N-Hydroxy-1-phenyl-2-propanimine (1-Phenylpropan-2-one oxime) [C9H11NO]

Page 1

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Reactions (37)

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Substances (33)

Targets (7)

Conditions

Citations (49)

References

1

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Rx-ID: 1040193 Find similar reactions

94%

With hydrogen in ethanol

T=60°C; P=15001.5 Torr; 0.333333 h; Autoclave; chemoselective reaction;

Ren, Yujing; Wei, Haisheng; Yin, Guangzhao; Zhang, Leilei; Wang, Aiqin; Zhang, Tao

Chemical Communications, 2017 , vol. 53, # 12 p. 1969 - 1972 Title/Abstract Full Text View citing articles Show Details

91%

With sulfuric acid in water; isopropyl alcohol

T=10 - 15°C; electrolysis;

Wessling, Michael; Schaefer, Hans J.

Chemische Berichte, 1991 , vol. 124, # 10 p. 2303 - 2306 Title/Abstract Full Text Show Details

82%

With sodium stannite in tetrahydrofuran; water

0.416667 h; Ambient temperature;

Varma, Rajender S.; Varma, Manju; Kabalka, George W.

Tetrahedron Letters, 1985 , vol. 26, # 49 p. 6013 - 6014 Title/Abstract Full Text View citing articles Show Details

81%

With zinc(II) tetrahydroborate in DME

6 h; Ambient temperature;

Ranu, Brindaban C.; Chakraborty, Rupak

Tetrahedron Letters, 1991 , vol. 32, # 29 p. 3579 - 3582 Title/Abstract Full Text View citing articles Show Details


81%

With zinc(II) tetrahydroborate in DME

T=25°C; 6 h;

Ranu; Chakraborty

Tetrahedron, 1992 , vol. 48, # 25 p. 5317 - 5322 Title/Abstract Full Text View citing articles Show Details

81%

With zinc(II) tetrahydroborate in DME

6 h; Ambient temperatureother α-substituted nitroalkenes;

Ranu, Brindaban C.; Chakraborty, Rupak

Tetrahedron Letters, 1991 , vol. 32, # 29 p. 3579 - 3582 Title/Abstract Full Text View citing articles Show Details

81%

With zinc(II) tetrahydroborate in DME

T=25°C; 6 h; other disubstituted nitroalkenes; Mechanism;

Ranu; Chakraborty

Tetrahedron, 1992 , vol. 48, # 25 p. 5317 - 5322 Title/Abstract Full Text View citing articles Show Details

67%

With sodium hypophosphite; palladium on activated charcoal in tetrahydrofuran

3 h; Ambient temperature;

Varma, Rajender S.; Varma, Manju; Kabalka, George W.

Synthetic Communications, 1986 , vol. 16, # 1 p. 91 - 96 Title/Abstract Full Text Show Details

With hydrogenchloride; tin(ll) chloride in methanol

T=-5°C;

Dornow,A.; Mueller,A.

Chemische Berichte, 1960 , vol. 93, p. 32 - 40 Full Text View citing articles Show Details

2

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Rx-ID: 780138 Find similar reactions

81%

With hydroxylamine hydrochloride; sodium carbonate in ethanol; water

24 h; Heating;

Langhals, Heinz; Range, Guenter; Wistuba, Eckehardt; Ruechardt, Christoph

Chemische Berichte, 1981 , vol. 114, # 12 p. 3813 - 3830 Title/Abstract Full Text Show Details

80%

With hydroxylamine hydrochloride; silica gel; tert-butanol

0.183333 h;

Kiasat, Ali Reza; Kazemi, Foad; Nourbakhsh, Kazem

Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 6 p. 1193 - 1196 Title/Abstract Full Text View citing articles Show Details

80%

With Zincite; hydroxylamine hydrochloride; silica gel in neat (no solvent) T=20°C; 0.05 h; Green chemistry; Hide Experimental Procedure

Kiasat, Ali Reza; Javaherian, Mohammad; Daei, Mina; Farbod, Mansoor

Revue Roumaine de Chimie, 2015 , vol. 60, # 9 p. 875 - 880 Title/Abstract Full Text View citing articles Show Details

2. General procedure for preparation of oximes from aldehydes and ketones in the presence of ZnO nanotubes under solvent free condition General procedure: Hydroxylamine hydrochloride (0.138 g, 2 mmol), ZnO nanotubes (0.071 g, 0.8 mmol), silica gel (0.43 g) and aldehyde (ketone) (1 mmol) were ground together in a mortar with a pestle at room temperature for a period of time as indicated in Tables 1 and 2. The progress of the reaction was monitored by TLC. After complete disappearance of the starting materials, the reaction mixture was poured with diethyl ether (2×10 mL) and filtered to remove silica gel and ZnO nanotubes, The filtrate mixed with water and extracted. The solvent was removed in vaccuo to give the product which was recrystallized from suitable solvent and afforded the TLC and 1H-NMR pure products in 75-98 percent isolated yields.

47%

With hydroxylamine hydrochloride; sodium acetate in ethanol

T=20°C; 4 h;

Portela-Cubillo, Fernando; Lymer, James; Scanlan, Eoin M.; Scott, Jackie S.; Walton, John C.

Tetrahedron, 2008 , vol. 64, # 52 p. 11908 - 11916 Title/Abstract Full Text View citing articles Show Details

18%

With hydroxylamine hydrochloride; sodium hydroxide in ethanol; water

1 h; Reflux;

Yamamoto, Yutaro; Hasegawa, Hiroto; Yamataka, Hiroshi

Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4652 - 4660 Title/Abstract Full Text View citing articles Show Details


With ethanol; hydroxylamine hydrochloride; sodium carbonate

Kolb

Justus Liebigs Annalen der Chemie, 1896 , vol. 291, p. 267 Full Text View citing articles Show Details

Dollfus

Chemische Berichte, 1892 , vol. 25, p. 1918 Chemische Berichte, 1893 , vol. 26, p. 1971 Full Text View citing articles Show Details

With ethanol; hydroxylamine hydrochloride; water; sodium acetate

Neber; v. Friedolsheim

Justus Liebigs Annalen der Chemie, 1926 , vol. 449, p. 129 Full Text View citing articles Show Details

With sodium hydroxide; hydroxylamine hydrochloride

Hey

Journal of the Chemical Society, 1930 , p. 18,20 Full Text View citing articles Show Details

With sodium hydroxide; hydroxylamine in water

0.25 h; Yield given;

Lozynski, Marek; Rusinska-Roszak, Danuta

Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 625 - 630 Title/Abstract Full Text Show Details

With pyridine; hydroxylamine hydrochloride in ethanol

Condensation; Heating;

Katritzky, Alan R.; Cui, Xilin; Long, Qiuhe; Yang, Baozhen; Wilcox, Allan L.; Zhang, Yong-Kang

Organic Preparations and Procedures International, 2000 , vol. 32, # 2 p. 175 - 183 Title/Abstract Full Text View citing articles Show Details

With hydroxylamine hydrochloride; sodium acetate in methanol; water

T=20°C;

Xuan, Jun; Xia, Xu-Dong; Zeng, Ting-Ting; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing

Angewandte Chemie - International Edition, 2014 , vol. 53, # 22 p. 5653 - 5656 Angew. Chem., 2014 , vol. 126, # 22 p. 5759 - 5762,4 Title/Abstract Full Text View citing articles Show Details

A

B

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3

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Multi-step reaction with 2 steps 1: N-butylamine / ethanol / |Reflux 2: acetic acid; tetraethylammonium tetrafluoroborate / DMFA; water / 20 °C / |Electrolysis View Scheme

A

4

Wessling, Michael; Schäfer, Hans J.

Beilstein Journal of Organic Chemistry, 2015 , vol. 11, p. 1163 - 1174 Title/Abstract Full Text View citing articles Show Details

B


Synthesize Find similar Rx-ID: 41124393 Find similar reactions

A: 20% B: 24%

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With tetraethylammonium tetrafluoroborate; acetic acid in water; DMFA

T=20°C; Electrolysis; Concentration; Hide Experimental Procedure

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Wessling, Michael; Schäfer, Hans J.

Beilstein Journal of Organic Chemistry, 2015 , vol. 11, p. 1163 - 1174 Title/Abstract Full Text View citing articles Show Details

Electrolyses

General procedure: The cathodic hydrodimerization is performed based on the results of the experiments shown in Tables 1 and 2 (Theoretical part) in an undivided cell (Figure 1a without diaphragm) at a mercury pool cathode at T = 0 °C (outside cooling). Electrolyte was a 0.2 M solution of tetraethylammonium p-toluenesulfonate (TEA-pTos) in DMF. The supporting electrolyte contained 2 percent water, is hygroscopic and was not dried. DMF is also not dried. To remove free amines the solvent was purged for some time with dry nitrogen gas. The supporting electrolyte is purged before the electrolyis for 10 min with nitrogen to remove dissolved oxygen. The given amount of substrate dissolved in 20 mL supporting electrolyte is given into the cell. The Luggin capillary is filled with electrolyte and positioned close to the cathode. Subsequently the anode is placed in the cell with a distance of 1 cm to the mercury surface. It is secured that in spite of the small distance to the cathode stirring of the mercury pool (500 t/min) can be done without disturbances of the current flow. Under argon the solution of the olefin is electrolyzed at the given potential until the current has decreased to 1–10 mA (istart = 250–450 mA). During the reduction – especially when stirring is stopped – at the cathode a deep colouring of the solution being red, brown or violet depending on the olefin can be observed. It diffuses into the solution and is discoloured at the anode. In the course of the electrolysis this leads to the colouring of the electrolyte. A

B

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5

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With tin(ll) chloride in acetone

0.75 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Varma, Rajender S.; Varma, Manju; Gai, Yuan-Zhu; Kabalka, George W.

Heterocycles, 1986 , vol. 24, # 9 p. 2581 - 2586 Title/Abstract Full Text View citing articles Show Details

With chromium dichloride; hydrogenchloride in tetrahydrofuran

0.166667 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Varma, Rajender S.; Varma, Manju; Kabalka, George W.

Synthetic Communications, 1985 , vol. 15, # 14 p. 1325 - 1332 Title/Abstract Full Text Show Details

With sodium hydrogencarbonate; tin(ll) chloride

1.) acetone, RT, 45 min, 2.) acetone, pH=8, 15 min; Yield given. Multistep reaction. Yields of byproduct given;

Varma, Rajender S.; Varma, Manju; Gai, Yuan-Zhu; Kabalka, George W.

Heterocycles, 1986 , vol. 24, # 9 p. 2581 - 2586 Title/Abstract Full Text View citing articles Show Details

With 5 palladium on charcoal; ammonium formate in methanol; toluene

T=20°C; Inert atmosphere; Overall yield = 72 percent; Overall yield = 8.6 g; Hide Experimental Procedure

Cai, Zhihua; Liu, Guodu; Jiao, Guangjun; Senanayake, Chris H.; Tang, Wenjun

Synthesis (Germany), 2013 , vol. 45, # 24 art. no. SS-2013-H0581-OP, p. 3355 - 3360 Title/Abstract Full Text View citing articles Show Details


Reduction of Nitroalkenes to Oximes 2; General Procedure15

General procedure: To a dry three-necked flask was charged nitroalkene (80 mmol), dryammonium formate (25.2 g, 400 mmol) and MeOH–toluene (1:1, 200 mL). Pd/C (9.5 g, 5 molpercent, wet) was added to the solution under stirring. The resulting mixture was stirred at r.t. until the complete disappearance of the starting material. The mixture was filtered and the filter cake was washed with CH2Cl2 (50 mL). The combined filtrates were concentrated, retreated with CH2Cl2 (50 mL), filtered to remove the insoluble salt, and concentrated. The residue was purified by column chromatography (silica gel, hexanes–EtOAc, 15:1) to afford the desired product as a mixture of E/Z isomers (E/Z 0.8:1 to 2.8:1).

6

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Rx-ID: 37546659 Find similar reactions

With hydroxylamine in water; isopropyl alcohol

T=140°C;

Loiseau, Francis; Beauchemin, Andre M.

Organic Syntheses, 2013 , vol. 90, p. 87 - 95 Title/Abstract Full Text View citing articles Show Details

A

B

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7

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With glucose-6-phosphate dehydrogenase; G-6-P; wild type pentaerythritol tetranitrate reductase; NADPH in N,Ndimethyl-formamide

T=30°C; 4 h; phosphate bufferInert atmosphereanaerobicEnzymatic reaction; enantioselective reaction;

Toogood, Helen S.; Fryszkowska, Anna; Hulley, Martyn; Sakuma, Michiyo; Mansell, David; Stephens, Gill M.; Gardiner, John M.; Scrutton, Nigel S.

ChemBioChem, 2011 , vol. 12, # 5 p. 738 - 749 Title/Abstract Full Text View citing articles Show Details

A

B

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8

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A: 41% B: 10%

With palladium 10 on activated carbon; hydrogen in methanol

T=20°C; 0.666667 h;

Durchschein, Katharina; Ferreira-Da Silva, Bianca; Wallner, Silvia; MacHeroux, Peter; Kroutil, Wolfgang; Glueck, Silvia Maria; Faber, Kurt

Green Chemistry, 2010 , vol. 12, # 4 p. 616 - 619 Title/Abstract Full Text View citing articles Show Details

9

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With hydroxylamine in water; isopropyl alcohol

T=110°C; 18.0833 h; Inert atmosphere; regioselective reaction;

Rx-ID: 28612839 Find similar reactions

Moran, Joseph; Pfeiffer, Jennifer Y.; Gorelsky, Serge I.; Beauchemin, Andre M.

Organic Letters, 2009 , vol. 11, # 9 p. 1895 - 1898 Title/Abstract Full Text View citing articles Show Details

A

B

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10

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A: 5% B: 53%

With hydroxylamine in isopropyl alcohol

T=140°C; intermolecular Cope-type hydroamination; 10 h; microwave irradiation;

Beauchemin, Andre M.; Moran, Joseph; Lebrun, Marie-Eve; Seguin, Catherine; Dimitrijevic, Elena; Zhang, Lili; Gorelsky, Serge I.

Angewandte Chemie - International Edition, 2008 , vol. 47, # 8 p. 1410 - 1413 Title/Abstract Full Text View citing articles Show Details

A

B

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11

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A: 53% B: 5%

With hydroxylamine in water; isopropyl alcohol

T=140°C; Cope-type hydroamination; Microwave irradiationInert atmosphere; regioselective reaction;

Moran, Joseph; Gorelsky, Serge I.; Dimitrijevic, Elena; Lebrun, Marie-Eve; Bedard, Anne-Catherine; Seguin, Catherine; Beauchemin, Andre M.

Journal of the American Chemical Society, 2008 , vol. 130, # 52 p. 17893 - 17906 Title/Abstract Full Text View citing articles Show Details

A

B

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12

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A: 5% B: 90%

With hydroxylamine hydrochloride; iron(III) chloride

T=50°C; 0.333333 h;

Eshghi, Hossein; Hassankhani, Asadollah

Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 575 - 579 Title/Abstract Full Text View citing articles Show Details

With hydroxylamine hydrochloride; sodium carbonate in tetrahydrofuran; water

2 h; Title compound not separated from byproducts;

Cashman, John R.; Xiong, Yeng N.; Lifen, Xu; Janowsky, Aaron

Journal of Pharmacology and Experimental Therapeutics, 1999 , vol. 288, # 3 p. 1251 - 1260 Title/Abstract Full Text View citing articles Show Details

A

B

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13

Synthesize Find similar Rx-ID: 8621051 Find similar reactions

With indium; ammonium chloride in methanol

Reduction; 3 h; Heating; Title compound not separated from byproducts;

14

Yadav; Subba Reddy; Srinivas; Ramalingam

Synlett, 2000 , # 10 p. 1447 - 1449 Title/Abstract Full Text View citing articles Show Details


Synthesize Find similar 67%

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Rx-ID: 5144276 Find similar reactions

Hwu, Jih Ru; Tseng, Wen Nan; Patel, Himatkumar V.; Wong, Fong Fuh; Horng, Den-Nan; Liaw, Ben Ruey; Lung Ching, Lin

Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2211 - 2218 Title/Abstract Full Text View citing articles Show Details

With n-butyllithium; hexamethyl-silane in tetrahydrofuran; hexane

24 h; Ambient temperature;

A

B

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15

Synthesize Find similar Rx-ID: 3984410 Find similar reactions

A: 50 % Spectr. B: 50 % Spectr.

With oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline in dichloromethane

T=0°C; 0.25 h;

Hanquet, Gilles; Lusinchi, Xavier

Tetrahedron, 1994 , vol. 50, # 42 p. 12185 - 12200 Title/Abstract Full Text View citing articles Show Details

16

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Multi-step reaction with 2 steps 1: n-BuNH2 / ethanol / Heating; or HOAc, NH4OAc 2: 91 percent / 0.1 M H2SO4 / propan-2-ol; H2O / 10 - 15 °C / electrolysis View Scheme

17

Rx-ID: 20915506 Find similar reactions

Wessling, Michael; Schaefer, Hans J.

Chemische Berichte, 1991 , vol. 124, # 10 p. 2303 - 2306 Title/Abstract Full Text Show Details


Synthesize Find similar 94%

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With ammonium formate; palladium on activated charcoal in tetrahydrofuran; methanol

0.33 h; Ambient temperature;

Rx-ID: 1553469 Find similar reactions

Kabalka, George W.; Pace, R. David; Wadgaonkar, P.P.

Synthetic Communications, 1990 , vol. 20, # 16 p. 2453 - 2458 Title/Abstract Full Text Show Details

A

B

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18

Synthesize Find similar Rx-ID: 2153011 Find similar reactions

A: 34% B: 35%

With ammonium formate; palladium on activated charcoal in tetrahydrofuran; methanol

2.5 h; Ambient temperature;

Kabalka, George W.; Pace, R. David; Wadgaonkar, P.P.

Synthetic Communications, 1990 , vol. 20, # 16 p. 2453 - 2458 Title/Abstract Full Text Show Details

A

B

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19

Synthesize Find similar Rx-ID: 1553470 Find similar reactions

A: 85% B: 4%

With sodium dithionite; 1,1'-di-n-octyl-4,4'-bipyridinium dibromide in water; ethyl acetate

1 h;

A

20

Synthesize

Tomioka, Hideo; Ueda, Koichi; Ohi, Hirofumi; Izawa, Yasuji

Chemistry Letters, 1986 , p. 1359 - 1362 Title/Abstract Full Text Show Details

B


Find similar Rx-ID: 1554138 Find similar reactions

A: 79%

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With sodium hydroxide; hydroxylamine in water; isopropyl alcohol

1 h; Ambient temperature;

Synthesize Find similar

Lozynski, Marek; Rusinska-Roszak, Danuta

Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 625 - 630 Title/Abstract Full Text Show Details

A

B

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21

Synthesize Find similar Rx-ID: 1716247 Find similar reactions

A: 3%

With sodium hydroxide; hydroxylamine; tert-butylamine hydrochloride in water; isopropyl alcohol

T=80°C; 2 h;

Lozynski, Marek; Rusinska-Roszak, Danuta

Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 625 - 630 Title/Abstract Full Text Show Details

A

B

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Synthesize Find similar

22

Synthesize Find similar Rx-ID: 2070996 Find similar reactions

A: 40% B: 30%

With sodium hypophosphite; palladium on activated charcoal in tetrahydrofuran

0.5 h; Ambient temperature;

A

23

Varma, Rajender S.; Varma, Manju; Kabalka, George W.

Synthetic Communications, 1986 , vol. 16, # 1 p. 91 - 96 Title/Abstract Full Text Show Details

B


Synthesize Find similar Rx-ID: 3935132 Find similar reactions

A: 57%

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Synthesize Find similar

With sodium hydroxide; hydroxylamine in water; isopropyl alcohol

0.25 h; Ambient temperature;

Lozynski, Marek; Rusinska-Roszak, Danuta

Polish Journal of Chemistry, 1986 , vol. 60, # 4-6 p. 625 - 630 Title/Abstract Full Text Show Details

A

B

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Synthesize Find similar

24

Synthesize Find similar Rx-ID: 1986971 Find similar reactions

A: 43% B: 6%

With sulfuric acid; toluene-4-sulfonic acid in methanol

T=0 - 5°C; ceramic diaphragm, carbon-rod anode, platinum cathode, 4.5 F/mol, 0.1A, cathode potential -1.45 to -1.65V vs. SCE;

Shono, Tatsuya; Hamaguchi, Hiroshi; Mikami, Hiroshi; Nogusa, Hideo; Kashimura, Shigenori

Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2103 - 2105 Title/Abstract Full Text View citing articles Show Details

25

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26

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Rx-ID: 2125434 Find similar reactions

With hydroxylamine hydrochloride; sodium acetate in 1,4-dioxane; perchloric acid; dichloromethane

2 h; Ambient temperature;

Torii, Sigeru; Tanaka, Hideo; Katoh, Tetsuo

Chemistry Letters, 1983 , p. 607 - 610 Title/Abstract Full Text Show Details


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in nitrobenzene

T=150°C; 1 h; other temperature, other solvent (DMSO), KOH; Product distribution;

Rx-ID: 2102946 Find similar reactions

Trofimov, B. A.; Korostova, S. E.; Sobenina, L. N.; Mikhaleva, A. I.; Bzhezovskii, V. M.; et al.

Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 148 - 152 Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 2 p. 193 - 198 Title/Abstract Full Text View citing articles Show Details

27

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Rx-ID: 7247825 Find similar reactions

Phenylaceton , H2NOH;

Alvernhe; Laurent

Bulletin de la Societe Chimique de France, 1970 , p. 3003,3004,3007 Full Text Show Details

Phenylpropan-2-on, NH2OH, Pyridin, wss.NaOH (neben d. anti-Isomeren);

Huitric et al.

Journal of Organic Chemistry, 1967 , vol. 32, p. 1661 Full Text View citing articles Show Details

N-Hydroxyamphetamin, Autoxid.;

Lindeke et al.

Acta Pharmaceutica Suecica, 1975 , vol. 12, p. 183,192, 193 Full Text View citing articles Show Details

N-Hydroxyphentermin, Autoxid.;

Lindeke et al.

Acta Pharmaceutica Suecica, 1975 , vol. 12, p. 183,192, 193 Full Text View citing articles Show Details

28

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Rx-ID: 7362548 Find similar reactions

Phenylpropan-2-on, NH2OH, Pyridin, wss.NaOH (neben d. syn-Isomeren);

Huitric et al.

Journal of Organic Chemistry, 1967 , vol. 32, p. 1661 Full Text View citing articles Show Details

entspr. Keton, NH2OH;

Foreman; Siegel; Mrtek

Journal of pharmaceutical sciences, 1969 , vol. 58, # 2 p. 189 - 192 Title/Abstract Full Text View citing articles Show Details


N-Hydroxyamphetamin, Autoxid.;

Lindeke et al.

Acta Pharmaceutica Suecica, 1975 , vol. 12, p. 183,192, 193 Full Text View citing articles Show Details

N-Hydroxyphentermin, Autoxid.;

Lindeke et al.

Acta Pharmaceutica Suecica, 1975 , vol. 12, p. 183,192, 193 Full Text View citing articles Show Details

29

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Rx-ID: 5856922 Find similar reactions

Alvernhe; Laurent

Bulletin de la Societe Chimique de France, 1970 , p. 3003,3004,3007 Full Text Show Details

Phenylaceton , H2NOH;

N-Hydroxy-N-n-propylamphetamin Ie, W., gelbes Quecksilberoxyd;

Beckett; Coutts; Ogunbona

Journal of Pharmacy and Pharmacology, 1974 , vol. 26, # 5 p. 312 - 316 Title/Abstract Full Text View citing articles Show Details

N-Aethyl-N-hydroxyamphetamin Id, W., gelbes Quecksilberoxyd;

Beckett; Coutts; Ogunbona

Journal of Pharmacy and Pharmacology, 1974 , vol. 26, # 5 p. 312 - 316 Title/Abstract Full Text View citing articles Show Details

Beckett; Coutts; Ogunbona

Tetrahedron, 1973 , vol. 29, # 24 p. 4189 - 4193 Title/Abstract Full Text View citing articles Show Details

8a, Chloroperbenzoesaeure, LiAlH4 (u. Homologe);

A

B

C

D

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30

Synthesize Find similar Rx-ID: 1048770 Find similar reactions


With hydrogenchloride; nitrosylchloride

T=20°C; 9 h; Irradiation; Further byproducts given;

Julliard,M.

Bulletin de la Societe Chimique de France, 1970 , p. 2001 - 2004 Full Text View citing articles Show Details

31

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With hydrogen; palladium on activated charcoal in methanol

Rx-ID: 1125567 Find similar reactions

Biela,R. et al.

Journal fuer Praktische Chemie (Leipzig), 1966 , vol. 33, p. 282 - 292 Full Text View citing articles Show Details

32

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Multi-step reaction with 2 steps 1: NOCl, HCl / diethyl ether 2: H2 / Pd-C / methanol View Scheme

Rx-ID: 22423453 Find similar reactions

Biela,R. et al.

Journal fuer Praktische Chemie (Leipzig), 1966 , vol. 33, p. 282 - 292 Full Text View citing articles Show Details

33

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Rx-ID: 8255750 Find similar reactions

Smith

Journal of the American Chemical Society, 1948 , vol. 70, p. 320,322 Journal of the American Chemical Society, 1954 , vol. 76, p. 436,441 Full Text View citing articles Show Details


34

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Rx-ID: 5856923 Find similar reactions

With hydrogenchloride; iron

weiteres Reagens: FeCl3;

Purdue Research Found.

Patent: US2233823 , 1939 ;

With hydrogenchloride; iron

weiteres Reagens: FeCl3;

Purdue Research Found.

Patent: US2233823 , 1939 ;

Full Text Show Details

Full Text Show Details

35

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With hydrogenchloride; diethyl ether

Rx-ID: 668824 Find similar reactions

Dollfus

Chemische Berichte, 1892 , vol. 25, p. 1918 Chemische Berichte, 1893 , vol. 26, p. 1971 Full Text View citing articles Show Details

36

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With ethanol

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Rx-ID: 5856924 Find similar reactions

Dollfus

Chemische Berichte, 1892 , vol. 25, p. 1918 Chemische Berichte, 1893 , vol. 26, p. 1971


Full Text View citing articles Show Details

37

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Synthesize Find similar

Rx-ID: 22069718 Find similar reactions

Multi-step reaction with 2 steps 1: alcohol 2: absolute diethyl ether; HCl View Scheme

Dollfus

Chemische Berichte, 1892 , vol. 25, p. 1918 Chemische Berichte, 1893 , vol. 26, p. 1971 Full Text View citing articles Show Details

Multi-step reaction with 2 steps 1: sodium carbonate; aqueous alcohol; hydroxylamine hydrochloride 2: absolute diethyl ether; HCl View Scheme

Dollfus

Chemische Berichte, 1892 , vol. 25, p. 1918 Chemische Berichte, 1893 , vol. 26, p. 1971 Full Text View citing articles Show Details


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