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Reactions (13)
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Substances (13)
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Citations (10)
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1 Synthesize
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Rx-ID: 436912
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With ethanol; with phosphoric acid impregnated pumice stone
T=220 - 225°C; P=100 - 125 Torr;
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
With ethanol; phosphoric acid; silica gel
T=220 - 225°C; P=100 - 125 Torr;
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
With sulfuric acid
Zincke
Justus Liebigs Annalen der Chemie, 1883 , vol. 216, p. 303 Justus Liebigs Annalen der Chemie, 1887 , vol. 240, p. 137 Full Text Show Details
Hide Details 98 % Chromat.
With H-ZS-5 zeolite
T=250°C; vaporised substrate diluted with steam, time of stream 6 h, WHSV 30 h-1;
Paparatto, G.; Gregorio, G.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1471 - 1472
Title/Abstract Full Text View citing articles Show Details
98 % Chromat.
With H-ZSM-5 zeolite
T=250°C; vaporized substrate diluted with steam; Silicalite, silica-alumina, and alumina catalysts, different temperature, time of stream and WHSV; Product distribution;
Paparatto, G.; Gregorio, G.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1471 - 1472
Title/Abstract Full Text View citing articles Show Details
96 % Chromat.
With silica gel
T=250°C; vaporized substrate diluted with steam; other silica gel catalysts, various pH, temperature, time of stream and WHSV; Product distribution;
Paparatto, G.; Gregorio, G.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1471 - 1472
Title/Abstract Full Text View citing articles Show Details
97 %Chromat.
With sulfuric acid in water
T=170°C; P=15001.5 Torr; 0.5 h; Microwave irradiationGreen chemistry; Catalytic behavior; Reagent/catalystSolventTime; Hide Experimental Procedure
Le Guenic, Sarah; Ceballos, Claire; Len, Christophe
Journal of Molecular Catalysis A: Chemical, 2016 , vol. 411, p. 72 - 77
Title/Abstract Full Text View citing articles Show Details
General procedure for the synthesis of phenylacetaldehyde in water-CPME as biphasic media from 1-phenylethan-1,2-diol
General procedure: General procedure for the synthesis of phenylacetaldehyde in water-CPME as biphasic media from 1-phenylethan-1,2-diol In a typical experiment, a 10 mL glass vessel was charged with water (0.5 mL), CPME (1.4 mL), 1-phenylethan-1,2-diol (1, 100 mg, 0.725 mmol) and a catalyst (20 molpercent). The vessel was sealed with a septum, placed in the microwave apparatus (AntonPaar Monowave 300) and heated to the desired temperature under magnetic stirring (600 rpm) for the desired time. Temperature in the vessel was measured by means of an IR sensor. At the end of the reaction, the vessel was cooled down to 40 °C using compressed air. Then, the reaction mixture was diluted in 100 mL of acetonitrile. An aliquot of the diluted solution was taken (ca. 1.5 mL) and filtered prior to analysis through a syringe filter (PTFE, 0.45 μm, VWR). A
B
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2 Synthesize
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Rx-ID: 30814227
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A: 85% B: 10%
With [Et3NH]+HSO4-
T=80°C; P=12751.3 Torr; 0.0833333 h; Microwave irradiation;
Henderson, Luke C.; Byrne, Nolene
Green Chemistry, 2011 , vol. 13, # 4 p. 813 - 816
Title/Abstract Full Text View citing articles Show Details
A: 25% B: 70%
With sulfuric acid in water; ethyl acetate
T=170°C; P=15001.5 Torr; 0.5 h; Microwave irradiation; Catalytic behavior; Reagent/catalystSolvent; Hide Experimental Procedure
Le Guenic, Sarah; Ceballos, Claire; Len, Christophe
Journal of Molecular Catalysis A: Chemical, 2016 , vol. 411, p. 72 - 77
Title/Abstract Full Text View citing articles Show Details
General procedure for the synthesis of phenylacetaldehyde in water-CPME as biphasic media from 1-phenylethan-1,2-diol
General procedure: General procedure for the synthesis of phenylacetaldehyde in water-CPME as biphasic media from 1-phenylethan-1,2-diol In a typical experiment, a 10 mL glass vessel was charged with water (0.5 mL), CPME (1.4 mL), 1-phenylethan-1,2-diol (1, 100 mg, 0.725 mmol) and a catalyst (20 molpercent). The vessel was sealed with a septum, placed in the microwave apparatus (AntonPaar Monowave 300) and heated to the desired temperature under magnetic stirring (600 rpm) for the desired time. Temperature in the vessel was measured by means of an IR sensor. At the end of the reaction, the vessel was cooled down to 40 °C using compressed air. Then, the reaction mixture was diluted in 100 mL of acetonitrile. An aliquot of the diluted solution was taken (ca. 1.5 mL) and filtered prior to analysis through a syringe filter (PTFE, 0.45 μm, VWR). A
B
C
D
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3 Synthesize
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A: 39 %Chromat.
With hydrogen in benzene
T=150°C; P=10501.1 Torr; 24 h; Autoclave;
Denning, Alana L.; Dang, Huong; Liu, Zhimin; Nicholas, Kenneth M.; Jentoft, Friederike C.
ChemCatChem, 2013 , vol. 5, # 12 p. 3567 - 3570
Title/Abstract Full Text View citing articles Show Details
A
B
C
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4 Synthesize
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Multi-step reaction with 2 steps 1: thionyl chloride; triethylamine / diethyl ether / 4 h 2: acetonitrile / 3 h / Photolysis
View Scheme
Rx-ID: 33845790
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White, Rick C.; Arney Jr., Benny E.; Ihmels, Heiko
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 1208 - 1212 Title/Abstract Full Text View citing articles Show Details
A
B
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5 Synthesize
Find similar A: 21 %Chromat.
Rx-ID: 33905502
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With water; sodium chloride
T=180°C; 16 h; Autoclave; chemoselective reaction;
Avola, Sabine; Goettmann, Frederic; Antonietti, Markus; Kunz, Werner
New Journal of Chemistry, 2012 , vol. 36, # 8 p. 1568 1573
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With water
T=200°C; 16 h; Autoclave; chemoselective reaction;
Avola, Sabine; Goettmann, Frederic; Antonietti, Markus; Kunz, Werner
New Journal of Chemistry, 2012 , vol. 36, # 8 p. 1568 1573
Title/Abstract Full Text View citing articles Show Details
B: 22 %Chromat.
A: 84 %Chromat. B: 16 %Chromat.
A
B
C
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6 Synthesize
Find similar A: 4.9 % Chromat. B: 59 % Chromat. C: 9.4 % Chromat.
With diazomethane; sulfuric acid in benzene
T=25°C; 0.5 h;
Rx-ID: 4152516
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Takeuchi, Hiroshi; Kishioka, Hiroaki; Kitajima, Kunio
Journal of Physical Organic Chemistry, 1995 , vol. 8, # 2 p. 121 - 126 Title/Abstract Full Text Show Details
7 Synthesize
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Rx-ID: 8236409
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=550 - 600°C; P=125 - 165 Torr;
Full Text Show Details
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=200 - 225°C; P=105 - 125 Torr;
Full Text Show Details
8 Synthesize
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Rx-ID: 8236412
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=200 - 225°C; P=105 - 125 Torr;
Full Text Show Details
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=550 - 600°C; P=125 - 165 Torr;
Full Text Show Details
9 Synthesize
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T=200 - 225°C; P=105 - 125 Torr;
Rx-ID: 8236413
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ; Full Text Show Details
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=550 - 600°C; P=125 - 165 Torr;
Full Text Show Details
10 Synthesize
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Rx-ID: 8236414
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=200 - 225°C; P=105 - 125 Torr;
Full Text Show Details
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=550 - 600°C; P=125 - 165 Torr;
Full Text Show Details
11 Synthesize
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T=550 - 600°C; P=125 - 165 Torr;
Rx-ID: 8236415
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ; Full Text Show Details
T=200 - 225°C; P=105 - 125 Torr;
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ; Full Text Show Details
12 Synthesize
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Rx-ID: 8236416
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Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=200 - 225°C; P=105 - 125 Torr;
Full Text Show Details
Emerson; Agnew
Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520 Full Text Show Details
Monsanto Chem. Co.
Patent: US2444400 , 1943 ;
T=550 - 600°C; P=125 - 165 Torr;
Full Text Show Details
13 Synthesize
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Rx-ID: 6680228
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Zincke
Justus Liebigs Annalen der Chemie, 1883 , vol. 216, p. 303 Justus Liebigs Annalen der Chemie, 1887 , vol. 240, p. 137 Full Text Show Details
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13 reactions out of 13 substances and 10 citations
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