Reaxys
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Reactions (11)
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Substances (13)
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Citations (13)
Conditions
References A
B
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1
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A: 12% B: 28%
2
With tetrapropylammonium perruthennate; 3 A molecular sieve; 4-methylmorpholine N-oxide in dichloromethane
T=20°C; Oxidation; 18 h;
Gill, Melvyn; Harte, Michael F.; Ten, Abilio
Australian Journal of Chemistry, 2000 , vol. 53, # 4 p. 245 256 Title/Abstract Full Text View citing articles Show Details
Synthesize Find similar 63%
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Rx-ID: 4769608 Find similar reactions
With jones reagent in acetone
T=0°C; 1 h;
Majetich, George; Liu, Shuang; Fang, Jing; Siesel, David; Zhang, Yong
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6928 6951 Title/Abstract Full Text View citing articles Show Details
3
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Rx-ID: 17131059 Find similar reactions
Multi-step reaction with 2 steps 1: 58 percent / n-BuLi, TMEDA / diethyl ether; hexane / 1.) room temperature, 6 h, 2.) room temperature, 8 h 2: 63 percent / Jones reagent / acetone / 1 h / 0 °C View Scheme
Majetich, George; Liu, Shuang; Fang, Jing; Siesel, David; Zhang, Yong
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6928 6951 Title/Abstract Full Text View citing articles Show Details
Multi-step reaction with 2 steps 1: 1.) trifluoromethanesulfonic acid (TFSA) / 1.) CH2Cl2, -40 deg C, 10 min, 2.) -78 deg C to 20 deg C 2: H2O, trifluoromethanesulfonic acid (TFSA) View Scheme
Okabe, Kazuaki; Ohwada, Tomohiko; Ohta, Toshiharu; Shudo, Koichi
Journal of Organic Chemistry, 1989 , vol. 54, # 4 p. 733 - 734 Title/Abstract Full Text View citing articles Show Details
4
Rx-ID: 3346538
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34%
With (bpy)NiBr2; tetra-n-butylammonium tetrafluoroborate
T=80°C; Al rod/nickel-sponge, electrolysis;
Durandetti; Sibille; Nedelec; Perichon
Synthetic Communications, 1994 , vol. 24, # 2 p. 145 - 151 Title/Abstract Full Text View citing articles Show Details
34%
With (bpy)NiBr2; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=70°C; i = 250 mA, nickel-sponge cathode;
Durandetti, Muriel; Nedelec, Jean-Yves; Perichon, Jacques
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1748 1755 Title/Abstract Full Text View citing articles Show Details
5
Synthesize Find similar 52%
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Rx-ID: 1798105 Find similar reactions
With hydrogen; acetic acid; nickel
T=25°C; 2 h;
Rosowsky, Andre; Mota, Clara E.; Wright, Joel E.; Freisheim, James H.; Heusner, James J.; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 21 p. 3103 3112 Title/Abstract Full Text View citing articles Show Details
With hydrogen; palladium on activated charcoal in ethanol
Coutts; Malicky
Canadian Journal of Chemistry, 1973 , vol. 51, # 9 p. 1402 1409 Title/Abstract Full Text View citing articles Show Details
6
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Rx-ID: 18743898 Find similar reactions
Multi-step reaction with 2 steps 1: 90 percent / NH4OAc / 7 h / 105 °C 2: 52 percent / H2, glacial AcOH / Raney Ni / 2 h / 25 °C View Scheme
Rosowsky, Andre; Mota, Clara E.; Wright, Joel E.; Freisheim, James H.; Heusner, James J.; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 21 p. 3103 3112 Title/Abstract Full Text View citing articles Show Details
Multi-step reaction with 2 steps 1: NH OAc / acetic acid
Coutts; Malicky
Canadian Journal of Chemistry, 1973 , vol. 51, # 9 p. 1402 -
4
1409 Title/Abstract Full Text View citing articles Show Details
2: H2 / Pd-C / ethanol View Scheme
7
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8
With trifluorormethanesulfonic acid; water
Yield given;
Rx-ID: 3528126 Find similar reactions
39%
Okabe, Kazuaki; Ohwada, Tomohiko; Ohta, Toshiharu; Shudo, Koichi
Journal of Organic Chemistry, 1989 , vol. 54, # 4 p. 733 - 734 Title/Abstract Full Text View citing articles Show Details
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With manganese triacetate; acetic acid
0.666667 h; Heating;
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Kurz, Michael E.; Baru, Vijayalakshmi; Nguyen, P-Nhi
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1603 1607 Title/Abstract Full Text View citing articles Show Details
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Rx-ID: 2556714 Find similar reactions
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9
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90%
With hydrogenchloride in methanol
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Rx-ID: 3704093 Find similar reactions
Shatzmiller, Shimon; Lidor, Ramy; Shalom, Eytan; Bahar,
Eliezer
Journal of the Chemical Society, Chemical Communications, 1984 , # 12 p. 795 - 796 Title/Abstract Full Text View citing articles Show Details
T=65°C; 10 h;
10
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Rx-ID: 7253745 Find similar reactions
Merck Co.Inc.
Patent: FR1496706 , 1962 ; Chem.Abstr., 1968 , vol. 69, # 36445n Full Text Show Details
Merck and Co.
Patent: BE614410 , 1962 ; Chem.Abstr., 1963 , vol. 59, # 1753 Full Text Show Details
Struck et al.
Tetrahedron Letters, 1967 , p. 1589,1590, 1591, 1593 Full Text View citing articles Show Details
11
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With chloroform; phosphorus pentachloride
Durch Eintragen der hergestellten Saeurechlorids in Benzol in aether. Diazomethan-Loesung und Behandeln einer Loesung des Reaktionsprodukts in Chloroform mit wss. HI;
Rx-ID: 384021 Find similar reactions
Weiss; Nord
Archives of Biochemistry, 1949 , vol. 22, p. 288,307 Full Text View citing articles Show Details