Bioactivities (2515)
Yield
Reactions (8)
Substances (12)
Targets (350)
Citations (42)
Conditions
References
1
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Rx-ID: 2013369
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100%
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite in acetonitrile
T=35°C; pH 6.7;
Zhao; Li; Mano; Song; Tschaen; Grabowski; Reider
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2564 - 2566 Title/Abstract Full Text View citing articles Show Details
100%
With sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical in aq. phosphate buffer; water; acetonitrile
T=35°C; pH=6.7; Green chemistry;
Zhao, Matthew M.; Li, Jing; Song, Zhiguo J.; Tschaen, David M.; Mano, Eiichi; Ghosh, Arun; Sieser, Jamie; Cai, Weiling; Kelly, Sarah E.
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2564 - 2566 Title/Abstract Full Text View citing articles Show Details
98%
With hydrogenchloride; 2,2,6,6-tetramethyl-piperidine-N-oxyl; Amberlite IRA 900 chlorite in dichloromethane
T=20°C; 4 h;
Kloth, Katrin; Bruenjes, Marco; Kunst, Eike; Joege, Thomas; Gallier, Florian; Adibekian, Alexander; Kirschning, Andreas
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 10 p. 1423 - 1434 Title/Abstract Full Text View citing articles Show Details
96%
With chromium(VI) oxide; periodic acid in water; acetonitrile
T=0°C;
Zhao, Mangzhu; Li, Jing; Song, Zhiguo; Desmond, Richard; Tschaen, David M.; Grabowski, Edward J. J.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5323 - 5326 Title/Abstract Full Text View citing articles Show Details
96%
With chromium(VI) oxide; periodic acid in water; acetonitrile
T=0°C; oxidation of various alcohols; Product distribution;
Zhao, Mangzhu; Li, Jing; Song, Zhiguo; Desmond, Richard; Tschaen, David M.; Grabowski, Edward J. J.; Reider, Paul J.
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5323 - 5326 Title/Abstract Full Text View citing articles Show Details
93%
With ruthenium trichloride; sodium periodate in ethyl acetate; acetonitrile
T=20°C; Oxidation; 2 h;
Prashad, Mahavir; Lu, Yansong; Kim, Hong-Yong; Hu, Bin; Repic, Oljan; Blacklock, Thomas J.
Synthetic Communications, 1999 , vol. 29, # 17 p. 2937 - 2942 Title/Abstract Full Text View citing articles Show Details
91%
With sodium tetrahydroborate; 1 Pd/C; water; potassium hydoxide in methanol
T=20°C; 17 h; In air;
An, Gwangil; Ahn, Hyunseok; De Castro, Kathlia A.; Rhee, Hakjune
Synthesis, 2010 , # 3 art. no. F19009SS, p. 477 - 485 Title/Abstract Full Text View citing articles Show Details
90%
Stage #1: With C29H44Cl2N2Ru; sodium hydroxide in water
24 h; Reflux; Stage #2: With hydrogenchloride in water
Malineni, Jagadeesh; Keul, Helmut; Möller, Martin
Dalton Transactions, 2015 , vol. 44, # 39 p. 17409 - 17414 Title/Abstract Full Text View citing articles Show Details
78%
Stage #1: With C20H28ClN2OPRu; water; sodium hydroxide
18 h; Inert atmosphereReflux; Stage #2: Acidic conditions;
Balaraman, Ekambaram; Khaskin, Eugene; Leitus, Gregory; Milstein, David
Nature Chemistry, 2013 , vol. 5, # 2 p. 122 - 125 Title/Abstract Full Text View citing articles Show Details
75%
Stage #1: With [RuCl2(p-cymene)(iPr2-imy)]; tricyclohexylphosphine tetrafluoroborate; potassium hydoxide in toluene
24 h; Schlenk techniqueInert atmosphereReflux; Stage #2: With hydrogenchloride in water
pH=1; Reagent/catalyst;
Santilli, Carola; Makarov, Ilya S.; Fristrup, Peter; Madsen, Robert
Journal of Organic Chemistry, 2016 , vol. 81, # 20 p. 9931 - 9938 Title/Abstract Full Text View citing articles Show Details
40%
With sodium bromate; hydrogen bromide; tert-butyl alcohol in tetrachloromethane; water
2 h; Ambient temperature;
Veeraiah, T.; Periasamy, M.
Synthetic Communications, 1989 , vol. 19, # 11-12 p. 2151 - 2158 Title/Abstract Full Text Show Details
With acetobacter sp. ALEG in water
3 h;
Gandolfi, Raffaella; Ferrara, Nicola; Molinari, Francesco
Tetrahedron Letters, 2001 , vol. 42, # 3 p. 513 - 514 Title/Abstract Full Text View citing articles Show Details
With N -hydroxyphthalimide; oxygen; benzaldehyde; nickel-cobalt-chromium in acetic acid
T=22°C; P=750.06 Torr; 7 h;
De Vondervoort, Lizette Schmieder-van; Bouttemy, Sabine; Heu, Ferdinand; Weissenboeck, Kurt; Alsters, Paul L.
European Journal of Organic Chemistry, 2003 , # 3 p. 578 - 586 Title/Abstract Full Text View citing articles Show Details
With ruthenium trichloride; (NH4)2Ce(NO3)2; nitric acid in acetonitrile
T=24.85°C; Kinetics;
Rao, N. Vijaya Bhaskar; Rao, M. Anand
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2005 , vol. 44, # 1 p. 80 - 84 Title/Abstract Full Text View citing articles Show Details
With NADH oxidase; nicotinamide adenine dinucleotide; 2-phenylethanol dehydrogenase; phenylacetaldehyde dehydrogenase T=25°C; P=760.051 Torr; pH=9.0; 12 h;
Hirano, Jun-ichiro; Miyamoto, Kenji; Ohta, Hiromichi
Tetrahedron Letters, 2008 , vol. 49, # 7 p. 1217 - 1219 Title/Abstract Full Text View citing articles Show Details
With Oxone in water
T=70°C; 21 h; chemoselective reaction;
Wu, Shang; Ma, Hengchang; Lei, Ziqiang
Synlett, 2010 , # 18 p. 2818 - 2822 Title/Abstract Full Text View citing articles Show Details
Multi-step reaction with 2 steps 1: oxygen / 5 h / 120 °C / Neat (no solvent) 2: oxygen / 5 h / 120 °C / Neat (no solvent) View Scheme
Choudhary, Vasant R.; Dumbre, Deepa K.
Catalysis Communications, 2011 , vol. 13, # 1 p. 82 - 86 Title/Abstract Full Text View citing articles Show Details
With Acetobacter sp. MIM 2000/61 in water
T=28°C; pH=7.5; 1 h; phosphate bufferEnzymatic reaction;
Zambelli, Paolo; Pinto, Andrea; Romano, Diego; Crotti, Elena; Conti, Paola; Tamborini, Lucia; Villa, Raffaella; Molinari, Francesco
33 % Chromat.
86 % Chromat.
Green Chemistry, 2012 , vol. 14, # 8 p. 2158 - 2161 Title/Abstract Full Text View citing articles Show Details
With tetrakis(tetrabutylammonium)decatungstate(VI); dihydrogen peroxide in water; 1,2-dichloro-ethane
T=80°C; 0.25 h; Microwave irradiation; Catalytic behavior; Time;
Galica, Mateusz; Kasprzyk, Wiktor; Bednarz, Szczepan; Bogdal, Dariusz
Chemical Papers, 2013 , vol. 67, # 9 p. 1240 - 1244 Title/Abstract Full Text View citing articles Show Details
With oxygen in toluene
T=100°C; P=7500.75 Torr; 24 h;
Wang, Min; Wang, Feng; Ma, Jiping; Chen, Chen; Shi, Song; Xu, Jie
Chemical Communications, 2013 , vol. 49, # 59 p. 6623 - 6625 Title/Abstract Full Text View citing articles Show Details
With iridium(III) chloride; cerium(IV) sulphate; sulfuric acid; acetic acid
T=35°C; Kinetics; Concentration;
Tandon, Praveen K.; Dwivedi, Priv B.; Singh, Santosh B.; Yadav, Suresh C.
Journal of the Indian Chemical Society, 2013 , vol. 90, # 12 p. 2237 - 2245 Title/Abstract Full Text View citing articles Show Details
With E. coli perisplasmic aldehyde oxidase; F. graminearum galactose oxidase; catalase in aq. phosphate buffer; acetonitrile
T=37°C; pH=7; 10 h; Enzymatic reaction;
McKenna, Shane M.; Leimkühler, Silke; Herter, Susanne; Turner, Nicholas J.; Carnell, Andrew J.
Green Chemistry, 2015 , vol. 17, # 6 p. 3271 - 3275 Title/Abstract Full Text View citing articles Show Details
75 %Spectr.
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; laccase from Trametes versicolor; oxygen in water
T=20°C; 144 h; Enzymatic reaction;
Galletti, Paola; Pori, Matteo; Funiciello, Federica; Soldati, Roberto; Ballardini, Alberto; Giacomini, Daria
ChemSusChem, 2014 , vol. 7, # 9 p. 2684 - 2689 Title/Abstract Full Text View citing articles Show Details
99 %Spectr.
With oxygen; potassium hydoxide in methanol; water
T=50°C; P=760.051 Torr; 16 h;
Ahmed, Maaz S.; Mannel, David S.; Root, Thatcher W.; Stahl, Shannon S.
Organic Process Research and Development, 2017 , vol. 21, # 9 p. 1388 - 1393 Title/Abstract Full Text View citing articles Show Details
A
B
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2
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A: 2 % Spectr. B: 37%
With 1H-imidazole; [bis(acetoxy)iodo]benzene in dichloromethane
T=20°C; 1 h;
Karimipour, Gholam Reza; Shadegan, Hamid Asadpour; Ahmadpour, Roxana
Journal of Chemical Research, 2007 , # 4 p. 252 - 256 Title/Abstract Full Text View citing articles Show Details
A: 26% B: 5%
With diphenylether; Fe(TAML)Li; [bis(acetoxy)iodo]benzene; water in acetone
T=25°C; 1 h; Green chemistry;
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787 Title/Abstract Full Text View citing articles Show Details
A: 13 % Chromat. B: 87 % Chromat.
With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; sodium chloride; potassium bromide in dichloromethane; water
1) 0 deg C, 1h, 20 deg C, 20 min;
Siedlecka; Skarzewski; Mlochowski
Tetrahedron Letters, 1990 , vol. 31, # 15 p. 2177 - 2180 Title/Abstract Full Text View citing articles Show Details
With tert.-butylhydroperoxide; [O-Cu4(triethanolamine)4(BOH)4][BF4]2 in acetonitrile
T=69.84°C; 19 h; Title compound not separated from byproducts.;
Zhu, Mingxia; Li, Bodong; He, Ping; Wei, Xin; Yuan, Youzhu
Tetrahedron, 2008 , vol. 64, # 39 p. 9239 - 9243 Title/Abstract Full Text View citing articles Show Details
With CpMo(CO)3(CCPh); dihydrogen peroxide in water
T=80°C; 8 h; chemoselective reaction;
Biradar, Ankush V.; Dongare, Mohan K.; Umbarkar, Shubhangi B.
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2885 - 2888 Title/Abstract Full Text View citing articles Show Details
Stage #1: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; carbon
Sonication; Stage #2: With nitric acid in water
T=50°C; 5 h;
Kuang, Yongbo; Rokubuichi, Hodaka; Nabae, Yuta; Hayakawa, Teruaki; Kakimoto, Masa-Aki
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2635 - 2642 Title/Abstract Full Text View citing articles Show Details
With Gluconobacter oxydans DSM 2343 in water
T=28°C; pH=7.5; 5 h; phosphate bufferEnzymatic reaction;
Zambelli, Paolo; Pinto, Andrea; Romano, Diego; Crotti, Elena; Conti, Paola; Tamborini, Lucia; Villa, Raffaella; Molinari, Francesco
Green Chemistry, 2012 , vol. 14, # 8 p. 2158 - 2161 Title/Abstract Full Text View citing articles Show Details
With tetrakis(tetrabutylammonium)decatungstate(VI); dihydrogen peroxide in water; acetonitrile
T=135 - 140°C; P=25502.6 - 27002.7 Torr; 0.25 h; Microwave irradiation; Catalytic behavior; TemperaturePressureTime;
Galica, Mateusz; Kasprzyk, Wiktor; Bednarz, Szczepan; Bogdal, Dariusz
Chemical Papers, 2013 , vol. 67, # 9 p. 1240 - 1244 Title/Abstract Full Text View citing articles Show Details
With E. coli perisplasmic aldehyde oxidase; F. graminearum galactose oxidase; catalase in aq. phosphate buffer; acetonitrile
T=37°C; pH=7; Enzymatic reaction;
McKenna, Shane M.; Leimkühler, Silke; Herter, Susanne; Turner, Nicholas J.; Carnell, Andrew J.
Green Chemistry, 2015 , vol. 17, # 6 p. 3271 - 3275 Title/Abstract Full Text View citing articles Show Details
A
B
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3
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A: 8% B: 82%
With oxygen; sodium t-butanolate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride in dichloromethane
T=20°C; 30 h; Molecular sieve; Reagent/catalyst; Hide Experimental Procedure
Yu, Dong-Fang; Xing, Ping; Jiang, Biao
Tetrahedron, 2015 , vol. 71, # 25 p. 4269 - 4273 Title/Abstract Full Text View citing articles Show Details
4.3. General procedure for the oxidation of the long chainalcohol 3a-3h
General procedure: Under Oxygen atmosphere, alcohol (2 mmol), precatalyst(SIMesHCl or SIPrHCl, 0.06 mmol), NaOtBu (960.5 mg, 10 mmol),and 1 g 3 A molecular sieve were added to dichloromethane(20 mL). This solution was allowed to stir for 30 h. After filtratingthrough a pad of Celite, the cake was added to hydrochloric acid(2N, 50 mL) and extracted with ethyl acetate (50 mL3). The organic layer was dried over Na2SO4 and concentrated under reduced pressure. A: 34 % Spectr. B: 19 % Spectr.
With sodium hydroxide
T=50°C; Electrochemical reaction; Product distribution; Further Variations:Temperatures;
A
Lyalin; Petrosyan
Russian Chemical Bulletin, 2007 , vol. 56, # 3 p. 499 - 503 Title/Abstract Full Text View citing articles Show Details
B
4
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5
Hofmann, Christine; Schümann, Jan M.; Schreiner, Peter R.
Journal of Organic Chemistry, 2015 , vol. 80, # 3 p. 1972 - 1978 Title/Abstract Full Text View citing articles Show Details
A
B
C
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Rx-ID: 28389140
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C: 80.4 %Chromat.
With (4,5-bis-(di-iso-propylphosphinomethyl)acridine)RuH(CO)Cl; ammonia; water
T=135°C; P=5700.38 Torr; 36 h; Inert atmosphere;
Gunanathan, Chidambaram; Milstein, David
Angewandte Chemie - International Edition, 2008 , vol. 47, # 45 p. 8661 - 8664 Title/Abstract Full Text View citing articles Show Details
A
B
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Synthesize Find similar Rx-ID: 4437093
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With Boc-L-(π-Me)-His-AGly-L-Cha-L-Phe-NH-TEMPO; 3-chloro-benzenecarboperoxoic acid in toluene
T=20°C; 15 h;
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6
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A: 50% B: 47%
With dihydrogen peroxide; methyltrioxorhenium (VII)
48 h;
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Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7728 - 7732 Title/Abstract Full Text View citing articles Show Details
A
B
C
D
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7
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A: 51% C: 17%
With dihydrogen peroxide; methyltrioctylammonium tetrakis(oxodiperoxotungsto)phosphate
T=90°C; 6 h;
Venturello, Carlo; Gambaro, Mario
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5924 - 5931 Title/Abstract Full Text View citing articles Show Details
A
B
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8
Synthesize Find similar Rx-ID: 7441838
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Grignard
Patent: DE164883 ; Full Text Show Details
Walbaum
Chemische Berichte, 1900 , vol. 33, p. 2300 Full Text Show Details
Grimal
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 144, p. 434 Full Text Show Details
v. Soden; Rojahn Chemische Berichte, 1900 , vol. 33, p. 1723 Full Text Show Details Radziszewski Chemische Berichte, 1876 , vol. 9, p. 373 Full Text View citing articles Show Details Grignard Annales de Chimie (Cachan, France), 1907 , vol. <8> 10, p. 30 Chem. Zentralbl., 1905 , vol. 76, # II p. 1751 Full Text View citing articles Show Details Grignard Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 141, p. 45 Annales de Chimie (Cachan, France), 1907 , vol. <8> 10, p. 30 Chem. Zentralbl., 1905 , vol. 76, # II p. 1751 Full Text View citing articles Show Details