1-Phenyl-2-propanol (P2Pol) [C9H12O] by Asch

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2018-05-22 18h:14m:25s (UTC)

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Search as: As drawn ) AND (IDE.XRN=1858667))

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Reaxys ID 1858667 View in Reaxys

1/1 CAS Registry Number: 698-87-3 Chemical Name: 3-phenyl-2-propanol; 1-Phenyl-2-propanol Linear Structure Formula: C6H5CH2CHOHCH3 Molecular Formula: C9H12O Molecular Weight: 136.194 Type of Substance: isocyclic InChI Key: WYTRYIUQUDTGSX-UHFFFAOYSA-N Note:

Substance Label (108) Label References 3

Ghanem, Ashraf; Schurig, Volker; Monatshefte fur Chemie; vol. 134; nb. 8; (2003); p. 1151 - 1157, View in Reaxys; Ley, Steven V.; Mitchell, Claire; Pears, David; Ramarao, Chandrashekar; Yu, Jin-Quan; Zhou, Wuzong; Organic Letters; vol. 5; nb. 24; (2003); p. 4665 - 4668, View in Reaxys; de Leeuw, Nicolas; Torrelo, Guzman; Bisterfeld, Carolin; Resch, Verena; Mestrom, Luuk; Straulino, Emanuele; van der Weel, Laura; Hanefeld, Ulf; Advanced Synthesis and Catalysis; vol. 360; nb. 2; (2018); p. 242 - 249, View in Reaxys

Patent; KAO CORPORATION; KINOSHITA, Kazuki; SHIRAI, Tomohiro; KUMIHASHI, Kentaro; FUJIHARA, Hirohisa; MUGITA, Nanae; WO2013/103155; (2013); (A1) English, View in Reaxys; Patent; Kao Corporation; Kinoshita, Kazuki; Shirai, Tomohiro; Kumihashi, Kentaro; Fujihara, Hirohisa; Mugita, Nanae; (17 pag.); US9856196; (2018); (B2) English, View in Reaxys

(±)-43

Neyyappadath, Rifahath Mon; Chisholm, Ross; Greenhalgh, Mark D.; Rodríguez-Escrich, Carles; Pericàs, Miquel A.; Hähner, Georg; Smith, Andrew D.; ACS Catalysis; vol. 8; nb. 2; (2018); p. 1067 - 1075, View in Reaxys

(rac)-2f

Musa, Musa M.; Bsharat, Odey; Karume, Ibrahim; Vieille, Claire; Takahashi, Masateru; Hamdan, Samir M.; European Journal of Organic Chemistry; vol. 2018; nb. 6; (2018); p. 798 - 805, View in Reaxys

rac-1b

Popłoński, Jarosław; Reiter, Tamara; Kroutil, Wolfgang; ChemCatChem; vol. 10; nb. 4; (2018); p. 763 - 768, View in Reaxys

Baumstark, Alfons L.; Kovac, Franci; Vasquez, Pedro C.; Canadian Journal of Chemistry; vol. 77; nb. 3; (1999); p. 308 - 312, View in Reaxys; Pedroli, Chiara; Ravelli, Davide; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio; Journal of Organic Chemistry; vol. 82; nb. 13; (2017); p. 6592 - 6603, View in Reaxys

Leblanc, Yves; Dufresne, Claude; Carson, Rebekah; Morency, Louis; Welch, Christopher J; Tetrahedron Asymmetry; vol. 12; nb. 22; (2001); p. 3063 - 3066, View in Reaxys; Dornan, Laura M.; Clendenning, Grainne M. A.; Pitak, Mateusz B.; Coles, Simon J.; Muldoon, Mark J.; Catalysis Science and Technology; vol. 4; nb. 8; (2014); p. 2526 2534, View in Reaxys; Wang, Min; Lu, Jianmin; Li, Lihua; Li, Hongji; Liu, Huifang; Wang, Feng; Journal of Catalysis; vol. 348; (2017); p. 160 - 167, View in Reaxys; Kim, Young-Hyun; Park, Seongsoon; Bulletin of the Korean Chemical Society; vol. 38; nb. 11; (2017); p. 1358 - 1361, View in Reaxys

Kim, Mahn-Joo; Chung, Yong Il; Choi, Yoon Kyung; Lee, Han Ki; Kim, Daeho; Park, Jaiwook; Journal of the American Chemical Society; vol. 125; nb. 38; (2003); p. 11494 - 11495, View in Reaxys; Park, Jung-Woo; Jun, ChulHo; Organic Letters; vol. 9; nb. 20; (2007); p. 4073 - 4076, View in Reaxys; Karume, Ibrahim; Takahashi, Masateru; Hamdan, Samir M.; Musa, Musa M.; ChemCatChem; vol. 8; nb. 8; (2016); p. 1459 - 1463, View in Reaxys; Liardo, Elisa; Ríos-Lombardía, Nicolás; Morís, Francisco; Rebolledo, Francisca; González-Sabín, Javier; ACS Catalysis; vol. 7; nb. 7; (2017); p. 4768 - 4774, View in Reaxys

Castelbou, Jessica Llop; Bres-Femenia, Emma; Blondeau, Pascal; Chaudret, Bruno; Castilln, Sergio; Claver, Carmen; Godard, Cyril; ChemCatChem; vol. 6; nb. 11; (2014); p. 3160 - 3168, View in Reaxys; Thorsheim, Karin; Manner, Sophie; Ellervik, Ulf; Tetrahedron; vol. 73; nb. 44; (2017); p. 6329 - 6333, View in Reaxys

15g

Khusainova, Liliya I.; Khafizova, Leila O.; Tyumkina, Tatyana V.; Ryazanov, Kirill S.; Dzhemilev, Usein M.; Journal of Organometallic Chemistry; vol. 832; (2017); p. 12 - 17, View in Reaxys

(rac)-2a

Vitale, Paola; Abbinante, Vincenzo Mirco; Perna, Filippo Maria; Salomone, Antonio; Cardellicchio, Cosimo; Capriati, Vito; Advanced Synthesis and Catalysis; vol. 359; nb. 6; (2017); p. 1049 - 1057, View in Reaxys

Hoang, Hai Nam; Nagashima, Yoshihiro; Mori, Shuichi; Kagechika, Hiroyuki; Matsuda, Tomoko; Tetrahedron; vol. 73; nb. 20; (2017); p. 2984 - 2989, View in Reaxys

15b

Martinez-Espinar, Francisco; Blondeau, Pascal; Nolis, Pau; Chaudret, Bruno; Claver, Carmen; Castillón, Sergio; Godard, Cyril; Journal of Catalysis; vol. 354; (2017); p. 113 - 127, View in Reaxys

(RS)-1P2P

Zhang, Shi-Yuan; Yang, Cheng-Xiong; Shi, Wei; Yan, Xiu-Ping; Cheng, Peng; Wojtas, Lukasz; Zaworotko, Michael J.; Chem; vol. 3; nb. 2; (2017); p. 281 - 289, View in Reaxys

Rac-1a

Knaus, Tanja; Cariati, Luca; Masman, Marcelo F; Mutti, Francesco G.; Organic and Biomolecular Chemistry; vol. 15; nb. 39; (2017); p. 8313 - 8325, View in Reaxys

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2ba

Hu, Xia; Zhang, Guoting; Bu, Faxiang; Lei, Aiwen; ACS Catalysis; vol. 7; nb. 2; (2017); p. 1432 - 1437, View in Reaxys

c2p

Luecke, Marcel-Philip; Porwal, Digvijay; Kostenko, Arseni; Zhou, Yu-Peng; Yao, Shenglai; Keck, Matthias; Limberg, Christian; Oestreich, Martin; Driess, Matthias; Dalton Transactions; vol. 46; nb. 47; (2017); p. 16412 - 16418, View in Reaxys

(rac)-1a

Musa, Musa M.; Patel, Jay M.; Nealon, Christopher M.; Kim, Chang Sup; Phillips, Robert S.; Karume, Ibrahim; Journal of Molecular Catalysis B: Enzymatic; vol. 115; (2015); p. 155 - 159, View in Reaxys; Karume, Ibrahim; Musa, Musa M.; Bsharat, Odey; Takahashi, Masateru; Hamdan, Samir M.; El Ali, Bassam; RSC Advances; vol. 6; nb. 99; (2016); p. 96616 - 96622, View in Reaxys

Min, Byul-Hana; Kim, Dong-Su; Park, Hyo-Soon; Jun, Chul-Ho; Chemistry - A European Journal; vol. 22; nb. 18; (2016); p. 6234 - 6238, View in Reaxys

11g

Gülcemal, Süleyman; Gülcemal, Derya; Whitehead, George F. S.; Xiao, Jianliang; Chemistry - A European Journal; vol. 22; nb. 30; (2016); p. 10513 - 10522, View in Reaxys

Park, Seongsoon; Bulletin of the Korean Chemical Society; vol. 37; nb. 10; (2016); p. 1720 - 1723, View in Reaxys

Kolakowski, Robert V.; Haelsig, Karl T.; Emmerton, Kim K.; Leiske, Chris I.; Miyamoto, Jamie B.; Cochran, Julia H.; Lyon, Robert P.; Senter, Peter D.; Jeffrey, Scott C.; Angewandte Chemie - International Edition; vol. 55; nb. 28; (2016); p. 7948 - 7951; Angew. Chem.; vol. 128; nb. 28; (2016); p. 8080 - 8083,4, View in Reaxys

Kim, Seok-In; Chu, Feixia; Dueno, Eric E.; Jung, Kyung Woon; Journal of Organic Chemistry; vol. 64; nb. 13; (1999); p. 4578 - 4579, View in Reaxys; Kazemi; Kiasat; Synthetic Communications; vol. 32; nb. 14; (2002); p. 2255 2260, View in Reaxys; Li, Yanjun; Izumi, Taeko; Journal of the Chinese Chemical Society (Taipei, Taiwan); vol. 49; nb. 4; (2002); p. 505 - 508, View in Reaxys; Suenaga, Toshiro; Schutz, Caroline; Nakata, Tadashi; Tetrahedron Letters; vol. 44; nb. 31; (2003); p. 5799 - 5801, View in Reaxys; Kitamoto, Yuichi; Kuruma, Yosuke; Suzuki, Kazumi; Hattori, Tetsutaro; Journal of Organic Chemistry; vol. 80; nb. 1; (2015); p. 521 - 527, View in Reaxys

Strunz, Ann Kathrin; Zweemer, Annelien J.M.; Weiss, Christina; Schepmann, Dirk; Junker, Anna; Heitman, Laura H.; Koch, Michael; Wünsch, Bernhard; Bioorganic and Medicinal Chemistry; vol. 23; nb. 14; (2015); p. 4034 4049, View in Reaxys

Xiong, Biao; Li, Ya; Lv, Wan; Tan, Zhenda; Jiang, Huanfeng; Zhang, Min; Organic Letters; vol. 17; nb. 16; (2015); p. 4054 - 4057, View in Reaxys

Khusainova; Khafizova; Tyumkina; Dzhemilev; Russian Journal of Organic Chemistry; vol. 51; nb. 11; (2015); p. 1517 - 1523; Zh. Org. Khim.; vol. 51; nb. 11; (2015); p. 1551 - 1557,7, View in Reaxys

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys; Martinez, Regina; Pastor, Isidro M.; Yus, Miguel; Arkivoc; vol. 2014; nb. 2; (2014); p. 71 - 84, View in Reaxys

Ema, Tadashi; Okada, Ryoichi; Fukumoto, Minoru; Jittani, Masahito; Ishida, Mikiko; Furuie, Kenji; Yamaguchi, Kunihiro; Sakai, Takashi; Utaka, Masanori; Tetrahedron Letters; vol. 40; nb. 23; (1999); p. 4367 - 4370, View in Reaxys; Ema, Tadashi; Yamaguchi, Kunihiro; Wakasa, Yuji; Tanaka, Nobuaki; Utaka, Masanori; Sakai, Takashi; Chemistry Letters; nb. 7; (2000); p. 782 - 783, View in Reaxys; Morrill, Terence C.; D'Souza, Christopher A.; Yang, Lu; Sampognaro, Anthony J.; Journal of Organic Chemistry; vol. 67; nb. 8; (2002); p. 2481 - 2484, View in Reaxys; Su, Erzheng; Xu, Jingjing; You, Pengyong; Journal of Molecular Catalysis B: Enzymatic; vol. 106; (2014); p. 11 - 16, View in Reaxys

2aa

Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); p. 48 - 51, View in Reaxys

Simonneau, Antoine; Friebel, Jonas; Oestreich, Martin; European Journal of Organic Chemistry; vol. 2014; nb. 10; (2014); p. 2077 - 2083, View in Reaxys

Apsunde, Tushar D.; Trudell, Mark L.; Synthesis (Germany); vol. 46; nb. 2; (2014); p. 230 - 234; Art.No: SS-2013M0636-OP, View in Reaxys

Dueno; Chu; Kim; Kyung Woon Jung; Tetrahedron Letters; vol. 40; nb. 10; (1999); p. 1843 - 1846, View in Reaxys; Hamada, Shohei; Furuta, Takumi; Wada, Yoshiyuki; Kawabata, Takeo; Angewandte Chemie - International Edition; vol. 52; nb. 31; (2013); p. 8093 - 8097; Angew. Chem.; vol. 125; nb. 31; (2013); p. 8251 - 8255,5, View in Reaxys

rac-21

Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys; Nakamura, Yukie; Egami, Hiromichi; Matsumoto, Kazuhiro; Uchida, Tatsuya; Katsuki, Tsutomu; Tetrahedron; vol. 63; nb. 28; (2007); p. 6383 - 6387, View in Reaxys; Hellmann, Gunther; Hack, Achim; Thiemermann, Eric; Luche, Olaf; Raabe, Gerhard; Gais, Hans-Joachim; Chemistry - A European Journal; vol. 19; nb. 12; (2013); p. 3869 - 3897, View in Reaxys

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Xia, Ji-Bao; Zhu, Chen; Chen, Chuo; Journal of the American Chemical Society; vol. 135; nb. 46; (2013); p. 17494 17500, View in Reaxys

Patent; GILEAD SCIENCES, INC.; BABAOGLU, Kerim; BJORNSON, Kyla; GUO, Hongyan; HALCOMB, Randall, L.; LINK, John, O.; MCFADDEN, Ryan; MITCHELL, Michael, L.; ROETHLE, Paul; TRENKLE, James, D.; VIVIAN, Randall, W.; XU, Lianhong; WO2012/3497; (2012); (A1) English, View in Reaxys

Patent; Dong, Guangbin; Grubbs, Robert H.; Teo, Peili; Wickens, Zach K.; US2012/172634; (2012); (A1) English, View in Reaxys

Maligres, Peter E.; Li, Jing; Krska, Shane W.; Schreier, John D.; Raheem, Izzat T.; Angewandte Chemie - International Edition; vol. 51; nb. 36; (2012); p. 9071 - 9074, View in Reaxys

Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.; Journal of Molecular Catalysis B: Enzymatic; vol. 83; (2012); p. 23 - 28, View in Reaxys

Wu, La-Xia; Wang, Huan; Xiao, Yan; Tu, Zhuo-Ying; Ding, Bin-Bin; Lu, Jia-Xing; Electrochemistry Communications; vol. 25; nb. 1; (2012); p. 116 - 118, View in Reaxys

Van Der Linden, Jacobus J. M.; Hilberink, Peter W.; Kronenburg, Claudia M. P.; Kemperman, Gerardus J.; Organic Process Research and Development; vol. 12; nb. 5; (2008); p. 911 - 920, View in Reaxys; Fujii, Hideaki; Yamada, Takaaki; Hayashida, Kohei; Kuwada, Miki; Hamasaki, Atom; Nobuhara, Kazunori; Ozeki, Sumio; Nagase, Hiroshi; Heterocycles; vol. 85; nb. 11; (2012); p. 2685 - 2691, View in Reaxys

(±)-11

Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu; Letters in Organic Chemistry; vol. 9; nb. 9; (2012); p. 615 - 621, View in Reaxys

PhCH2CH(OH)CH3

Lakouraj, Moslem M.; Tajbakhsh, Mahmood; Mahalli, Majid S.; Monatshefte fur Chemie; vol. 139; nb. 2; (2008); p. 117 - 123, View in Reaxys

2-ol (Table 1)

Whitehouse, Christopher J. C.; Bell, Stephen G.; Tufton, Henry G.; Kenny, Richard J. P.; Ogilvie, Lydia C. I.; Wong, Luet-Lok; Chemical Communications; nb. 8; (2008); p. 966 - 968, View in Reaxys

rac-3a

Csajagi, Csaba; Szatzker, Gabor; Rita Toke, Eniko; Uerge, Laszlo; Darvas, Ferenc; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 19; nb. 2; (2008); p. 237 - 246, View in Reaxys

A18

Cesarini, Sara; Spallarossa, Andrea; Ranise, Angelo; Bruno, Olga; La Colla, Paolo; Secci, Barbara; Collu, Gabriella; Loddo, Roberta; Bioorganic and Medicinal Chemistry; vol. 16; nb. 7; (2008); p. 4173 - 4185, View in Reaxys

Demizu, Yosuke; Shiigi, Hirofumi; Oda, Takahisa; Matsumura, Yoshihiro; Onomura, Osamu; Tetrahedron Letters; vol. 49; nb. 1; (2008); p. 48 - 52, View in Reaxys

(+/-)-17a

Machado, Luciana L.; Lemos, Telma L.G.; de Mattos, Marcos Carlos; de Oliveira, Maria da Conceicao F.; de Gonzalo, Gonzalo; Gotor-Fernandez, Vicente; Gotor, Vicente; Tetrahedron Asymmetry; vol. 19; nb. 12; (2008); p. 1418 - 1423, View in Reaxys

(+/-)-8a

Kerti, Gabor; Kurtan, Tibor; Illyes, Tuende-Zita; Koever, Katalin E.; Solyom, Sandor; Pescitelli, Gennaro; Fujioka, Naoko; Berova, Nina; Antus, Sandor; European Journal of Organic Chemistry; nb. 2; (2007); p. 296 - 305, View in Reaxys

substrate, tab 2/8

Sun, Wei; Wu, Xiaomei; Xia, Chungu; Helvetica Chimica Acta; vol. 90; nb. 3; (2007); p. 623 - 626, View in Reaxys

rac-2b

Erdelyi, Balazs; Szabo, Antal; Seres, Gabor; Birincsik, Laszlo; Ivanics, Jozsef; Szatzker, Gabor; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 17; nb. 2; (2006); p. 268 - 274, View in Reaxys

entry 23 (Tab.1, R2-OH)

Shirini, Farhad; Zolfigol; Safari; Journal of Chemical Research; nb. 3; (2006); p. 154 - 156, View in Reaxys

rac-1

Kiss, Violetta; Egri, Gabriella; Balint, Jozsef; Ling, Istvan; Barkoczi, Jozsef; Fogassy, Elemer; Tetrahedron Asymmetry; vol. 17; nb. 15; (2006); p. 2220 - 2234, View in Reaxys

15a

Masutani, Kouta; Minowa, Tomofumi; Hagiwara, Yoshiaki; Mukaiyama, Teruaki; Bulletin of the Chemical Society of Japan; vol. 79; nb. 7; (2006); p. 1106 - 1117, View in Reaxys

subs., Tab. 1, entry 7

Park, Jung-Woo; Chang, Hoon-Jo; Jun, Chul-Ho; Synlett; nb. 5; (2006); p. 771 - 775, View in Reaxys

C6H5CH2CH(CH3 Khosropour, Ahmad R.; Khodaei, Mohammad M.; Ghaderi, Sattar; Zeitschrift fur Naturforschung - Section B Jour)OH nal of Chemical Sciences; vol. 61; nb. 3; (2006); p. 326 - 330, View in Reaxys 6h

Boren, Linnea; Martin-Matute, Belen; Xu, Yongmei; Cordova, Armando; Baeckvall, Jan-E.; Chemistry - A European Journal; vol. 12; nb. 1; (2006); p. 225 - 232, View in Reaxys

Mamedov; Russian Journal of Applied Chemistry; vol. 79; nb. 3; (2006); p. 408 - 410, View in Reaxys

PhCH2CH(OH)CH 3

Shirini; Zolfigol; Mallakpour; Russian Journal of Organic Chemistry; vol. 41; nb. 4; (2005); p. 625 - 626, View in Reaxys; Shirini, Farhad; Zolfigol, Mohammad Ali; Paktinat, Maryam; Synthesis; nb. 24; (2006); p. 4252 4256, View in Reaxys

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Li, Yanjun; Izumi, Taeko; Journal of Chemical Research - Part S; nb. 3; (2003); p. 128 - 129, View in Reaxys; Clay, Julia M.; Vedejs, Edwin; Journal of the American Chemical Society; vol. 127; nb. 16; (2005); p. 5766 - 5767, View in Reaxys

tab1, col1, entry6

Hunsen, Mo; Tetrahedron Letters; vol. 46; nb. 10; (2005); p. 1651 - 1653, View in Reaxys

Tab. 1, entry 11

Mu, Ruizhu; Liu, Zhongquan; Yang, Zhanjun; Liu, Zhengang; Wu, Longmin; Liu, Zhong-Li; Advanced Synthesis and Catalysis; vol. 347; nb. 10; (2005); p. 1333 - 1336, View in Reaxys

PhCH2CH(CH3)O H

Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.; Organic and Biomolecular Chemistry; vol. 3; nb. 6; (2005); p. 1049 - 1057, View in Reaxys

T.2/1 ROH

Masutani, Kouta; Minowa, Tomofumi; Mukaiyama, Teruaki; Chemistry Letters; vol. 34; nb. 8; (2005); p. 1124 1125, View in Reaxys

Tab. 1, entry 18

Mohanazadeh, Farajollah; Hosini, Mostafa; Tajbakhsh, Mahmoud; Monatshefte fur Chemie; vol. 136; nb. 12; (2005); p. 2041 - 2043, View in Reaxys

Hamamoto, Hiromi; Suzuki, Yachiyo; Yamada, Yoichi M. A.; Tabata, Hidetsugu; Takahashi, Hideyo; Ikegami, Shiro; Angewandte Chemie - International Edition; vol. 44; nb. 29; (2005); p. 4536 - 4538, View in Reaxys

Hatzakis, Nikos S.; Smonou, Ioulia; Bioorganic Chemistry; vol. 33; nb. 4; (2005); p. 325 - 337, View in Reaxys

Tab. 1, entry 1, subst.

Hunsen, Mo; Journal of Fluorine Chemistry; vol. 126; nb. 9-10; (2005); p. 1356 - 1360, View in Reaxys

Allan; Carnell; Journal of Organic Chemistry; vol. 66; nb. 19; (2001); p. 6495 - 6497, View in Reaxys; ChoukchouBraham; Mostefa-Kara; Cheikh; Didi; Villemin; Synthetic Communications; vol. 35; nb. 2; (2005); p. 169 - 178, View in Reaxys

C6H5CH2CH(OH )CH3

Shirini, Farhad; Zolfigol, Mohammad A.; Abedini, Masoumeh; Monatshefte fur Chemie; vol. 135; nb. 3; (2004); p. 279 - 282, View in Reaxys

Yasuda, Makoto; Yamasaki, Satoshi; Onishi, Yoshiyuki; Baba, Akio; Journal of the American Chemical Society; vol. 126; nb. 23; (2004); p. 7186 - 7187, View in Reaxys

5 (Tab. 2)

Yamasaki, Yuki; Hirayama, Takaharu; Oshima, Koichiro; Matsubara, Seijiro; Chemistry Letters; vol. 33; nb. 7; (2004); p. 864 - 865, View in Reaxys

BnCH(OH)Me

Zhang, Mianji; Vedantham, Punitha; Flynn, Daniel L.; Hanson, Paul R.; Journal of Organic Chemistry; vol. 69; nb. 24; (2004); p. 8340 - 8344, View in Reaxys

text on p. 8581

Ranu, Brindaban C.; Banerjee, Subhash; Das, Arijit; Tetrahedron Letters; vol. 45; nb. 46; (2004); p. 8579 - 8581, View in Reaxys

PhCH2CHMeOH

Ochiai, Masahito; Sueda, Takuya; Tetrahedron Letters; vol. 45; nb. 18; (2004); p. 3557 - 3559, View in Reaxys

(rac)-12

Csjernyik, Gabor; Bogar, Krisztian; Baeckvall, Jan-E.; Tetrahedron Letters; vol. 45; nb. 36; (2004); p. 6799 - 6802, View in Reaxys

Table 2, entries 10, 11

Sun, Wei; Wang, Hongwang; Xia, Chungu; Li, Jingwei; Zhao, Peiqing; Angewandte Chemie - International Edition; vol. 42; nb. 9; (2003); p. 1042 - 1044, View in Reaxys

prod 1b

Kim, Ji Duck; Han, Gyoonhee; Zee, Ok Pyo; Jung, Young Hoon; Tetrahedron Letters; vol. 44; nb. 4; (2003); p. 733 735, View in Reaxys

T., substr. run 10

Xu, Liang; Trudell, Mark L.; Tetrahedron Letters; vol. 44; nb. 12; (2003); p. 2553 - 2555, View in Reaxys

Romanelli; Vazquez; Pizzio; Caceres; Blanco; Autino; Synthetic Communications; vol. 33; nb. 8; (2003); p. 1359 1365, View in Reaxys

Tab. 1, substrate, run8

Shirini, Farhad; Zolfigol, Mohammad A.; Abedini, Masoumeh; Salehi, Peyman; Mendeleev Communications; vol. 13; nb. 6; (2003); p. 265 - 267, View in Reaxys

Ghanem, Ashraf; Schurig, Volker; Tetrahedron Asymmetry; vol. 14; nb. 17; (2003); p. 2547 - 2555, View in Reaxys

39b

Stampfer, Wolfgang; Kosjek, Birgit; Faber, Kurt; Kroutil, Wolfgang; Journal of Organic Chemistry; vol. 68; nb. 2; (2003); p. 402 - 406, View in Reaxys

Salvatore, Ralph N; Chu, Feixia; Nagle, Advait S; Kapxhiu, Elona A; Cross, Richard M; Jung, Kyung Woon; Tetrahedron; vol. 58; nb. 17; (2002); p. 3329 - 3347, View in Reaxys

50a

Matsuo, Jun-Ichi; Iida, Daisuke; Tatani, Kazuya; Mukaiyama, Teruaki; Bulletin of the Chemical Society of Japan; vol. 75; nb. 2; (2002); p. 223 - 234, View in Reaxys

rac-17b

Pogorevc, Mateja; Faber, Kurt; Tetrahedron Asymmetry; vol. 13; nb. 13; (2002); p. 1435 - 1441, View in Reaxys

product from d

Dahlen, Anders; Hilmersson, Goeran; Tetrahedron Letters; vol. 43; nb. 40; (2002); p. 7197 - 7200, View in Reaxys

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tab, run9 substrate

Mamaghani; Shirini; Parsa; Russian Journal of Organic Chemistry; vol. 38; nb. 8; (2002); p. 1113 - 1115, View in Reaxys

Matsugi, Masato; Itoh, Kinuyo; Nojima, Masatomo; Hagimoto, Yuri; Kita, Yasuyuki; Chemistry - A European Journal; vol. 8; nb. 24; (2002); p. 5551 - 5564, View in Reaxys

Alcohol T2 entry 9

Matsuo, Jun-Ichi; Kitagawa, Hideo; Iida, Daisuke; Mukaiyama, Teruaki; Chemistry Letters; nb. 2; (2001); p. 150 151, View in Reaxys

6-d0

Angelis, Yiannis S.; Hatzakis, Nikos S.; Smonou, Ioulia; Orfanopoulos, Michael; Tetrahedron Letters; vol. 42; nb. 22; (2001); p. 3753 - 3756, View in Reaxys

21a

Weik, Steffen; Nicholson, Graeme; Jung, Gnther; Rademann, Jrg; Angewandte Chemie - International Edition; vol. 40; nb. 8; (2001); p. 1436 - 1439, View in Reaxys

table 4, entry 3

Oriyama; Watahiki; Kobayashi; Hirano; Suzuki; Synthetic Communications; vol. 31; nb. 15; (2001); p. 2305 - 2311, View in Reaxys

(+/-)-1h

Matsugi, Masato; Itoh, Kinuyo; Nojima, Masatomo; Hagimoto, Yuri; Kita, Yasuyuki; Tetrahedron Letters; vol. 42; nb. 45; (2001); p. 8019 - 8022, View in Reaxys

Nakamura, Kaoru; Fujii, Mikio; Ida, Yoshiteru; Tetrahedron Asymmetry; vol. 12; nb. 22; (2001); p. 3147 - 3153, View in Reaxys

Talukdar; Fang; Journal of Organic Chemistry; vol. 66; nb. 1; (2001); p. 330 - 333, View in Reaxys

Nishiyama, Tomihiro; Kameyama, Hideaki; Maekawa, Hideki; Watanuki, Kouhei; Canadian Journal of Chemistry; vol. 77; nb. 2; (1999); p. 258 - 262, View in Reaxys; Yasuda; Onishi; Ueba; Miyai; Baba; Journal of Organic Chemistry; vol. 66; nb. 23; (2001); p. 7741 - 7744, View in Reaxys

19b

Schneider, Christoph; Brauner, Joerg; European Journal of Organic Chemistry; nb. 23; (2001); p. 4445 - 4450, View in Reaxys

alcohol T2, entry I

Subramanyam; Tetrahedron Letters; vol. 41; nb. 34; (2000); p. 6537 - 6540, View in Reaxys

Tab.1, entry 7,βisom.

McCarthy, Mary; Hooper, Mark W.; Guiry, Patrick J.; Chemical Communications; nb. 14; (2000); p. 1333 - 1334, View in Reaxys

Jung, Hyun M.; Koh, Jeong H.; Kim, Mahn-Joo; Park, Jaiwook; Organic Letters; vol. 2; nb. 3; (2000); p. 409 - 411, View in Reaxys

Sakumo, Kunihiro; Kuki, Noriko; Kuno, Terumi; Takagi, Toshiyuki; Koyama, Mayumi; Ando, Akira; Kumadaki, Itsumaro; Journal of Fluorine Chemistry; vol. 93; nb. 2; (1999); p. 165 - 170, View in Reaxys; Falck; Lai, Jing-Yu; Venkata Ramana; Lee, Sang-Gyeong; Tetrahedron Letters; vol. 40; nb. 14; (1999); p. 2715 - 2718, View in Reaxys

(+/-)-1j

Sano, Tomohumi; Imai, Keisuke; Ohashi, Kousaburo; Oriyama, Takeshi; Chemistry Letters; nb. 3; (1999); p. 265 266, View in Reaxys

Roever, Stephan; Wipf, Peter; Tetrahedron Letters; vol. 40; nb. 31; (1999); p. 5667 - 5670, View in Reaxys

7. ROH, Scheme 1

Wipf, Peter; Reeves, Jonathan T.; Tetrahedron Letters; vol. 40; nb. 28; (1999); p. 5139 - 5142, View in Reaxys

Tab.3, entry 4

Koh, Jeong Hwan; Jung, Hyun Min; Kim, Mahn-Joo; Park, Jaiwook; Tetrahedron Letters; vol. 40; nb. 34; (1999); p. 6281 - 6284, View in Reaxys

Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Misawa, Ibuki; Journal of the Chemical Society - Perkin Transactions 1; nb. 16; (1999); p. 2397 - 2402, View in Reaxys

Table 1, Entry 14

Mohammadpoor-Baltork, Iraj; Hajipour, Abdol Reza; Mohammadi, Hasan; Bulletin of the Chemical Society of Japan; vol. 71; nb. 7; (1998); p. 1649 - 1653, View in Reaxys

Patent-Specific Data (5) Location in Patent References Page/Page column

Patent; Nimbus Apollo, Inc.; Harriman, Geraldine C.; Masse, Craig E.; Harwood, James; Bhat, Sathesh; Greenwood, Jeremy Robert; US2013/123231; (2013); (A1) English, View in Reaxys Patent; Dong, Guangbin; Grubbs, Robert H.; Teo, Peili; Wickens, Zach K.; US2012/172634; (2012); (A1) English, View in Reaxys Patent; Pfizer Inc; US2009/170886; (2009); (A1) English, View in Reaxys Patent; Goedecke GmbH; US6740768; (2004); (B1) English, View in Reaxys

Claim

Patent; Lever Brothers Company; US3944568; (1976); (A) English, View in Reaxys; Patent; Bush Boake Allen Limited; US3947574; (1976); (A) English, View in Reaxys; Patent; Omya AG; US6569229; (2003); (B1) English, View in Reaxys; Patent; Repsol Quimica, S.A.; US6429323; (2002); (B1) English, View in Reaxys

Druglikeness (1)

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1 of 1

LogP

1.829

H Bond Donors

H Bond Acceptors

Rotatable Bonds

TPSA

20.23

Lipinski Number

Veber Number

Related Structure (3) Related Structure References Meyers,A.I.; Kendall,P.M.; Tetrahedron Letters; nb. 14; (1974); p. 1337 - 1340, View in Reaxys; Marshall; Prager; Australian Journal of Chemistry; vol. 30; (1977); p. 141,144. 150, View in Reaxys; Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys The author investi- Hirota, Minoru; Sekiya, Toshiyuki; Abe, Kazuhisa; Tashiro, Hiroshi; Karatsu, Makoto; et al.; Tetrahedron; vol. gated the configura- 39; nb. 19; (1983); p. 3091 - 3100, View in Reaxys tion Configuration.

Levene; Walti; Journal of Biological Chemistry; vol. 90; (1931); p. 81,86, View in Reaxys

Derivative (7) Comment (Derivative)

References

p-Toluolsulfonat: F: DePuy,C.H. et al.; Journal of Organic Chemistry; vol. 35; (1970); p. 2746 - 2750, View in Reaxys 93.5-95grad; Eliminierung von Tosylat: k(E2), ΔH(excit.), ΔS(excit.) p-Nitrobenzoat: F.: 60-60.5grad

Suga et al.; Kogyo Kagaku Zasshi; vol. 70; (1967); p. 487,489, View in Reaxys

3,5-dinitro-benzoyl derivative (mp: 87.7-88.1 degree )

Bost et al.; Journal of Organic Chemistry; vol. 22; (1957); p. 51,54, View in Reaxys

4-nitro-benzoyl de- Truffault; Bulletin de la Societe Chimique de France; vol. <5> 6; (1939); p. 726,733, View in Reaxys rivative (mp: 61 degree ) naphthyl-(1)-carba- Golumbic; Cottle; Journal of the American Chemical Society; vol. 61; (1939); p. 996,999, View in Reaxys moyl derivative (mp: 91-92 degree ) phenyl urethane (mp: 90 degree )

Emde; Runne; Archiv der Pharmazie (Weinheim, Germany); vol. 249; (1911); p. 379, View in Reaxys

phenyl urethane (mp: 92 degree )

Tiffeneau; Fourneau; Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences; vol. 146; (1908); p. 699, View in Reaxys

Boiling Point (42) Boiling Point [°C]

Pressure (Boiling Point) [Torr]

Comment (Boiling Point)

References

71 - 72

Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys

92 - 93

Mamedov; Russian Journal of Applied Chemistry; vol. 79; nb. 3; (2006); p. 408 - 410, View in Reaxys

125

Thakar; Rao; Journal of Scientific and Industrial Research, Section B: Physical Sciences; vol. 21; (1962); p. 583,586, View in Reaxys; Li, Yanjun; Izumi, Taeko; Journal of the Chinese Chemical Society (Taipei, Taiwan); vol. 49; nb. 4; (2002); p. 505 - 508, View in Reaxys; Li, Yanjun; Izumi, Taeko; Journal of Chemical Research - Part S; nb. 3; (2003); p. 128 - 129, View in Reaxys

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103 - 104

9.8

Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Protiva, Miroslav; Collection of Czechoslovak Chemical Communications; vol. 52; nb. 12; (1987); p. 3013 - 3023, View in Reaxys

95 - 98

Chiba; Okimoto; Nagai; Takata; Bulletin of the Chemical Society of Japan; vol. 56; nb. 3; (1983); p. 719 - 723, View in Reaxys

51 - 60

Rao et al.; Journal of Organometallic Chemistry; vol. 166; (1979); p. 9,10, 12, 15, View in Reaxys

96 - 97

Schadt,F.L. et al.; Journal of the American Chemical Society; vol. 100; (1978); p. 228 - 246, View in Reaxys

60 - 61

Mason; Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999); (1975); p. 1664, View in Reaxys

121

Kursanov et al.; Synthesis; (1974); p. 633,647, View in Reaxys

McKillop; Ford; Tetrahedron; vol. 30; nb. 15; (1974); p. 2467 - 2475, View in Reaxys

65 - 66

Snook; Hamilton; Journal of the American Chemical Society; vol. 96; (1974); p. 860,862, View in Reaxys

103.5 - 104

House,H.O. et al.; Journal of Organic Chemistry; vol. 38; (1973); p. 514 522, View in Reaxys

50 - 51

0.3

Beckwith,A.L.J.; Thomas,C.B.; Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999); (1973); p. 861 872, View in Reaxys

84 - 86

Schulz; Jassmann; Bekker; Die Pharmazie; vol. 26; nb. 8; (1971); p. 477 481, View in Reaxys

103

Thibault; Annales de Chimie (Cachan, France); vol. 6; nb. 14; (1971); p. 263,264,265,269, View in Reaxys

62 - 63

0.1

Newman,H.; Angier,R.B.; Tetrahedron; vol. 26; (1970); p. 825 - 836, View in Reaxys

109

Lundeen,A.J.; Oehlschlager,A.C.; Journal of Organometallic Chemistry; vol. 25; (1970); p. 337 - 344, View in Reaxys

127 - 128

DePuy,C.H. et al.; Journal of Organic Chemistry; vol. 35; (1970); p. 2746 2750, View in Reaxys

109 - 111

Deniau et al.; Bulletin de la Societe Chimique de France; (1969); p. 4414, View in Reaxys

110 - 112

Desai,V.R. et al.; Journal of the Chemical Society [Section] B: Physical Organic; (1969); p. 30 - 32, View in Reaxys

118 - 120

Horner; Singer; Chemische Berichte; vol. 101; (1968); p. 3329, View in Reaxys

82 - 83

Nordlander,J.E.; Deadman,W.G.; Journal of the American Chemical Society; vol. 90; (1968); p. 1590 - 1598, View in Reaxys

126

Herling; Pines; Journal of Organic Chemistry; vol. 31; (1966); p. 4088,4091, View in Reaxys

115 - 116

Sacharkin et al.; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); (1965); p. 1159; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; (1965); p. 1194, View in Reaxys

Pines; Schappell; Journal of Organic Chemistry; vol. 29; (1964); p. 1503,1507, View in Reaxys

111 - 112

Gelli et al.; Annali di Chimica (Rome, Italy); vol. 54; (1964); p. 1143,1146, View in Reaxys

103 - 104

Traynelis,V.J. et al.; Journal of Organic Chemistry; vol. 29; (1964); p. 123 129, View in Reaxys

Urry,W.H. et al.; Journal of Organic Chemistry; vol. 29; nb. 7; (1964); p. 1663 - 1669, View in Reaxys; Huston; Bostwick; Journal of Organic Chemistry; vol. 13; (1948); p. 334, View in Reaxys

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98 - 100

Kharasch,M.S. et al.; Journal of the American Chemical Society; vol. 83; (1961); p. 3229 - 3232, View in Reaxys

120 - 121

Kharasch,M.S. et al.; Journal of the American Chemical Society; vol. 83; (1961); p. 3229 - 3232, View in Reaxys

100

Christol et al.; Bulletin de la Societe Chimique de France; (1961); p. 2317, View in Reaxys

103

Sacharkin; Gawrilenko; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); (1960); p. 2081; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; (1960); p. 2245, View in Reaxys

Lichterow; Etlis; Zhurnal Obshchei Khimii; vol. 27; (1957); p. 2867; engl. Ausg. S. 2903, View in Reaxys

123

van der Zanden; Rix; Recueil des Travaux Chimiques des Pays-Bas; vol. 76; (1957); p. 75,77, View in Reaxys

101 - 101.5

Eliel; Lukach; Journal of the American Chemical Society; vol. 79; (1957); p. 5986,5990, View in Reaxys

110

Kornblum et al.; Journal of the American Chemical Society; vol. 77; (1955); p. 5528,5529,5532,6269,6279, View in Reaxys

116

Zeiss; Tsutsui; Journal of the American Chemical Society; vol. 75; (1953); p. 897,899, View in Reaxys

64 - 65

0.7

Siegel et al.; Journal of the American Chemical Society; vol. 73; (1951); p. 3237,3238, View in Reaxys

101 - 102

v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys

219 - 221

Austerweil; Cochin; Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences; vol. 150; (1910); p. 1694, View in Reaxys

212 - 213

fluessig.

Tiffeneau; Annales de Chimie (Cachan, France); vol. <8> 10; (1907); p. 359; Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences; vol. 134; (1902); p. 1506, View in Reaxys

214.5 - 215.5

Errera; Gazzetta Chimica Italiana; vol. 16; (1886); p. 322, View in Reaxys

Refractive Index (24) Refractive Index Wavelength (ReTemperature (Refractive Index) [nm] fractive Index) [°C]

References

1.5218

589

Mamedov; Russian Journal of Applied Chemistry; vol. 79; nb. 3; (2006); p. 408 - 410, View in Reaxys

1.5626

589

Kursanov et al.; Synthesis; (1974); p. 633,647, View in Reaxys

1.5169

589

House,H.O. et al.; Journal of Organic Chemistry; vol. 38; (1973); p. 514 522, View in Reaxys

1.5201

589

Schulz; Jassmann; Bekker; Die Pharmazie; vol. 26; nb. 8; (1971); p. 477 481, View in Reaxys

1.5188

589

Horner; Singer; Chemische Berichte; vol. 101; (1968); p. 3329, View in Reaxys

1.5193

589

Herling; Pines; Journal of Organic Chemistry; vol. 31; (1966); p. 4088,4091, View in Reaxys

1.5179

589

Gelli et al.; Annali di Chimica (Rome, Italy); vol. 54; (1964); p. 1143,1146, View in Reaxys

1.5241

589

Urry,W.H. et al.; Journal of Organic Chemistry; vol. 29; nb. 7; (1964); p. 1663 - 1669, View in Reaxys

1.5194

589

Pines; Schappell; Journal of Organic Chemistry; vol. 29; (1964); p. 1503,1507, View in Reaxys

1.52

589

Traynelis,V.J. et al.; Journal of Organic Chemistry; vol. 29; (1964); p. 123 129, View in Reaxys

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1.5205 - 1.5208

589

Kharasch,M.S. et al.; Journal of the American Chemical Society; vol. 83; (1961); p. 3229 - 3232, View in Reaxys

1.521

589

Kharasch,M.S. et al.; Journal of the American Chemical Society; vol. 83; (1961); p. 3229 - 3232, View in Reaxys; Kornblum et al.; Journal of the American Chemical Society; vol. 77; (1955); p. 5528,5529,5532,6269,6279, View in Reaxys; Lichterow; Etlis; Zhurnal Obshchei Khimii; vol. 27; (1957); p. 2867; engl. Ausg. S. 2903, View in Reaxys

1.5226

589

1.5208

589

Eliel; Lukach; Journal of the American Chemical Society; vol. 79; (1957); p. 5986,5990, View in Reaxys

1.519

589

van der Zanden; Rix; Recueil des Travaux Chimiques des Pays-Bas; vol. 76; (1957); p. 75,77, View in Reaxys

1.5195

589

Zeiss; Tsutsui; Journal of the American Chemical Society; vol. 75; (1953); p. 897,899, View in Reaxys

1.5205

589

Siegel et al.; Journal of the American Chemical Society; vol. 73; (1951); p. 3237,3238, View in Reaxys

1.5221

589

Huston; Bostwick; Journal of Organic Chemistry; vol. 13; (1948); p. 334, View in Reaxys

1.5196

589

Newman; Journal of the American Chemical Society; vol. 62; (1940); p. 2295,2298, View in Reaxys

1.521

589

Golumbic; Cottle; Journal of the American Chemical Society; vol. 61; (1939); p. 996,999, View in Reaxys

1.5202

656.3

14.5

v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys

1.5243

589

14.5

v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys

1.5345

486.1

14.5

v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys

1.5436

434

14.5

v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys

Density (4) 1 of 4

Density [g·cm-3]

0.9981

Reference Temperature [°C]

Measurement Temperature 20 [°C] Sacharkin; Gawrilenko; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); (1960); p. 2081; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; (1960); p. 2245, View in Reaxys 2 of 4

Density [g·cm-3]

1.0021

Reference Temperature [°C]

Measurement Temperature 20 [°C] Lichterow; Etlis; Zhurnal Obshchei Khimii; vol. 27; (1957); p. 2867; engl. Ausg. S. 2903, View in Reaxys 3 of 4

Density [g·cm-3]

0.997

Reference Temperature [°C]

Measurement Temperature 20 [°C] Golumbic; Cottle; Journal of the American Chemical Society; vol. 61; (1939); p. 996,999, View in Reaxys

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4 of 4

Density [g·cm-3]

0.9988

Reference Temperature [°C]

Measurement Temperature 14.5 [°C] v. Auwers; Jordan; Biochemische Zeitschrift; vol. 144; (1924); p. 35,41, View in Reaxys Chromatographic Data (4) Chromatographic Location data

References

LC (Liquid chromatography)

supporting informa- Luecke, Marcel-Philip; Porwal, Digvijay; Kostenko, Arseni; Zhou, Yu-Peng; Yao, Shenglai; tion Keck, Matthias; Limberg, Christian; Oestreich, Martin; Driess, Matthias; Dalton Transactions; vol. 46; nb. 47; (2017); p. 16412 - 16418, View in Reaxys

GC (Gas chromatography)

supporting informa- Chidara, Vamshi K.; Du, Guodong; Organometallics; vol. 32; nb. 18; (2013); p. 5034 - 5037, tion View in Reaxys; Gaertner, Dominik; Welther, Alice; Rad, Babak Rezaei; Wolf, Robert; Von Wangelin, Axel Jacobi; Angewandte Chemie - International Edition; vol. 53; nb. 14; (2014); p. 3722 - 3726; Angew. Chem.; vol. 126; nb. 14; (2014); p. 3796 - 3800,5, View in Reaxys; Deuss, Peter J.; Scott, Martin; Tran, Fanny; Westwood, Nicholas J.; De Vries, Johannes G.; Barta, Katalin; Journal of the American Chemical Society; vol. 137; nb. 23; (2015); p. 7456 - 7467, View in Reaxys

GC (Gas chromatography)

Masek, Anna; Chrzescijanska, Ewa; Kosmalska, Anna; Zaborski, Marian; Food Chemistry; vol. 156; (2014); p. 353 - 361, View in Reaxys; Castelbou, Jessica Llop; Bres-Femenia, Emma; Blondeau, Pascal; Chaudret, Bruno; Castilln, Sergio; Claver, Carmen; Godard, Cyril; ChemCatChem; vol. 6; nb. 11; (2014); p. 3160 - 3168, View in Reaxys

HPLC (High performance liquid chromatography)

Ryu, Dae Won; Lee, Woo Ram; Lim, Kwang Soo; Phang, Won Ju; Hong, Chang Seop; Crystal Growth and Design; vol. 14; nb. 12; (2014); p. 6472 - 6477, View in Reaxys

Conformation (3) Object of Investiga- References tion The author investigated the; Conformation

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys

Conformation

Ditter; Luck; Berichte der Bunsen-Gesellschaft; vol. 73; (1969); p. 526,532, View in Reaxys; Laurent et al.; Bulletin de la Societe Chimique de France; (1967); p. 1995, View in Reaxys; Bakke, Jan M.; Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry; vol. 40; nb. 6; (1986); p. 407 - 410, View in Reaxys; Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys; Ivanov, Petko M.; Spassov, Stefan L.; Journal of Molecular Structure; vol. 145; (1986); p. 181 - 184, View in Reaxys

Energy difference between the conformers

Ivanov, Petko M.; Spassov, Stefan L.; Journal of Molecular Structure; vol. 145; (1986); p. 181 - 184, View in Reaxys

Crystal Property Description (4) Colour & Other Location Properties

References

colourless

supporting informa- Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); tion p. 48 - 51, View in Reaxys; Gaertner, Dominik; Welther, Alice; Rad, Babak Rezaei; Wolf, Robert; Von Wangelin, Axel Jacobi; Angewandte Chemie - International Edition; vol. 53; nb. 14; (2014); p. 3722 - 3726; Angew. Chem.; vol. 126; nb. 14; (2014); p. 3796 - 3800,5, View in Reaxys; Du, Xiaoyong; Zhang, Yanlu; Peng, Dongjie; Huang, Zheng; Angewandte Chemie - International Edition; vol. 55; nb. 23; (2016); p. 6671 - 6675; Angew. Chem.; vol. 128; (2016); p. 6783 - 6787,5, View in Reaxys

colourless

Paragraph 1296

colourless

supporting informa- Gansaeuer, Andreas; Klatte, Max; Braendle, Gerhard M.; Friedrich, Joachim; Angewandte tion Chemie - International Edition; vol. 51; nb. 35; (2012); p. 8891 - 8894, View in Reaxys

light-yellow

Patent; Nimbus Apollo, Inc.; Harriman, Geraldine C.; Masse, Craig E.; Harwood, James; Bhat, Sathesh; Greenwood, Jeremy Robert; US2013/123231; (2013); (A1) English, View in Reaxys

Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys

Further Information (5)

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Description (Further Information)

References

Further information Coutts; Jones; Liu; Biomedical Mass Spectrometry; vol. 5; nb. 6; (1978); p. 418 - 422, View in Reaxys Further information Bulkin et al.; Analytical Chemistry; vol. 43; (1971); p. 974,975, View in Reaxys Further information Namy et al.; Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques; vol. 269; (1969); p. 1222, View in Reaxys Further information Nibbering; de Boer; Organic Mass Spectrometry; vol. 1; (1968); p. 365,372,376,388,389, View in Reaxys Further information Benkeser; Johnston; Journal of the American Chemical Society; vol. 88; (1966); p. 2220,2223, View in Reaxys Ionization Potential (1) References Harrison et al.; Organic Mass Spectrometry; vol. 5; (1971); p. 1313,1318, View in Reaxys Liquid/Liquid Systems (MCS) (1) 1 of 1

Description (Liquid/Liquid Distribution between solvent 1 + 2 Systems (MCS)) Barfknecht; Smith; Nichols; Leseney; Long; Engelbrecht; Journal of pharmaceutical sciences; vol. 60; nb. 5; (1971); p. 799 801, View in Reaxys

Optical Rotatory Power (7) 1 of 7

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

4.56

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Asami; Mukaiyama; Heterocycles; vol. 12; (1979); p. 499,501, View in Reaxys 2 of 7

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

17.8

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Asami; Mukaiyama; Heterocycles; vol. 12; (1979); p. 499,501, View in Reaxys 3 of 7

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

12.9

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Asami et al.; Bulletin of the Chemical Society of Japan; vol. 51; (1978); p. 1869, View in Reaxys 4 of 7

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

11.92

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

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Vigneron; Jacquet; Tetrahedron; vol. 32; (1976); p. 939,944, View in Reaxys 5 of 7

Patent; Monsanto Company; US3968147; (1976); (A) English, View in Reaxys

6 of 7

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

0.12

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Meyers,A.I.; Kendall,P.M.; Tetrahedron Letters; nb. 14; (1974); p. 1337 - 1340, View in Reaxys 7 of 7

Laurent et al.; Bulletin de la Societe Chimique de France; (1967); p. 1995, View in Reaxys

Other Thermochemical Data (1) Description (Other References Thermochemical Data) Thermodynamic properties

Luck; Ditter; Berichte der Bunsen-Gesellschaft; vol. 75; (1971); p. 163,165, View in Reaxys

NMR Spectroscopy (41) 1 of 41

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 400 scopy) [MHz] Location

supporting information

Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); p. 48 - 51, View in Reaxys; Kitamoto, Yuichi; Kuruma, Yosuke; Suzuki, Kazumi; Hattori, Tetsutaro; Journal of Organic Chemistry; vol. 80; nb. 1; (2015); p. 521 - 527, View in Reaxys; Du, Xiaoyong; Zhang, Yanlu; Peng, Dongjie; Huang, Zheng; Angewandte Chemie International Edition; vol. 55; nb. 23; (2016); p. 6671 - 6675; Angew. Chem.; vol. 128; (2016); p. 6783 - 6787,5, View in Reaxys; Luecke, Marcel-Philip; Porwal, Digvijay; Kostenko, Arseni; Zhou, Yu-Peng; Yao, Shenglai; Keck, Matthias; Limberg, Christian; Oestreich, Martin; Driess, Matthias; Dalton Transactions; vol. 46; nb. 47; (2017); p. 16412 16418, View in Reaxys 2 of 41

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 101 scopy) [MHz] Location

supporting information

Du, Xiaoyong; Zhang, Yanlu; Peng, Dongjie; Huang, Zheng; Angewandte Chemie - International Edition; vol. 55; nb. 23; (2016); p. 6671 - 6675; Angew. Chem.; vol. 128; (2016); p. 6783 - 6787,5, View in Reaxys; Luecke, Marcel-Philip; Porwal, Digvijay; Kostenko, Arseni; Zhou, Yu-Peng; Yao, Shenglai; Keck, Matthias; Limberg, Christian; Oestreich, Martin; Driess, Matthias; Dalton Transactions; vol. 46; nb. 47; (2017); p. 16412 - 16418, View in Reaxys 3 of 41

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

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Frequency (NMR Spectro- 100 scopy) [MHz] Location

supporting information

Kitamoto, Yuichi; Kuruma, Yosuke; Suzuki, Kazumi; Hattori, Tetsutaro; Journal of Organic Chemistry; vol. 80; nb. 1; (2015); p. 521 - 527, View in Reaxys 4 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 101 scopy) [MHz] Location

supporting information

Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); p. 48 - 51, View in Reaxys 5 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 300 scopy) [MHz] Location

supporting information

Gaertner, Dominik; Welther, Alice; Rad, Babak Rezaei; Wolf, Robert; Von Wangelin, Axel Jacobi; Angewandte Chemie International Edition; vol. 53; nb. 14; (2014); p. 3722 - 3726; Angew. Chem.; vol. 126; nb. 14; (2014); p. 3796 - 3800,5, View in Reaxys 6 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 75 scopy) [MHz] Location

supporting information

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Temperature (NMR Spectroscopy) [°C]

24.84

Frequency (NMR Spectro- 500 scopy) [MHz] Location

supporting information

Chidara, Vamshi K.; Du, Guodong; Organometallics; vol. 32; nb. 18; (2013); p. 5034 - 5037, View in Reaxys

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8 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 400 scopy) [MHz] Vitale, Paola; Perna, Filippo Maria; Perrone, Maria Grazia; Scilimati, Antonio; Tetrahedron Asymmetry; vol. 22; nb. 23; (2011); p. 1985 - 1993, View in Reaxys 9 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 100 scopy) [MHz] Vitale, Paola; Perna, Filippo Maria; Perrone, Maria Grazia; Scilimati, Antonio; Tetrahedron Asymmetry; vol. 22; nb. 23; (2011); p. 1985 - 1993, View in Reaxys 10 of 41

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

Frequency (NMR Spectro- 500 scopy) [MHz] Location

supporting information

Blasio, Nadia Di; Lopardo, Maria Teresa; Lupattelli, Paolo; European Journal of Organic Chemistry; nb. 6; (2009); p. 938 944, View in Reaxys 11 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 400 scopy) [MHz] Location

supporting information

Lee, Yunmi; Hoveyda, Amir H.; Journal of the American Chemical Society; vol. 131; (2009); p. 3160 - 3161, View in Reaxys 12 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 100 scopy) [MHz] Location

supporting information

Lee, Yunmi; Hoveyda, Amir H.; Journal of the American Chemical Society; vol. 131; (2009); p. 3160 - 3161, View in Reaxys 13 of 41

Description (NMR Spectroscopy)

Chemical shifts

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Nucleus (NMR Spectroscopy)

Sonawane, H. R.; Sethi, S. C.; Merchant, S. N.; Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry; vol. 23; nb. 10; (1984); p. 940 - 943, View in Reaxys; Scheideman, Matthew; Wang, Guoqiang; Vedejs, Edwin; Journal of the American Chemical Society; vol. 130; nb. 27; (2008); p. 8669 - 8676, View in Reaxys 14 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Frequency (NMR Spectro- 300 scopy) [MHz] Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys; Erdelyi, Balazs; Szabo, Antal; Seres, Gabor; Birincsik, Laszlo; Ivanics, Jozsef; Szatzker, Gabor; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 17; nb. 2; (2006); p. 268 - 274, View in Reaxys 15 of 41

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Frequency (NMR Spectro- 300 scopy) [MHz] Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys 16 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

CDCl3

Frequency (NMR Spectro- 74 scopy) [MHz] Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys 17 of 41

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

CDCl3

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

CDCl3

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Frequency (NMR Spectro- 75 scopy) [MHz] Erdelyi, Balazs; Szabo, Antal; Seres, Gabor; Birincsik, Laszlo; Ivanics, Jozsef; Szatzker, Gabor; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 17; nb. 2; (2006); p. 268 - 274, View in Reaxys 19 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CCl4

Temperature (NMR Spectroscopy) [°C]

Frequency (NMR Spectro- 80 scopy) [MHz] Mamedov; Russian Journal of Applied Chemistry; vol. 79; nb. 3; (2006); p. 408 - 410, View in Reaxys 20 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Frequency (NMR Spectro- 500 scopy) [MHz] Li, Yanjun; Izumi, Taeko; Journal of the Chinese Chemical Society (Taipei, Taiwan); vol. 49; nb. 4; (2002); p. 505 - 508, View in Reaxys; Li, Yanjun; Izumi, Taeko; Journal of Chemical Research - Part S; nb. 3; (2003); p. 128 - 129, View in Reaxys; Hatzakis, Nikos S.; Smonou, Ioulia; Bioorganic Chemistry; vol. 33; nb. 4; (2005); p. 325 - 337, View in Reaxys 21 of 41

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

CDCl3

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Frequency (NMR Spectro- 250 scopy) [MHz] Choukchou-Braham; Mostefa-Kara; Cheikh; Didi; Villemin; Synthetic Communications; vol. 35; nb. 2; (2005); p. 169 178, View in Reaxys 23 of 41

Description (NMR Spectroscopy)

NOE

Nucleus (NMR Spectroscopy)

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys

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24 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys 25 of 41

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys 26 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Frequency (NMR Spectro- 400.1 scopy) [MHz] Ley, Steven V.; Mitchell, Claire; Pears, David; Ramarao, Chandrashekar; Yu, Jin-Quan; Zhou, Wuzong; Organic Letters; vol. 5; nb. 24; (2003); p. 4665 - 4668, View in Reaxys 27 of 41

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Frequency (NMR Spectro- 100.6 scopy) [MHz]

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Ley, Steven V.; Mitchell, Claire; Pears, David; Ramarao, Chandrashekar; Yu, Jin-Quan; Zhou, Wuzong; Organic Letters; vol. 5; nb. 24; (2003); p. 4665 - 4668, View in Reaxys 29 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Brown, Herbert C.; Narasimhan, S.; Somayaji, Vishwanatha; Journal of Organic Chemistry; vol. 48; nb. 18; (1983); p. 3091 - 3096, View in Reaxys; Hayashi; Matsumoto; Ito; Tetrahedron Asymmetry; vol. 2; nb. 7; (1991); p. 601 - 612, View in Reaxys; Deniau, Jean; Van Duong, Kiem Nguyen; Merienne, Claude; Gaudemer, Alain; Bulletin de la Societe Chimique de France; vol. 2; nb. 5-6; (1983); p. 180 - 184, View in Reaxys; Sosnovskii, G. M.; Astapovich, I. V.; Journal of Organic Chemistry USSR (English Translation); vol. 28; nb. 7.1; (1992); p. 1082 - 1084; Zhurnal Organicheskoi Khimii; vol. 28; nb. 7; (1992); p. 1377 - 1379, View in Reaxys 30 of 41

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CDCl3

Comment (NMR Spectroscopy)

1H-1H

Hayashi; Matsumoto; Ito; Tetrahedron Asymmetry; vol. 2; nb. 7; (1991); p. 601 - 612, View in Reaxys; Deniau, Jean; Van Duong, Kiem Nguyen; Merienne, Claude; Gaudemer, Alain; Bulletin de la Societe Chimique de France; vol. 2; nb. 5-6; (1983); p. 180 - 184, View in Reaxys 31 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

neat (no solvent)

Eisch, John J.; Galle, James E.; Journal of Organometallic Chemistry; vol. 341; (1988); p. 293 - 314, View in Reaxys 32 of 41

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CCl4; CCl3F

Comment (NMR Spectroscopy)

1H-1H.

Bakke, Jan M.; Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry; vol. 40; nb. 6; (1986); p. 407 410, View in Reaxys 33 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Dao, Le Thi Anh; Blau, Karla; Pritzkow, Wilhelm; Schmidt-Renner, Wolfgang; Voerckel, Volkmar; Willecke, Lothar; Journal fuer Praktische Chemie (Leipzig); vol. 326; nb. 1; (1984); p. 73 - 80, View in Reaxys 34 of 41

Description (NMR Spectroscopy)

Spin-spin coupling constants

Comment (NMR Spectroscopy)

1H-1H

Sonawane, H. R.; Sethi, S. C.; Merchant, S. N.; Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry; vol. 23; nb. 10; (1984); p. 940 - 943, View in Reaxys 35 of 41

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

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Solvents (NMR Spectroscopy)

CCl4

Temperature (NMR Spectroscopy) [°C]

Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys 36 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CCl4

Temperature (NMR Spectroscopy) [°C]

Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys 37 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

CDCl3

Temperature (NMR Spectroscopy) [°C]

Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys 38 of 41

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CCl4

Temperature (NMR Spectroscopy) [°C]

Comment (NMR Spectroscopy)

1H-1H.

Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys 39 of 41

Description (NMR Spectroscopy)

NMR with shift reagents

Zushi, Shoji; Kodama, Yoshio; Fukuda, Yoshimasa; Nishihata, Ken; Nishio, Motohiro; et aol.; Bulletin of the Chemical Society of Japan; vol. 54; nb. 7; (1981); p. 2113 - 2119, View in Reaxys 40 of 41

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CCl4

Bourgain-Commercon, Monique; Normant, Jean F.; Bulletin de la Societe Chimique de France; vol. 2; nb. 5-6; (1980); p. 289 - 294, View in Reaxys 41 of 41

Description (NMR Spectroscopy)

NMR

Schwartz et al.; Journal of Organic Chemistry; vol. 39; (1974); p. 219,221, View in Reaxys; Mason; Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999); (1975); p. 1664, View in Reaxys; Vigneron et al.; Tetrahedron; vol. 29; (1973); p. 1055,1056, 1059, View in Reaxys

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IR Spectroscopy (13) 1 of 13

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

neat (no solvent)

Vitale, Paola; Perna, Filippo Maria; Perrone, Maria Grazia; Scilimati, Antonio; Tetrahedron Asymmetry; vol. 22; nb. 23; (2011); p. 1985 - 1993, View in Reaxys 2 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

neat (no solvent)

Blakemore, Paul R.; Marsden, Stephen P.; Vater, Huw D.; Organic Letters; vol. 8; nb. 4; (2006); p. 773 - 776, View in Reaxys 3 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

film

Erdelyi, Balazs; Szabo, Antal; Seres, Gabor; Birincsik, Laszlo; Ivanics, Jozsef; Szatzker, Gabor; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 17; nb. 2; (2006); p. 268 - 274, View in Reaxys 4 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

CCl4

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys; Mamedov; Russian Journal of Applied Chemistry; vol. 79; nb. 3; (2006); p. 408 - 410, View in Reaxys 5 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

CHCl3

Choukchou-Braham; Mostefa-Kara; Cheikh; Didi; Villemin; Synthetic Communications; vol. 35; nb. 2; (2005); p. 169 178, View in Reaxys 6 of 13

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

CCl4

Takahashi, Osamu; Saito, Ko; Kohno, Yuji; Suezawa, Hiroko; Ishihara, Shinji; Nishio, Motohiro; European Journal of Organic Chemistry; nb. 11; (2004); p. 2398 - 2403, View in Reaxys 7 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

neat liquid

Ley, Steven V.; Mitchell, Claire; Pears, David; Ramarao, Chandrashekar; Yu, Jin-Quan; Zhou, Wuzong; Organic Letters; vol. 5; nb. 24; (2003); p. 4665 - 4668, View in Reaxys 8 of 13

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

various solvent(s)

Comment (IR Spectroscopy)

3620 - 3598 cm**(-1)

Bakke, Jan M.; Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry; vol. 40; nb. 6; (1986); p. 407 410, View in Reaxys 9 of 13

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

3250 - 706 cm**(-1)

Sonawane, H. R.; Sethi, S. C.; Merchant, S. N.; Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry; vol. 23; nb. 10; (1984); p. 940 - 943, View in Reaxys

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10 of 13

Description (IR Spectroscopy)

Eliel; Rerick; Journal of the American Chemical Society; vol. 82; (1960); p. 1362,1365, View in Reaxys; Ditter; Luck; Berichte der Bunsen-Gesellschaft; vol. 73; (1969); p. 526,532, View in Reaxys; Kirchner; Richter; Zeitschrift fuer Physikalische Chemie (Muenchen, Germany); vol. 81; (1972); p. 274, View in Reaxys 11 of 13

Description (IR Spectroscopy)

Spectrum

Suga et al.; Kogyo Kagaku Zasshi; vol. 70; (1967); p. 487,489, View in Reaxys 12 of 13

Description (IR Spectroscopy)

Spectrum

Comment (IR Spectroscopy)

1020 - 952 cm**(-1); Fluessigkeit.

Winstein; Trifan; Journal of the American Chemical Society; vol. 74; (1952); p. 1154,1159; Journal of the American Chemical Society; vol. 71; (1949); p. 2953, View in Reaxys 13 of 13

Description (IR Spectroscopy)

Spectrum

Comment (IR Spectroscopy)

12500 - 8333 cm**(-1)

Freymann; Annales de Physique (Paris, France); vol. <10> 20; (1933); p. 243,266, 289, 305-307; Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences; vol. 206; (1938); p. 1812, View in Reaxys Mass Spectrometry (8) Description (Mass Location Spectrometry) gas chromatography mass spectrometry (GCMS); spectrum

References Masek, Anna; Chrzescijanska, Ewa; Kosmalska, Anna; Zaborski, Marian; Food Chemistry; vol. 156; (2014); p. 353 - 361, View in Reaxys; Sarkar, Md. Raihan; Lee, Joel H. Z.; Bell, Stephen G.; ChemBioChem; vol. 18; nb. 21; (2017); p. 2119 - 2128, View in Reaxys

gas chromatograsupporting informa- Chidara, Vamshi K.; Du, Guodong; Organometallics; vol. 32; nb. 18; (2013); p. 5034 - 5037, phy mass spectrom- tion View in Reaxys; Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. etry (GCMS); spec136; nb. 1; (2014); p. 48 - 51, View in Reaxys trum electron impact (EI); spectrum

supporting informa- Gaertner, Dominik; Welther, Alice; Rad, Babak Rezaei; Wolf, Robert; Von Wangelin, Axel tion Jacobi; Angewandte Chemie - International Edition; vol. 53; nb. 14; (2014); p. 3722 - 3726; Angew. Chem.; vol. 126; nb. 14; (2014); p. 3796 - 3800,5, View in Reaxys Page/Page column 18

GCMS (Gas chromatography mass spectrometry); Spectrum

Patent; Dong, Guangbin; Grubbs, Robert H.; Teo, Peili; Wickens, Zach K.; US2012/172634; (2012); (A1) English, View in Reaxys

supporting informa- Protti, Stefano; Ravelli, Davide; Mannucci, Barbara; Albini, Angelo; Fagnoni, Maurizio; Antion gewandte Chemie - International Edition; vol. 51; nb. 34; (2012); p. 8577 - 8580, View in Reaxys

Spectrum

Vitale, Paola; Perna, Filippo Maria; Perrone, Maria Grazia; Scilimati, Antonio; Tetrahedron Asymmetry; vol. 22; nb. 23; (2011); p. 1985 - 1993, View in Reaxys

spectrum; electron impact (EI)

Marques, Carlos Alberto; Selva, Maurizio; Tundo, Pietro; Journal of Organic Chemistry; vol. 60; nb. 8; (1995); p. 2430 - 2435, View in Reaxys Coutts; Jones; Liu; Biomedical Mass Spectrometry; vol. 5; nb. 6; (1978); p. 418 - 422, View in Reaxys; Harrison et al.; Organic Mass Spectrometry; vol. 5; (1971); p. 1313,1318, View in Reaxys; Nibbering; de Boer; Organic Mass Spectrometry; vol. 1; (1968); p. 365,372,376,388,389, View in Reaxys

UV/VIS Spectroscopy (1) 1 of 1

Description (UV/VIS Spectroscopy)

UV/VIS

Barfknecht; Smith; Nichols; Leseney; Long; Engelbrecht; Journal of pharmaceutical sciences; vol. 60; nb. 5; (1971); p. 799 801, View in Reaxys Rotational Spectroscopy (1)

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Description (Rotational Spectroscopy)

References

Microwave spectrum

Luck; Ditter; Berichte der Bunsen-Gesellschaft; vol. 75; (1971); p. 163,165, View in Reaxys

Raman Spectroscopy (1) Description (Ram- References an Spectroscopy) Spectrum

Bulkin et al.; Analytical Chemistry; vol. 43; (1971); p. 974,975, View in Reaxys

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