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6 reactions in Reaxys
2018-05-13 18h:58m:43s (UTC)
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1. Query
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Search as: Product, As drawn, No mixtures ))
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Rx-ID: 46790082 View in Reaxys 1/6 Yield
Conditions & References
63 %
in tetrahydrofuran, Time= 30h, T= 25 °C , Sealed tube Gallo, Rafael D. C.; Ahmad, Anees; Metzker, Gustavo; Burtoloso, Antonio C. B.; Chemistry - A European Journal; vol. 23; nb. 67; (2017); p. 16980 - 16984 View in Reaxys
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Cl
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Rx-ID: 46790092 View in Reaxys 2/6 Yield
Conditions & References Reaction Steps: 2 1.1: potassium tert-butylate / tetrahydrofuran / 2 h / Inert atmosphere; Reflux 1.2: 3 h / 0 - 25 °C / Inert atmosphere 2.1: tetrahydrofuran / 30 h / 25 °C / Sealed tube With potassium tert-butylate in tetrahydrofuran Gallo, Rafael D. C.; Ahmad, Anees; Metzker, Gustavo; Burtoloso, Antonio C. B.; Chemistry - A European Journal; vol. 23; nb. 67; (2017); p. 16980 - 16984 View in Reaxys
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Rx-ID: 9248167 View in Reaxys 3/6 Yield 90 %
Conditions & References With N-iodo-succinimide, toluene-4-sulfonic acid, Microwave irradiation Lee, Jong Chan; Bae, Yong Hun; Synlett; nb. 4; (2003); p. 507 - 508 View in Reaxys
84 %
With [hydroxy(tosyloxy)iodo]benzene, iodine, 1-butyl-3-methylimidazolium Tetrafluoroborate, T= 60 °C , Ionic liquid Lee, Jong Chan; Kim, Jimi; Park, Hyun Jung; Kwag, Byungmook; Lee, Seung Bae; Bulletin of the Korean Chemical Society; vol. 31; nb. 5; (2010); p. 1385 - 1386 View in Reaxys O O
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Rx-ID: 5222163 View in Reaxys 4/6 Yield
Conditions & References With 18-crown-6 ether, potassium iodide in acetonitrile, Time= 1h, T= 20 °C , Iodination
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Lee, Jong Chan; Jin, Yong Suk; Synthetic Communications; vol. 29; nb. 16; (1999); p. 2769 - 2774 View in Reaxys
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2-methyl-5-propyl-phenyl magnesium bromide O
Rx-ID: 16259636 View in Reaxys 5/6 Yield
Conditions & References Reaction Steps: 2 1: acetonitrile / Heating 2: potassium iodide; 18-crown-6 / acetonitrile / 1 h / 20 °C With 18-crown-6 ether, potassium iodide in acetonitrile, 1: sulfonyloxylation / 2: Iodination Lee, Jong Chan; Jin, Yong Suk; Synthetic Communications; vol. 29; nb. 16; (1999); p. 2769 - 2774 View in Reaxys O
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Rx-ID: 333108 View in Reaxys 6/6 Yield
Conditions & References With potassium iodide Collet; Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences; vol. 128; (1899); p. 313 View in Reaxys
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