Full Text Show Details

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268

Synthesize Find similar Rx-ID: 1934910 Find similar reactions

A: 85%

in diethyl ether

T=25°C; 24 h;

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Kresteleva, I. V.; Spivak, A. Yu.; Tolstikov, G. A.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 424 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 463 Title/Abstract Full Text View citing articles Show Details

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269

Synthesize Find similar Rx-ID: 2141402 Find similar reactions

With sodium tetrahydroborate; carbon monoxide; oxygen

1.) dichloromethane; 2.) methanol; Yield given. Multistep reaction. Yields of byproduct given;

Nishinaga, Akira; Yamazaki, Shigekazu; Matsuura, Teruo

Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6309 - 6312 Title/Abstract Full Text View citing articles Show Details

270

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Rx-ID: 2925045 Find similar reactions

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 350 - 355 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 391 - 396 Title/Abstract Full Text View citing articles Show Details

With TiCl(OiPr)3; bis(η3-allyl-μ-chloropalladium(II))

1.) hexane, ether, 20 deg C, 1 h, 2.) benzene, 40 h; Yield given. Multistep reaction;

271

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Rx-ID: 2926396 Find similar reactions

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With TiCl(OiPr)3; bis(η3-allyl-μ-chloropalladium(II))

1.) hexane, ether, 20 deg C, 1 h, 2.) benzene, 0.5 h; Yield given. Multistep reaction;

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

272

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Rx-ID: 2926496 Find similar reactions

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

With TiCl(OiPr)3; bis(η3-allyl-μ-chloropalladium(II))

1.) hexane, ether, 20 deg C, 1 h, 2.) benzene, 1.5 h; Yield given. Multistep reaction;

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273

Synthesize Find similar Rx-ID: 3422106 Find similar reactions

A: 50 % Chromat. B: 42 % Chromat. C: 8 % Chromat.

With N,N,N',N,-tetramethylethylenediamine; tert-butyl alcohol in diethyl ether; hexane

T=0°C; 0.0166667 h; other reagents and additive, reaction without additive, other temperature; Product distribution;

Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu; Nagase, Shigeru

Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 673 - 678 Title/Abstract Full Text View citing articles Show Details

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274

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Rx-ID: 3917148 Find similar reactions

T=100°C; P=60 - 720 Torr; labelled with tritium; -ΔH; Product distributionKineticsThermodynamic data;

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Fornarini, Simonetta; Speranza, Maurizio

Journal of Physical Chemistry, 1987 , vol. 91, # 8 p. 2154 - 2160 Title/Abstract Full Text View citing articles Show Details

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275

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Rx-ID: 5802744 Find similar reactions

A: 82% B: 18% C: 7%

With copper(l) iodide; nitrobenzene in tetrahydrofuran

-8 deg C, 1 hr.; r.t. 30 min.; reflux 30 min.;

Rahman, Mohammed T.; Nahar, Syeda K.

Journal of Organometallic Chemistry, 1987 , vol. 329, # 1 p. 133 - 138 Title/Abstract Full Text Show Details

With copper(l) iodide; nitrobenzene in tetrahydrofuran

-8 deg C, 1 hr.; r.t. 30 min; reflux 30 min.; Product distribution;

Rahman, Mohammed T.; Nahar, Syeda K.

Journal of Organometallic Chemistry, 1987 , vol. 329, # 1 p. 133 - 138 Title/Abstract Full Text Show Details

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276

Synthesize Find similar Rx-ID: 26459582 Find similar reactions

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With bis(η3-allyl-μ-chloropalladium(II)) in diethyl ether; benzene

reaction of soln. of PhTi(i-OPr)3 in ether (obtained from reaction of PhLi with ClTi(i-OPr)3 in ether) with soln. of allylbromide and (C3H5PdCl)2 in benzene at 20°C under Ar;; not isolated;;

277

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

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Rx-ID: 26482598 Find similar reactions

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With bis(η3-allyl-μ-chloropalladium(II)) in diethyl ether; benzene

reaction of soln. of PhTi(i-OPr)3 in ether (obtained from reaction of PhLi with ClTi(i-OPr)3 in ether) with soln. of allylchloride and (C3H5PdCl)2 in benzene at 20°C under Ar;; not isolated;;

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Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

278

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Rx-ID: 26495865 Find similar reactions

With bis(η3-allyl-μ-chloropalladium(II)) in diethyl ether; benzene

reaction of soln. of PhTi(i-OPr)3 in ether (obtained from reaction of PhLi with ClTi(i-OPr)3 in ether) with soln. of allyliodide and (C3H5PdCl)2 in benzene at 20°C under Ar;; not isolated;;

Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.

279

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Rx-ID: 747009 Find similar reactions

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With diethyl ether

Hershberg

Helvetica Chimica Acta, 1934 , vol. 17, p. 351,354 Full Text View citing articles Show Details

With vanadium(III) chloride

1.) dichloromethane, -78 grad C, 20 min, 2.) dichloromethane, -78 grad C, 1.5 h, room temp., 14 h; Yield given. Multistep reaction;

Hirao, Toshikazu; Misu, Daisuke; Yao, Koichi; Agawa, Toshio

Tetrahedron Letters, 1986 , vol. 27, # 8 p. 929 - 932 Title/Abstract Full Text View citing articles Show Details

280

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Rx-ID: 1899471 Find similar reactions

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Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu

Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244 Title/Abstract Full Text View citing articles Show Details

in diethyl ether

T=20°C; addition of TMEDA or HMPA, preferred pathway tested; Product distribution;

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281

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Rx-ID: 1899472 Find similar reactions

Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu

Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244 Title/Abstract Full Text View citing articles Show Details

in diethyl ether

T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

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282

Synthesize Find similar Rx-ID: 1899473 Find similar reactions

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in diethyl ether

T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu

Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244 Title/Abstract Full Text View citing articles Show Details

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283

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Rx-ID: 1899474 Find similar reactions

Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu

Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244 Title/Abstract Full Text View citing articles Show Details

in diethyl ether

T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

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284

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Rx-ID: 1899475 Find similar reactions

Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu

Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 242 - 244 Title/Abstract Full Text View citing articles Show Details

in diethyl ether

T=20°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

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285

Synthesize Find similar Rx-ID: 2068011 Find similar reactions

With samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran

1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru

Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602 Title/Abstract Full Text View citing articles Show Details

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286

Synthesize Find similar Rx-ID: 2068102 Find similar reactions

B: 3%

With sodium formate; bis(η3-allyl-μ-chloropalladium(II)); polyether phosphine in water; toluene

T=100°C; 1 h; Yield given;

Okano, Tamon; Moriyama, Yoshiyuki; Konishi, Hisatoshi; Kiji, Jitsuo

Chemistry Letters, 1986 , p. 1463 - 1466 Title/Abstract Full Text Show Details

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287

Synthesize Find similar Rx-ID: 2101609 Find similar reactions

A: 17% B: 32% C: 19% D: 6%

in methanol

T=20°C; 72 h; electrolysis; Zn cathode, platinum anode; -1.8 V vs SCE; 0.1 mol/l Ba(ClO4)2;

Ismail, M. T.; Abdel-Wahab, A. A.; Mohamed, O. S.; Khalaf, A. A.

Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1174 - 1176 Title/Abstract Full Text Show Details

A: 17% B: 32% C: 19% D: 6%

in methanol

T=20°C; 72 h; electrolysis; Zn cathode, platinum anode; -1.8 V vs SCE; 0.1 mol/l Ba(ClO4)2;

Ismail, M. T.; Abdel-Wahab, A. A.; Mohamed, O. S.; Khalaf, A. A.

Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1174 - 1176 Title/Abstract Full Text Show Details

A: 17% B: 32% C: 19% D: 6%

in methanol

T=20°C; 72 h; electrolysis; Zn cathode, platinum anode; -1.8 V vs SCE; 0.1 mol/l Ba(ClO4)2;

Ismail, M. T.; Abdel-Wahab, A. A.; Mohamed, O. S.; Khalaf, A. A.

Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1174 - 1176 Title/Abstract Full Text Show Details

Hide Details

A: 17% B: 32% C: 19% D: 6%

in methanol

T=20°C; 72 h; electrolysis; Zn cathode, platinum anode; -1.8 V vs SCE; 0.1 mol/l Ba(ClO4)2;

Ismail, M. T.; Abdel-Wahab, A. A.; Mohamed, O. S.; Khalaf, A. A.

Bulletin de la Societe Chimique de France, 1985 , # 6 p. 1174 - 1176 Title/Abstract Full Text Show Details

A: 30 % Chromat. B: 35 % Chromat.

in methanol

T=20°C; 72 h; anodic oxidation; Product distribution;

Ismail, M. T.; Abdel-Wahab, A. A.; El-Khawaga, A. M.; Mohamed, O. S.; Khalaf, A. A.

Bulletin de la Societe Chimique de France, 1986 , # 1 p. 23 - 25 Title/Abstract Full Text Show Details

C: 5 % Chromat. D: 5 % Chromat. A

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288

Synthesize Find similar Rx-ID: 2137674 Find similar reactions

With sodium tetrahydroborate in diethylene glycol dimethyl ether; water

T=30°C; 1 h; regio- and stereoselectivity of various reductions of (E)- and (Z)-compounds; comparison with Grignard reactions; Product distribution;

Muraoka, Kiyoshige; Nojima, Masatomo; Kusabayashi, Shigekazu; Nagase, Shigeru

Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 761 - 768 Title/Abstract Full Text Show Details

289

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84%

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Rx-ID: 2546853 Find similar reactions

With lead(IV) acetate; copper diacetate in acetic acid; N,N-dimethyl-formamide

3 h; Ambient temperature;

Nishiyama, Hisao; Matsumoto, Makoto; Arai, Hiroyuki; Sakaguchi, Hisao; Itoh, Kenji

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1599 - 1602 Title/Abstract Full Text View citing articles Show Details

290

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81%

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With lead(IV) acetate; copper diacetate in acetic acid; N,N-dimethyl-formamide

9 h; Ambient temperature;

Rx-ID: 2578158 Find similar reactions

Nishiyama, Hisao; Matsumoto, Makoto; Arai, Hiroyuki; Sakaguchi, Hisao; Itoh, Kenji

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1599 - 1602 Title/Abstract Full Text View citing articles Show Details

291

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89%

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Rx-ID: 2580738 Find similar reactions

With lead(IV) acetate; copper diacetate in pyridine; dichloromethane

T=0°C; 6 h;

Nishiyama, Hisao; Matsumoto, Makoto; Arai, Hiroyuki; Sakaguchi, Hisao; Itoh, Kenji

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1599 - 1602 Title/Abstract Full Text View citing articles Show Details

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292

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Rx-ID: 3745452 Find similar reactions

B: 45%

With PdCl2lt;PPh2-m-C6H4-COONagt;2 in n-heptane; water

T=100°C; 5 h; Yields of byproduct given;

Okano, Tamon; Moriyama, Yoshiyuki; Konishi, Hisatoshi; Kiji, Jitsuo

Chemistry Letters, 1986 , p. 1463 - 1466 Title/Abstract Full Text Show Details

With PdCl2lt;polyether phosphinegt;2 in n-heptane; water

T=100°C; 3 h; variation of catalyst, organic phase, reaction time; Product distributionMechanism;

Okano, Tamon; Moriyama, Yoshiyuki; Konishi, Hisatoshi; Kiji, Jitsuo

Chemistry Letters, 1986 , p. 1463 - 1466 Title/Abstract Full Text Show Details

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293

Synthesize Find similar Rx-ID: 3745480 Find similar reactions

B: 27%

With sodium formate; bis(η3-allyl-μ-chloropalladium(II)); polyether phosphine in water; toluene

Okano, Tamon; Moriyama, Yoshiyuki; Konishi, Hisatoshi; Kiji, Jitsuo

T=100°C; 3 h; Yield given;

Chemistry Letters, 1986 , p. 1463 - 1466 Title/Abstract Full Text Show Details

294

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95%

Rx-ID: 6330293 Find similar reactions

With Cu(acac)2-PPh3 in tetrahydrofuran

Dzhemilev, U. M.; Ibragimov, A. G.; Saraev, R. A.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 397 - 401 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 429 - 433 Title/Abstract Full Text View citing articles Show Details

295

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Rx-ID: 21401935 Find similar reactions

Multi-step reaction with 2 steps 1: 53 percent / lithium di-isopropylamide / tetrahydrofuran; various solvent(s) / -78 - -10 °C 2: 84 percent / lead tetraacetate / cupric acetate / acetic acid; dimethylformamide / 3 h / Ambient temperature View Scheme

Nishiyama, Hisao; Matsumoto, Makoto; Arai, Hiroyuki; Sakaguchi, Hisao; Itoh, Kenji

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1599 - 1602 Title/Abstract Full Text View citing articles Show Details

Multi-step reaction with 2 steps 1: 71 percent / lithium di-isopropylamide / tetrahydrofuran; various solvent(s) / -78 - -10 °C 2: 89 percent / lead tetraacetate / cupric acetate / CH2Cl2; pyridine / 6 h / 0 °C View Scheme

Nishiyama, Hisao; Matsumoto, Makoto; Arai, Hiroyuki; Sakaguchi, Hisao; Itoh, Kenji

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1599 - 1602 Title/Abstract Full Text View citing articles Show Details

296

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Rx-ID: 1934909 Find similar reactions

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98%

With Cu(acac)2-PPh3 in tetrahydrofuran

T=40°C; 4 h;

Ibragimov, A. G.; Saraev, R. A.; Dzhemilev, U. M.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 199 - 201 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 211 - 213 Title/Abstract Full Text View citing articles Show Details

With Cu(acac)2-PPh3 in tetrahydrofuran

T=40°C; 4 h; effects of solvent, catalyst and catalyst activator; further solvents, further catalysts; Product distribution;

Ibragimov, A. G.; Saraev, R. A.; Dzhemilev, U. M.

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297

Synthesize Find similar Rx-ID: 2153388 Find similar reactions

A: 6% B: 79%

With RhCl(PPh3)3; lithium perchlorate in acetonitrile

17 h;

Yasui, Shinro; Nakamura, Kaoru; Fujii, Masayuki; Ohno, Atsuyoshi

Journal of Organic Chemistry, 1985 , vol. 50, # 18 p. 3283 - 3287 Title/Abstract Full Text View citing articles Show Details

A: 5.5 % Chromat. B: 79 % Chromat.

With N-propyl-1,4-dihydronicotinamide; lithium perchlorate; RhCl(PPh3)3 in acetonitrile

T=70°C; 17 h;

Nakamura, Kaoru; Ohno, Atsuyoshi; Oka, Shinzaburo

Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3335 - 3336 Title/Abstract Full Text View citing articles Show Details

A: 5.5 % Chromat. B: 79 % Chromat.

With N-propyl-1,4-dihydronicotinamide; lithium perchlorate; RhCl(PPh3)3 in acetonitrile

T=70°C; 17 h;

Nakamura, Kaoru; Ohno, Atsuyoshi; Oka, Shinzaburo

Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3335 - 3336 Title/Abstract Full Text View citing articles Show Details