Dichlorodeuteriomethyl methyl ether [dichloro(methoxy)methane-d]

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Query 1. Query

Query

Results

Date

IDE.XRN=1847462

3 reactions in Reaxys

2016-06-02 17h:08m:08s (EST)

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2016-06-02 17:08:59


O O 2H

Cl

O

Cl

O O

2

H

O

Rx-ID: 1976836 View in Reaxys 1/3 Yield

Conditions & References

78 %

With tin(IV) chloride in dichloromethane, a) 0 deg C, 1 h, b) 0 deg C, 30 min, c) to room temperature Meier, Herbert; Kretzschmann, Holger; Kolshorn, Heinz; Journal of Organic Chemistry; vol. 57; nb. 25; (1992); p. 6847 - 6852 View in Reaxys 2H

Cl

O

Cl

Rx-ID: 7015018 View in Reaxys 2/3 Yield

Conditions & References Deuteroameisensaeure-methylester, PCl5 <8h, 20grad; 5h, kochen> Hine et al.; Journal of the American Chemical Society; vol. 82; (1960); p. 6120,6123 View in Reaxys

2H

Cl

O

Cl

Rx-ID: 6770814 View in Reaxys 3/3 Yield

Conditions & References Kinetics, Rk. mit K-isopropylat und K-thiophenoxyd bei -11.5 u.+ 0.8grad in Isopropylalkohol Hine et al.; Journal of the American Chemical Society; vol. 82; (1960); p. 6120,6123 View in Reaxys

Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.

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