(R)-1-Phenyl-2-propanol (P2Pol) [C9H12O] by Asch

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1 substances in Reaxys

2018-05-22 18h:55m:49s (UTC)

1. Query

Search as: As drawn ) AND (IDE.XRN=3195620))

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Reaxys ID 3195620 View in Reaxys

1/1 CAS Registry Number: 1572-95-8 Chemical Name: (R)-1-phenyl-propan-2-ol; (2R)-1-phenylpropan-2ol; (R)-1-Phenyl-2-propanol; (R)-1-Phenylpropan-2-ol; phenyl 2propanol; 1-phenyl-2-propanol; 1-phenylpropan-2-ol Linear Structure Formula: C9H12O Molecular Formula: C9H12O Molecular Weight: 136.194 Type of Substance: isocyclic InChI Key: WYTRYIUQUDTGSX-MRVPVSSYSA-N Note:

Substance Label (48) Label References R-3

de Leeuw, Nicolas; Torrelo, Guzman; Bisterfeld, Carolin; Resch, Verena; Mestrom, Luuk; Straulino, Emanuele; van der Weel, Laura; Hanefeld, Ulf; Advanced Synthesis and Catalysis; vol. 360; nb. 2; (2018); p. 242 - 249, View in Reaxys

(R)-43

Neyyappadath, Rifahath Mon; Chisholm, Ross; Greenhalgh, Mark D.; Rodríguez-Escrich, Carles; Pericàs, Miquel A.; Hähner, Georg; Smith, Andrew D.; ACS Catalysis; vol. 8; nb. 2; (2018); p. 1067 - 1075, View in Reaxys

(R)-10b

Qu, Ge; Lonsdale, Richard; Yao, Peiyuan; Li, Guangyue; Liu, Beibei; Reetz, Manfred T.; Sun, Zhoutong; ChemBioChem; vol. 19; nb. 3; (2018); p. 239 - 246, View in Reaxys

(R)-2a

Musidlowska, Anna; Lange, Stefan; Bornscheuer, Uwe T.; Angewandte Chemie - International Edition; vol. 40; nb. 15; (2001); p. 2851 - 2853, View in Reaxys; Vitale, Paola; Abbinante, Vincenzo Mirco; Perna, Filippo Maria; Salomone, Antonio; Cardellicchio, Cosimo; Capriati, Vito; Advanced Synthesis and Catalysis; vol. 359; nb. 6; (2017); p. 1049 - 1057, View in Reaxys; Hoang, Hai Nam; Nagashima, Yoshihiro; Mori, Shuichi; Kagechika, Hiroyuki; Matsuda, Tomoko; Tetrahedron; vol. 73; nb. 20; (2017); p. 2984 - 2989, View in Reaxys

(R)-1a

Musa, Musa M.; Phillips, Robert S.; Laivenieks, Maris; Vieille, Claire; Takahashi, Masateru; Hamdan, Samir M.; Organic and Biomolecular Chemistry; vol. 11; nb. 17; (2013); p. 2911 - 2915, View in Reaxys; Musa, Musa M.; Patel, Jay M.; Nealon, Christopher M.; Kim, Chang Sup; Phillips, Robert S.; Karume, Ibrahim; Journal of Molecular Catalysis B: Enzymatic; vol. 115; (2015); p. 155 - 159, View in Reaxys; Karume, Ibrahim; Musa, Musa M.; Bsharat, Odey; Takahashi, Masateru; Hamdan, Samir M.; El Ali, Bassam; RSC Advances; vol. 6; nb. 99; (2016); p. 96616 - 96622, View in Reaxys; Knaus, Tanja; Cariati, Luca; Masman, Marcelo F; Mutti, Francesco G.; Organic and Biomolecular Chemistry; vol. 15; nb. 39; (2017); p. 8313 - 8325, View in Reaxys

(R)-1P2P

Zhang, Shi-Yuan; Yang, Cheng-Xiong; Shi, Wei; Yan, Xiu-Ping; Cheng, Peng; Wojtas, Lukasz; Zaworotko, Michael J.; Chem; vol. 3; nb. 2; (2017); p. 281 - 289, View in Reaxys

Song, Heng; Ye, Ke; Geng, Peiyu; Han, Xiao; Liao, Rongzhen; Tung, Chen-Ho; Wang, Wenguang; ACS Catalysis; vol. 7; nb. 11; (2017); p. 7709 - 7717, View in Reaxys

(R)-2g

Benítez-Mateos, Ana I.; San Sebastian, Eneko; Ríos-Lombardía, Nicolás; Morís, Francisco; González-Sabín, Javier; López-Gallego, Fernando; Chemistry - A European Journal; vol. 23; nb. 66; (2017); p. 16843 - 16852, View in Reaxys

(R)-4b

Musa, Musa M.; Ziegelmann-Fjeld, Karla I.; Vieille, Claire; Zeikus, J. Gregory; Phillips, Robert S.; Angewandte Chemie - International Edition; vol. 46; nb. 17; (2007); p. 3091 - 3094, View in Reaxys; Sun, Zhoutong; Li, Guangyue; Ilie, Adriana; Reetz, Manfred T.; Tetrahedron Letters; vol. 57; nb. 32; (2016); p. 3648 - 3651, View in Reaxys

Veguillas, Marcos; Solà, Ricard; Shaw, Luke; Maciá, Beatriz; European Journal of Organic Chemistry; vol. 2016; nb. 9; (2016); p. 1788 - 1794, View in Reaxys

(R)-1d

Karume, Ibrahim; Takahashi, Masateru; Hamdan, Samir M.; Musa, Musa M.; ChemCatChem; vol. 8; nb. 8; (2016); p. 1459 - 1463, View in Reaxys

Veguillas, Marcos; Solà, Ricard; Fernández-Ibañez, M. Ángeles; Maciá, Beatriz; Tetrahedron Asymmetry; vol. 27; nb. 14-15; (2016); p. 643 - 648, View in Reaxys

Bódai, Viktória; Nagy-Győr, László; Örkényi, Róbert; Molnár, Zsófia; Kohári, Szabolcs; Erdélyi, Balázs; Nagymáté, Zsuzsanna; Romsics, Csaba; Paizs, Csaba; Poppe, László; Hornyánszky, Gábor; Journal of Molecular Catalysis B: Enzymatic; vol. 134; (2016); p. 206 - 214, View in Reaxys

(R)-5

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys; Kitamoto, Yuichi; Kuruma, Yosuke; Suzuki, Kazumi; Hattori, Tetsutaro; Journal of Organic Chemistry; vol. 80; nb. 1; (2015); p. 521 - 527, View in Reaxys

Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 137; nb. 9; (2015); p. 3327 - 3340, View in Reaxys

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2aj

Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); p. 48 - 51, View in Reaxys

Su, Erzheng; Xu, Jingjing; You, Pengyong; Journal of Molecular Catalysis B: Enzymatic; vol. 106; (2014); p. 11 - 16, View in Reaxys

Yin, Yue-Cai; Yu, Hui-Lei; Luan, Zheng-Jiao; Li, Ren-Jie; Ouyang, Peng-Fei; Liu, Jing; Xu, Jian-He; ChemBioChem; vol. 15; nb. 16; (2014); p. 2443 - 2449, View in Reaxys; Yin, Yue-Cai; Yu, Hui-Lei; Luan, Zheng-Jiao; Li, Ren-Jie; Ouyang, Peng-Fei; Liu, Jing; Xu, Jian-He; ChemBioChem; vol. 15; nb. 16; (2014); p. 2443 - 2449, View in Reaxys

(R)-21

Nakamura, Yukie; Egami, Hiromichi; Matsumoto, Kazuhiro; Uchida, Tatsuya; Katsuki, Tsutomu; Tetrahedron; vol. 63; nb. 28; (2007); p. 6383 - 6387, View in Reaxys; Hellmann, Gunther; Hack, Achim; Thiemermann, Eric; Luche, Olaf; Raabe, Gerhard; Gais, Hans-Joachim; Chemistry - A European Journal; vol. 19; nb. 12; (2013); p. 3869 - 3897, View in Reaxys

3; 8a

Villalpando, Andres; Ayala, Caitlan E.; Watson, Christopher B.; Kartika, Rendy; Journal of Organic Chemistry; vol. 78; nb. 8; (2013); p. 3989 - 3996, View in Reaxys

Pinaka, Afroditi; Dimotikali, Dimitra; Chankvetadze, Bezhan; Papadopoulos, Kyriakos; Vougioukalakis, Georgios C.; Synlett; vol. 24; nb. 18; (2013); p. 2401 - 2406; Art.No: ST-2013-B0829-L, View in Reaxys

Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei; Organic and Biomolecular Chemistry; vol. 10; nb. 14; (2012); p. 2730 - 2732, View in Reaxys

(R)-11

Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu; Letters in Organic Chemistry; vol. 9; nb. 9; (2012); p. 615 - 621, View in Reaxys

(R)-1c

Csajagi, Csaba; Szatzker, Gabor; Rita Toke, Eniko; Uerge, Laszlo; Darvas, Ferenc; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 19; nb. 2; (2008); p. 237 - 246, View in Reaxys

(R)-2b

Erdelyi, Balazs; Szabo, Antal; Seres, Gabor; Birincsik, Laszlo; Ivanics, Jozsef; Szatzker, Gabor; Poppe, Laszlo; Tetrahedron Asymmetry; vol. 17; nb. 2; (2006); p. 268 - 274, View in Reaxys

(R)-(-)-1

Kiss, Violetta; Egri, Gabriella; Balint, Jozsef; Ling, Istvan; Barkoczi, Jozsef; Fogassy, Elemer; Tetrahedron Asymmetry; vol. 17; nb. 15; (2006); p. 2220 - 2234, View in Reaxys

(R)-6h

Boren, Linnea; Martin-Matute, Belen; Xu, Yongmei; Cordova, Armando; Baeckvall, Jan-E.; Chemistry - A European Journal; vol. 12; nb. 1; (2006); p. 225 - 232, View in Reaxys

Boros, Eric E.; Deaton, David N.; Hassell, Anne M.; McFadyen, Robert B.; Miller, Aaron B.; Miller, Larry R.; Paulick, Margot G.; Shewchuk, Lisa M.; Thompson, James B.; Willard Jr., Derril H.; Wright, Lois L.; Bioorganic and Medicinal Chemistry Letters; vol. 14; nb. 13; (2004); p. 3425 - 3429, View in Reaxys

t.5, β-product, (R)

Connolly, David J.; Lacey, Patrick M.; McCarthy, Mary; Saunders, Cormac P.; Carroll, Anne-Marie; Goddard, Richard; Guiry, Patrick J.; Journal of Organic Chemistry; vol. 69; nb. 20; (2004); p. 6572 - 6589, View in Reaxys

Shi, Xiao-Xin; Yao, Jian-Zhong; Kang, Li; Shen, Chun-Li; Yi, Fei; Journal of Chemical Research; nb. 10; (2004); p. 681 - 683, View in Reaxys

Masaki, Yukio; Arasaki, Hideki; Iwata, Masashi; Chemistry Letters; vol. 32; nb. 1; (2003); p. 4 - 5, View in Reaxys

(R)-39b

Stampfer, Wolfgang; Kosjek, Birgit; Faber, Kurt; Kroutil, Wolfgang; Journal of Organic Chemistry; vol. 68; nb. 2; (2003); p. 402 - 406, View in Reaxys

(R)-3b

Nakamura, Kaoru; Fujii, Mikio; Ida, Yoshiteru; Tetrahedron Asymmetry; vol. 12; nb. 22; (2001); p. 3147 - 3153, View in Reaxys

(R)-3a

Allan; Carnell; Journal of Organic Chemistry; vol. 66; nb. 19; (2001); p. 6495 - 6497, View in Reaxys

Sano, Tomohumi; Imai, Keisuke; Ohashi, Kousaburo; Oriyama, Takeshi; Chemistry Letters; nb. 3; (1999); p. 265 266, View in Reaxys

(R)-1k

Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Misawa, Ibuki; Journal of the Chemical Society - Perkin Transactions 1; nb. 16; (1999); p. 2397 - 2402, View in Reaxys

(R)-4

Ema, Tadashi; Kobayashi, Juka; Maeno, Soichi; Sakai, Takashi; Utaka, Masanori; Bulletin of the Chemical Society of Japan; vol. 71; nb. 2; (1998); p. 443 - 453, View in Reaxys

(R)-5c

Gutman, Arie L.; Brenner, Dov; Boltanski, Aviv; Tetrahedron: Asymmetry; vol. 4; nb. 5; (1993); p. 839 - 844, View in Reaxys; Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

prod. Tab 2, entry 3 Chiodi, Olivier; Fotiadu, Frederic; Sylvestre, Maud; Buono, Gerard; Tetrahedron Letters; vol. 37; nb. 1; (1996); p. 39 - 42, View in Reaxys (-)-7d

Corelli; Summa; Brogi; Monteagudo; Botta; Journal of Organic Chemistry; vol. 60; nb. 7; (1995); p. 2008 - 2015, View in Reaxys

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(R)-C6H5CH2CH(OH)-CH3

Kim, Yong Hae; Park, Doo Han; Byun, Il Suk; Yoon, I. K.; Park, C. S.; Journal of Organic Chemistry; vol. 58; nb. 17; (1993); p. 4511 - 4512, View in Reaxys

(R)-7; R1= CH2Ph R2= Me

Yamamoto, Koji; Ueno, Koji; Naemura, Koichiro; Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999); nb. 4; (1991); p. 2607 - 2608, View in Reaxys

Conte, V.; Furia, F. Di; Licini, G.; Modena, G.; Sbampato, G.; Valle, G.; Tetrahedron: Asymmetry; vol. 2; nb. 4; (1991); p. 257 - 276, View in Reaxys

DeNinno; Perner; Lijewski; Tetrahedron Letters; vol. 31; nb. 51; (1990); p. 7415 - 7418, View in Reaxys

(-)-(7)

Laumen, Kurt; Schneider, Manfred P.; Journal of the Chemical Society, Chemical Communications; (1988); p. 598 600, View in Reaxys

(R)-3, Table I entry 6

Imai, Toshiro; Tamura, Tadashi; Yamamuro, Akira; Sato, Tsuneo; Wollmann, Theodor A.; et al.; Journal of the American Chemical Society; vol. 108; nb. 23; (1986); p. 7402 - 7404, View in Reaxys

R(-)-IV

Prelusky; Coutts; Pasutto; Journal of Pharmaceutical Sciences; vol. 71; nb. 12; (1982); p. 1390 - 1393, View in Reaxys

(R)-15

Kirmse, Wolfgang; Guenther, Bernd-Rainer; Loosen, Karin; Chemische Berichte; vol. 113; nb. 6; (1980); p. 2140 2153, View in Reaxys

Druglikeness (1) 1 of 1

LogP

1.829

H Bond Donors

H Bond Acceptors

Rotatable Bonds

TPSA

20.23

Lipinski Number

Veber Number

Related Structure (1) Related Structure References Configuration.

Levene; Walti; Journal of Biological Chemistry; vol. 90; (1931); p. 81,86, View in Reaxys

Derivative (1) Comment (Derivative)

References

naphthyl-(1)-carbamoyl derivative (mp: 111-113 degree ) Purification (2) Purification (method)

Levene; Walti; Journal of Biological Chemistry; vol. 90; (1931); p. 81,86, View in Reaxys

References

via selective acyla- Gutman, Arie L.; Brenner, Dov; Boltanski, Aviv; Tetrahedron: Asymmetry; vol. 4; nb. 5; (1993); p. 839 - 844, tion with succinic View in Reaxys anhydride in the presence of lipase Amano PS and subsequent hydrolysis optical purity: 28.1 percent Boiling Point (4) Boiling Point [°C]

Brunner, Henri; Reiter, Barbara; Riepl, Georg; Chemische Berichte; vol. 117; nb. 4; (1984); p. 1330 - 1354, View in Reaxys Pressure (Boiling Point) [Torr]

120

References Conte, V.; Furia, F. Di; Licini, G.; Modena, G.; Sbampato, G.; Valle, G.; Tetrahedron: Asymmetry; vol. 2; nb. 4; (1991); p. 257 - 276, View in Reaxys

116 - 117

Arcus; Hallgarten; Journal of the Chemical Society; (1956); p. 2987,2990, View in Reaxys

114

Levene; Walti; Journal of Biological Chemistry; vol. 90; (1931); p. 81,86, View in Reaxys

108

Phillips; Journal of the Chemical Society; vol. 123; (1923); p. 46,56, View in Reaxys

Refractive Index (2)

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Refractive Index

Wavelength (ReTemperature (Refractive Index) [nm] fractive Index) [°C]

References

1.5182

589

Arcus; Hallgarten; Journal of the Chemical Society; (1956); p. 2987,2990, View in Reaxys

1.5204

589

Arcus; Hallgarten; Journal of the Chemical Society; (1956); p. 2987,2990, View in Reaxys

Location

References

Chromatographic Data (5) Chromatographic Original string data GC (Gas chromatography)

supporting informa- Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei; tion Organic and Biomolecular Chemistry; vol. 10; nb. 14; (2012); p. 2730 2732, View in Reaxys; Villalpando, Andres; Ayala, Caitlan E.; Watson, Christopher B.; Kartika, Rendy; Journal of Organic Chemistry; vol. 78; nb. 8; (2013); p. 3989 - 3996, View in Reaxys; Zhao, Yang; Weix, Daniel J.; Journal of the American Chemical Society; vol. 136; nb. 1; (2014); p. 48 - 51, View in Reaxys; Yang, Yi; Liu, Ji; Li, Zhi; Angewandte Chemie - International Edition; vol. 53; nb. 12; (2014); p. 3120 - 3124; Angew. Chem.; vol. 126; nb. 12; (2014); p. 3348,1, View in Reaxys; Borràs, Carlota; Biosca, Maria; Pàmies, Oscar; Diéguez, Montserrat; Organometallics; vol. 34; nb. 21; (2015); p. 5321 - 5334, View in Reaxys; Veguillas, Marcos; Solà, Ricard; Shaw, Luke; Maciá, Beatriz; European Journal of Organic Chemistry; vol. 2016; nb. 9; (2016); p. 1788 - 1794, View in Reaxys; Veguillas, Marcos; Solà, Ricard; Fernández-Ibañez, M. Ángeles; Maciá, Beatriz; Tetrahedron Asymmetry; vol. 27; nb. 14-15; (2016); p. 643 - 648, View in Reaxys; de Leeuw, Nicolas; Torrelo, Guzman; Bisterfeld, Carolin; Resch, Verena; Mestrom, Luuk; Straulino, Emanuele; van der Weel, Laura; Hanefeld, Ulf; Advanced Synthesis and Catalysis; vol. 360; nb. 2; (2018); p. 242 - 249, View in Reaxys

GC (Gas chromatography)

Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu; Letters in Organic Chemistry; vol. 9; nb. 9; (2012); p. 615 621, View in Reaxys; Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys; Sun, Zhoutong; Li, Guangyue; Ilie, Adriana; Reetz, Manfred T.; Tetrahedron Letters; vol. 57; nb. 32; (2016); p. 3648 - 3651, View in Reaxys; Karume, Ibrahim; Musa, Musa M.; Bsharat, Odey; Takahashi, Masateru; Hamdan, Samir M.; El Ali, Bassam; RSC Advances; vol. 6; nb. 99; (2016); p. 96616 - 96622, View in Reaxys; Bódai, Viktória; Nagy-Győr, László; Örkényi, Róbert; Molnár, Zsófia; Kohári, Szabolcs; Erdélyi, Balázs; Nagymáté, Zsuzsanna; Romsics, Csaba; Paizs, Csaba; Poppe, László; Hornyánszky, Gábor; Journal of Molecular Catalysis B: Enzymatic; vol. 134; (2016); p. 206 - 214, View in Reaxys; Hoang, Hai Nam; Nagashima, Yoshihiro; Mori, Shuichi; Kagechika, Hiroyuki; Matsuda, Tomoko; Tetrahedron; vol. 73; nb. 20; (2017); p. 2984 - 2989, View in Reaxys

HPLC (High performance liquid chromatography)

supporting informa- Pinaka, Afroditi; Dimotikali, Dimitra; Chankvetadze, Bezhan; Papadotion poulos, Kyriakos; Vougioukalakis, Georgios C.; Synlett; vol. 24; nb. 18; (2013); p. 2401 - 2406; Art.No: ST-2013-B0829-L, View in Reaxys; Kleman, Patryk; Gonzalez-Liste, Pedro J.; Garcia-Garrido, Sergio E.; Cadierno, Victorio; Pizzano, Antonio; Chemistry - A European Journal; vol. 19; nb. 48; (2013); p. 16209 - 16212, View in Reaxys; Veguillas, Marcos; Solà, Ricard; Shaw, Luke; Maciá, Beatriz; European Journal of Organic Chemistry; vol. 2016; nb. 9; (2016); p. 1788 - 1794, View in Reaxys; Cozett, Rudy E.; Venter, Gerhard A.; Gokada, Maheswara Rao; Hunter, Roger; Organic and Biomolecular Chemistry; vol. 14; nb. 46; (2016); p. 10914 - 10925, View in Reaxys; Vitale, Paola; Abbinante, Vincenzo Mirco; Perna, Filippo Maria; Salomone, Antonio; Cardellicchio, Cosimo; Capriati, Vito; Advanced Synthesis and Catalysis; vol. 359; nb. 6; (2017); p. 1049 - 1057, View in Reaxys; Benítez-Mateos, Ana I.; San Sebastian, Eneko; Ríos-Lombardía, Nicolás; Morís, Francisco; González-Sabín, Javier; López-Gallego, Fernando; Chemistry - A European Journal; vol. 23; nb. 66; (2017); p. 16843 - 16852, View in Reaxys

TLC (Thin layer chromatography)

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Molecular Catalysis B: Enzymatic; vol. 134; (2016); p. 206 - 214, View in Reaxys GC (Gas chromatography)

retention time [min] Page/Page column 22.5 24

Circular Dichroism (5) Solvent (Circular Comment (Circular Dichroism) Dichroism)

Patent; B.R.A.I.N. AG; Liebeton, Klaus; Eck, Jürgen; Bornscheuer, Uwe; Böttcher, Dominique; Langer, Peter; Bellur, Esen; US9193961; (2015); (B2) English, View in Reaxys

References

H2O

277 - 230 nm

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

cyclohexane

277 - 230 nm

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

methanol

278 - 230 nm

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

tetrahydrofuran

278 - 230 nm

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

dioxane

282 - 245 nm

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

Crystal Property Description (2) Colour & Other Location Properties

References

colourless

Paragraph 0057

yellow

supporting informa- Kleman, Patryk; Gonzalez-Liste, Pedro J.; Garcia-Garrido, Sergio E.; Cadierno, Victorio; tion Pizzano, Antonio; Chemistry - A European Journal; vol. 19; nb. 48; (2013); p. 16209 - 16212, View in Reaxys

Patent; University of Kentucky Research Foundation; DWOSKIN, Linda; CROOKS, Peter Anthony; ZHENG, Guangrong; NICKELL, Justin R.; CAO, Zheng; LEE, Na-Ra; (15 pag.); US2017/304227; (2017); (A1) English, View in Reaxys

Optical Rotatory Power (28) 1 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

4.3 g/100ml

Enantiomeric excess [%ee] 73 Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-23

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Veguillas, Marcos; Solà, Ricard; Shaw, Luke; Maciá, Beatriz; European Journal of Organic Chemistry; vol. 2016; nb. 9; (2016); p. 1788 - 1794, View in Reaxys 2 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

0.7 g/100ml

Enantiomeric excess [%ee] 85 Length of Path [cm]

0.5

Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-35.4

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Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Veguillas, Marcos; Solà, Ricard; Fernández-Ibañez, M. Ángeles; Maciá, Beatriz; Tetrahedron Asymmetry; vol. 27; nb. 14-15; (2016); p. 643 - 648, View in Reaxys 3 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

1.48 g/100ml

Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-38.5

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys 4 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

0.5 g/100ml

Enantiomeric excess [%ee] 99 Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

32.5

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kleman, Patryk; Gonzalez-Liste, Pedro J.; Garcia-Garrido, Sergio E.; Cadierno, Victorio; Pizzano, Antonio; Chemistry A European Journal; vol. 19; nb. 48; (2013); p. 16209 - 16212, View in Reaxys 5 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

0.75 g/100ml

Enantiomeric excess [%ee] 99 Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-35.4

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kataoka, Noriyuki; Okudomi, Masayuki; Chihara, Naoka; Matsumoto, Kazutsugu; Letters in Organic Chemistry; vol. 9; nb. 9; (2012); p. 615 - 621, View in Reaxys 6 of 28

Type (Optical Rotatory Power)

[alpha]

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Concentration (Optical Rotatory Power)

0.9 g/100ml

Enantiomeric excess [%ee] 11 Length of Path [cm]

Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-2.9

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Location

supporting information

Boukachabia, Mourad; Zeror, Saoussen; Collin, Jacqueline; Fiaud, Jean-Claude; Zouioueche, Louisa Aribi; Tetrahedron Letters; vol. 52; nb. 13; (2011); p. 1485 - 1489, View in Reaxys 7 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

0.67 g/100ml

Enantiomeric excess [%ee] 99 Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-32.8

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Okudomi, Masayuki; Ageishi, Kanpei; Yamada, Tomomi; Chihara, Naoka; Nakagawa, Takuya; Mizuochi, Katsumi; Matsumoto, Kazutsugu; Tetrahedron; vol. 66; nb. 40; (2010); p. 8060 - 8067, View in Reaxys 8 of 28

Type (Optical Rotatory Power)

[alpha]

Enantiomeric excess [%ee] 98 Length of Path [cm]

Optical Rotatory Power [deg]

-26.4

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Location

supporting information

Comment (Optical Rotato- neat (no solvent) ry Power) Scholz, Roland; Hellmann, Gunther; Rohs, Susanne; Oezdemir, Diana; Raabe, Gerhard; Vermeeren, Cornelia; Gais, Hans-Joachim; European Journal of Organic Chemistry; nb. 24; (2010); p. 4588 - 4616, View in Reaxys 9 of 28

Type (Optical Rotatory Power)

[alpha]

Enantiomeric excess [%ee] 97 Length of Path [cm]

Optical Rotatory Power [deg]

-26.2

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Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Location

supporting information

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

1.08 g/100ml

Enantiomeric excess [%ee] 50.7 Solvent (Optical Rotatory Power)

chloroform

Optical Rotatory Power [deg]

-20.7

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Ema, Tadashi; Ura, Norichika; Yoshii, Masataka; Korenaga, Toshinobu; Sakai, Takashi; Tetrahedron; vol. 65; nb. 46; (2009); p. 9583 - 9591, View in Reaxys 11 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

1.11 g/100ml

Solvent (Optical Rotatory Power)

CHCl3

Optical Rotatory Power [deg]

-38.7

Wavelength (Optical Rota- 589 tory Power) [nm] Nakamura, Kaoru; Fujii, Mikio; Ida, Yoshiteru; Tetrahedron Asymmetry; vol. 12; nb. 22; (2001); p. 3147 - 3153, View in Reaxys 12 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

5.7 g/100ml

Solvent (Optical Rotatory Power)

benzene

Optical Rotatory Power [deg]

-36

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys 13 of 28

Type (Optical Rotatory Power)

[alpha]

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Concentration (Optical Rotatory Power)

0.01 g/100ml

Solvent (Optical Rotatory Power)

CHCl3

Optical Rotatory Power [deg]

-39

Wavelength (Optical Rota- 578 tory Power) [nm] Besse; Renard; Veschambre; Tetrahedron Asymmetry; vol. 5; nb. 7; (1994); p. 1249 - 1268, View in Reaxys 14 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

3 g/100ml

Solvent (Optical Rotatory Power)

CHCl3

Optical Rotatory Power [deg]

-35.3

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Conte, V.; Furia, F. Di; Licini, G.; Modena, G.; Sbampato, G.; Valle, G.; Tetrahedron: Asymmetry; vol. 2; nb. 4; (1991); p. 257 - 276, View in Reaxys 15 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

1.5 g/100ml

Solvent (Optical Rotatory Power)

CHCl3

Optical Rotatory Power [deg]

-35.5

Wavelength (Optical Rota- 589 tory Power) [nm] DeNinno; Perner; Lijewski; Tetrahedron Letters; vol. 31; nb. 51; (1990); p. 7415 - 7418, View in Reaxys 16 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-31.6

Wavelength (Optical Rota- 546.1 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Arcus; Hallgarten; Journal of the Chemical Society; (1956); p. 2987,2990, View in Reaxys 17 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

Solvent (Optical Rotatory Power)

neat (no solvent)

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Optical Rotatory Power [deg]

-26.2

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Arcus; Hallgarten; Journal of the Chemical Society; (1956); p. 2987,2990, View in Reaxys 18 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

2.5

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-6.8

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 19 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

2.5

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-8.1

Wavelength (Optical Rota- 546.1 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 20 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

2.5

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-15.3

Wavelength (Optical Rota- 435.8 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 21 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-13.9

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Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 22 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

c=5

Solvent (Optical Rotatory Power)

ethanol

Optical Rotatory Power [deg]

-19.4

Wavelength (Optical Rota- 546.1 tory Power) [nm] Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 23 of 28

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

-20.2

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 24 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

c=5

Solvent (Optical Rotatory Power)

diethyl ether

Optical Rotatory Power [deg]

-45.6

Wavelength (Optical Rota- 435.9 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys 25 of 28

Type (Optical Rotatory Power)

[alpha]

Concentration (Optical Rotatory Power)

c=5

Solvent (Optical Rotatory Power)

diethyl ether

Optical Rotatory Power [deg]

-27.7

Wavelength (Optical Rota- 589 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Kenyon; Phillips; Pittman; Journal of the Chemical Society; (1935); p. 1079, View in Reaxys

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26 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-32.18

Wavelength (Optical Rota- 546.1 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Phillips; Journal of the Chemical Society; vol. 123; (1923); p. 27,29, 31, View in Reaxys 27 of 28

Type (Optical Rotatory Power)

alpha

Length of Path [cm]

Solvent (Optical Rotatory Power)

neat (no solvent)

Optical Rotatory Power [deg]

-30.9

Wavelength (Optical Rota- 546.1 tory Power) [nm] Temperature (Optical Rotatory Power) [°C]

Phillips; Journal of the Chemical Society; vol. 123; (1923); p. 27,29, 31, View in Reaxys 28 of 28

Type (Optical Rotatory Power)

[alpha]

Optical Rotatory Power [deg]

-26.6

Wavelength (Optical Rota- 589 tory Power) [nm] Pickard; Kenyon; Proceedings of the Chemical Society, London; vol. 28; (1913); p. 42, View in Reaxys NMR Spectroscopy (19) 1 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 500 scopy) [MHz] Musa, Musa M.; Bsharat, Odey; Karume, Ibrahim; Vieille, Claire; Takahashi, Masateru; Hamdan, Samir M.; European Journal of Organic Chemistry; vol. 2018; nb. 6; (2018); p. 798 - 805, View in Reaxys 2 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 125 scopy) [MHz] Musa, Musa M.; Bsharat, Odey; Karume, Ibrahim; Vieille, Claire; Takahashi, Masateru; Hamdan, Samir M.; European Journal of Organic Chemistry; vol. 2018; nb. 6; (2018); p. 798 - 805, View in Reaxys

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3 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 400 scopy) [MHz] Location

supporting information

Yi, Jun; Liu, Jin-Hui; Liang, Jun; Dai, Jian-Jun; Yang, Chu-Ting; Fu, Yao; Liu, Lei; Advanced Synthesis and Catalysis; vol. 354; nb. 9; (2012); p. 1685 - 1691, View in Reaxys; Vitale, Paola; Abbinante, Vincenzo Mirco; Perna, Filippo Maria; Salomone, Antonio; Cardellicchio, Cosimo; Capriati, Vito; Advanced Synthesis and Catalysis; vol. 359; nb. 6; (2017); p. 1049 - 1057, View in Reaxys 4 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 100 scopy) [MHz] Location

supporting information

Vitale, Paola; Abbinante, Vincenzo Mirco; Perna, Filippo Maria; Salomone, Antonio; Cardellicchio, Cosimo; Capriati, Vito; Advanced Synthesis and Catalysis; vol. 359; nb. 6; (2017); p. 1049 - 1057, View in Reaxys 5 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 300 scopy) [MHz] Fernandez-Mateos, Emilio; MacIa, Beatriz; Yus, Miguel; Tetrahedron Asymmetry; vol. 23; nb. 10; (2012); p. 789 - 794, View in Reaxys; Bódai, Viktória; Nagy-Győr, László; Örkényi, Róbert; Molnár, Zsófia; Kohári, Szabolcs; Erdélyi, Balázs; Nagymáté, Zsuzsanna; Romsics, Csaba; Paizs, Csaba; Poppe, László; Hornyánszky, Gábor; Journal of Molecular Catalysis B: Enzymatic; vol. 134; (2016); p. 206 - 214, View in Reaxys 6 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 75 scopy) [MHz] Fernandez-Mateos, Emilio; MacIa, Beatriz; Yus, Miguel; Tetrahedron Asymmetry; vol. 23; nb. 10; (2012); p. 789 - 794, View in Reaxys; Bódai, Viktória; Nagy-Győr, László; Örkényi, Róbert; Molnár, Zsófia; Kohári, Szabolcs; Erdélyi, Balázs; Nagymáté, Zsuzsanna; Romsics, Csaba; Paizs, Csaba; Poppe, László; Hornyánszky, Gábor; Journal of Molecular Catalysis B: Enzymatic; vol. 134; (2016); p. 206 - 214, View in Reaxys 7 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

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Location

supporting information

Borràs, Carlota; Biosca, Maria; Pàmies, Oscar; Diéguez, Montserrat; Organometallics; vol. 34; nb. 21; (2015); p. 5321 5334, View in Reaxys 8 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Temperature (NMR Spectroscopy) [°C]

Frequency (NMR Spectro- 300 scopy) [MHz] Location

supporting information

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys 9 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Temperature (NMR Spectroscopy) [°C]

Frequency (NMR Spectro- 75 scopy) [MHz] Location

supporting information

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys 10 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 300 scopy) [MHz] Location

supporting information

Fernandez-Mateos, Emilio; MacIa, Beatriz; Ramon, Diego J.; Yus, Miguel; European Journal of Organic Chemistry; nb. 34; (2011); p. 6851 - 6855, View in Reaxys; Fernandez-Mateos, Emilio; MacIa, Beatriz; Yus, Miguel; European Journal of Organic Chemistry; nb. 20; (2012); p. 3732 - 3736, View in Reaxys 11 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 75 scopy) [MHz] Location

supporting information

15/18

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Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 101 scopy) [MHz] Location

supporting information

Yi, Jun; Liu, Jin-Hui; Liang, Jun; Dai, Jian-Jun; Yang, Chu-Ting; Fu, Yao; Liu, Lei; Advanced Synthesis and Catalysis; vol. 354; nb. 9; (2012); p. 1685 - 1691, View in Reaxys 13 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 400 scopy) [MHz] Location

supporting information

Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei; Organic and Biomolecular Chemistry; vol. 10; nb. 14; (2012); p. 2730 - 2732, View in Reaxys 14 of 19

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 75 scopy) [MHz] Location

supporting information

Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei; Organic and Biomolecular Chemistry; vol. 10; nb. 14; (2012); p. 2730 - 2732, View in Reaxys 15 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Frequency (NMR Spectro- 500 scopy) [MHz] Ema, Tadashi; Ura, Norichika; Yoshii, Masataka; Korenaga, Toshinobu; Sakai, Takashi; Tetrahedron; vol. 65; nb. 46; (2009); p. 9583 - 9591, View in Reaxys 16 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Frequency (NMR Spectro- 150 scopy) [MHz]

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Ema, Tadashi; Ura, Norichika; Yoshii, Masataka; Korenaga, Toshinobu; Sakai, Takashi; Tetrahedron; vol. 65; nb. 46; (2009); p. 9583 - 9591, View in Reaxys 17 of 19

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Conte, V.; Furia, F. Di; Licini, G.; Modena, G.; Sbampato, G.; Valle, G.; Tetrahedron: Asymmetry; vol. 2; nb. 4; (1991); p. 257 - 276, View in Reaxys; Shi, Xiao-Xin; Yao, Jian-Zhong; Kang, Li; Shen, Chun-Li; Yi, Fei; Journal of Chemical Research; nb. 10; (2004); p. 681 - 683, View in Reaxys; Nakamura, Yukie; Egami, Hiromichi; Matsumoto, Kazuhiro; Uchida, Tatsuya; Katsuki, Tsutomu; Tetrahedron; vol. 63; nb. 28; (2007); p. 6383 - 6387, View in Reaxys 18 of 19

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Solvents (NMR Spectroscopy)

CDCl3

Shi, Xiao-Xin; Yao, Jian-Zhong; Kang, Li; Shen, Chun-Li; Yi, Fei; Journal of Chemical Research; nb. 10; (2004); p. 681 683, View in Reaxys 19 of 19

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CDCl3

Comment (NMR Spectroscopy)

1H-1H

Conte, V.; Furia, F. Di; Licini, G.; Modena, G.; Sbampato, G.; Valle, G.; Tetrahedron: Asymmetry; vol. 2; nb. 4; (1991); p. 257 - 276, View in Reaxys IR Spectroscopy (4) 1 of 4

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

film

Description (IR Spectroscopy)

Intensity of IR bands; Bands

Solvent (IR Spectroscopy)

neat liquid

Comment (IR Spectroscopy)

film

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys 3 of 4

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

neat (no solvent)

Ema, Tadashi; Ura, Norichika; Yoshii, Masataka; Korenaga, Toshinobu; Sakai, Takashi; Tetrahedron; vol. 65; nb. 46; (2009); p. 9583 - 9591, View in Reaxys 4 of 4

Description (IR Spectroscopy)

Bands

Solvent (IR Spectroscopy)

neat liquid

Shi, Xiao-Xin; Yao, Jian-Zhong; Kang, Li; Shen, Chun-Li; Yi, Fei; Journal of Chemical Research; nb. 10; (2004); p. 681 683, View in Reaxys

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Mass Spectrometry (5) Description (Mass Location Spectrometry)

References

gas chromatography mass spectrometry (GCMS); electron impact (EI); spectrum

Taguri, Tomonori; Yamamoto, Masanobu; Fujii, Toru; Muraki, Yuta; Ando, Tetsu; European Journal of Organic Chemistry; nb. 30; (2013); p. 6924 - 6933, View in Reaxys

EI (Electron impact); Spectrum

Fernandez-Mateos, Emilio; MacIa, Beatriz; Yus, Miguel; Tetrahedron Asymmetry; vol. 23; nb. 10; (2012); p. 789 - 794, View in Reaxys

EI (Electron impact); GCMS (Gas chromatography mass spectrometry); Spectrum

supporting informa- Fernandez-Mateos, Emilio; MacIa, Beatriz; Yus, Miguel; European Journal of Organic Chemtion istry; nb. 20; (2012); p. 3732 - 3736, View in Reaxys

electron impact (EI); spectrum

supporting informa- Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei; Organic and Biomotion lecular Chemistry; vol. 10; nb. 14; (2012); p. 2730 - 2732, View in Reaxys

EI (Electron impact); Spectrum

supporting informa- Fernandez-Mateos, Emilio; MacIa, Beatriz; Ramon, Diego J.; Yus, Miguel; European Journal tion of Organic Chemistry; nb. 34; (2011); p. 6851 - 6855, View in Reaxys

UV/VIS Spectroscopy (2) 1 of 2

Description (UV/VIS Spectroscopy)

Absorption maxima

Solvent (UV/VIS Spectroscopy)

methanol

Absorption Maxima (UV/ VIS) [nm]

247

Ext./Abs. Coefficient [l·mol-1cm-1]

110

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys 2 of 2

Description (UV/VIS Spectroscopy)

Absorption maxima

Solvent (UV/VIS Spectroscopy)

methanol

Absorption Maxima (UV/ VIS) [nm]

267; 264; 258; 252

Ext./Abs. Coefficient [l·mol-1cm-1]

120; 120; 190; 160

Smith, Howard E.; Neergaard, Jon R.; Journal of the American Chemical Society; vol. 118; nb. 33; (1996); p. 7694 - 7701, View in Reaxys

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