Query Query
1. Query N
O
Results
Date
4 reactions in Reaxys
2018-02-14 06h:58m:30s (EST)
4 reactions in Reaxys
2018-02-14 07h:00m:33s (EST)
Search as: As drawn 2. Query
(1. Query) AND itemno in (1)
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N
O
N
Rx-ID: 44448384 View in Reaxys 1/4 Yield
Conditions & References
52 %
With tert.-butylnitrite, 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile, Time= 15h, T= 20 °C , Irradiation Rusch, Fabian; Schober, Jan-Christian; Brasholz, Malte; ChemCatChem; vol. 8; nb. 18; (2016); p. 2881 - 2884 View in Reaxys
NH O
N Cl
O
Rx-ID: 36754079 View in Reaxys 2/4 Yield
Conditions & References Reaction Steps: 2 1: aluminum oxide / neat (no solvent) / 0.13 h / 100 °C / Microwave irradiation; Green chemistry 2: sodium carbonate / neat (no solvent) / 0.07 h / 100 °C / Microwave irradiation With aluminum oxide, sodium carbonate in neat (no solvent) Lai, Qiu Yu; Liao, Rong Su; Wu, Shao Yong; Zhang, Jia Xin; Duan, Xin Hong; New Journal of Chemistry; vol. 37; nb. 12; (2013); p. 4069 - 4076 View in Reaxys
Br HN
O
O
N
Rx-ID: 36754097 View in Reaxys 3/4 Yield
Conditions & References With sodium carbonate in neat (no solvent), Time= 0.0666667h, T= 100 °C , Microwave irradiation Lai, Qiu Yu; Liao, Rong Su; Wu, Shao Yong; Zhang, Jia Xin; Duan, Xin Hong; New Journal of Chemistry; vol. 37; nb. 12; (2013); p. 4069 - 4076 View in Reaxys
O
S N
Br
O N
O
O
Rx-ID: 29656426 View in Reaxys 4/4 Yield 99 %
Conditions & References Stage 1: With pentan-1-ol, tetrabutylammomium bromide, caesium carbonate in toluene, Time= 24h, Reflux, In air Stage 2: in toluene, Time= 8h, Reflux, in air
Copyright © 2018 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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Denton, Justin R.; Synthesis; nb. 5; (2010); p. 775 - 782; Art.No: M05709SS View in Reaxys
Copyright © 2018 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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