Query Query H 2N
1. Query
HO H 2N
H
H
Results
Date
1 reactions in Reaxys
2018-03-28 09h:21m:28s (EST)
Search as: As drawn, No salts, No mixtures
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2018-03-28 09:23:08
H 2N
HO H 2N
H
H
Cl
H
Rx-ID: 15763373 View in Reaxys 1/1 Yield
Conditions & References Reaction Steps: 4 1.1: 95 percent / CHCl3 / 0 - 20 °C 2.1: 88 percent / iodine; triphenylphosphine polystyryl-supported; imidazole / CH2Cl2 / 2 h / Heating 3.1: 94 percent / N-Selectride / tetrahydrofuran / 1.5 h / 5 °C 4.1: trifluoroacetic acid / CH2Cl2 / 18 h / 20 °C 4.2: 91 percent / HCl / diethyl ether; CHCl3 With 1H-imidazole, triphenylphosphine polystyryl-supported, iodine, sodium tri-sec-butylborohydride, trifluoroacetic acid in tetrahydrofuran, dichloromethane, chloroform, 1.1: Substitution / 2.1: Substitution / 3.1: Reduction / 4.1: Hydrolysis / 4.2: Addition Quagliato, Dominick A.; Andrae, Patrick M.; Matelan, Edward M.; Journal of Organic Chemistry; vol. 65; nb. 16; (2000); p. 5037 - 5042 View in Reaxys
Copyright © 2018 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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2018-03-28 09:23:08