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Date
7 reactions in Reaxys
2016-06-11 20h:02m:02s (EST)
I
1. Query NH
Search as: As drawn
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NH
NH
OH
I
Rx-ID: 10494644 View in Reaxys 1/7 Yield
Conditions & References
75 %
With 1H-imidazole, iodine, triphenylphosphine in benzene, Time= 1h, T= 20 °C Menozzi, Candice; Dalko, Peter I.; Cossy, Janine; Chemical Communications; nb. 44; (2006); p. 4638 - 4640 View in Reaxys
60 %
With 1H-imidazole, iodine, triphenylphosphine, Reflux Yang, Yi; Jiang, Xueliang; Qing, Feng-Ling; Journal of Organic Chemistry; vol. 77; nb. 17; (2012); p. 7538 - 7547 View in Reaxys With 1H-imidazole, iodine, triphenylphosphine in dichloromethane, T= 0 - 20 °C , Inert atmosphere Lombardo, Vince M.; Thomas, Christopher D.; Scheidt, Karl A.; Angewandte Chemie - International Edition; vol. 52; nb. 49; (2013); p. 12910 - 12914; Angew. Chem.; vol. 125; nb. 49; (2013); p. 13148 - 13152,5 View in Reaxys
NH
NH
O
I
Rx-ID: 38375731 View in Reaxys 2/7 Yield
Conditions & References With 1H-imidazole, iodine, triphenylphosphine in dichloromethane, T= 0 - 20 °C , Inert atmosphere Gao, Run-Duo; Liu, Chuan; Dai, Li-Xin; Zhang, Wei; You, Shu-Li; Organic Letters; vol. 16; nb. 15; (2014); p. 3919 - 3921 View in Reaxys
NH
NH O
O
O
I
Rx-ID: 11818259 View in Reaxys 3/7 Yield
Conditions & References Reaction Steps: 2 1: 100 percent / LiAlH4 / tetrahydrofuran / 12 h / 20 °C 2: 75 percent / I2; imidazole; PPh3 / benzene / 1 h / 20 °C With 1H-imidazole, lithium aluminium tetrahydride, iodine, triphenylphosphine in tetrahydrofuran, benzene Menozzi, Candice; Dalko, Peter I.; Cossy, Janine; Chemical Communications; nb. 44; (2006); p. 4638 - 4640 View in Reaxys Reaction Steps: 2 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 80 °C / |Inert atmosphere 2: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / |Inert atmosphere With 1H-imidazole, lithium aluminium tetrahydride, iodine, triphenylphosphine in tetrahydrofuran, dichloromethane Gao, Run-Duo; Liu, Chuan; Dai, Li-Xin; Zhang, Wei; You, Shu-Li; Organic Letters; vol. 16; nb. 15; (2014); p. 3919 - 3921 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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NH
NH
fluorobenzene*Cr(CO)3 complex I
Rx-ID: 11815579 View in Reaxys 4/7 Yield
Conditions & References Reaction Steps: 4 1: diethyl ether 2: diethyl ether / 12 h / 20 °C 3: 100 percent / LiAlH4 / tetrahydrofuran / 12 h / 20 °C 4: 75 percent / I2; imidazole; PPh3 / benzene / 1 h / 20 °C With 1H-imidazole, lithium aluminium tetrahydride, iodine, triphenylphosphine in tetrahydrofuran, diethyl ether, benzene, 1: Friedel-Crafts acylation Menozzi, Candice; Dalko, Peter I.; Cossy, Janine; Chemical Communications; nb. 44; (2006); p. 4638 - 4640 View in Reaxys
NH
NH
O O
Cl
I
Rx-ID: 11817538 View in Reaxys 5/7 Yield
Conditions & References Reaction Steps: 3 1: diethyl ether / 12 h / 20 °C 2: 100 percent / LiAlH4 / tetrahydrofuran / 12 h / 20 °C 3: 75 percent / I2; imidazole; PPh3 / benzene / 1 h / 20 °C With 1H-imidazole, lithium aluminium tetrahydride, iodine, triphenylphosphine in tetrahydrofuran, diethyl ether, benzene Menozzi, Candice; Dalko, Peter I.; Cossy, Janine; Chemical Communications; nb. 44; (2006); p. 4638 - 4640 View in Reaxys
NH
NH
I
Rx-ID: 38375692 View in Reaxys 6/7 Yield
Conditions & References Reaction Steps: 3 1.1: diethyl ether / 0 - 20 °C / |Inert atmosphere 1.2: 0 - 20 °C / |Inert atmosphere 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 80 °C / |Inert atmosphere 3.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / |Inert atmosphere With 1H-imidazole, lithium aluminium tetrahydride, iodine, triphenylphosphine in tetrahydrofuran, diethyl ether, dichloromethane Gao, Run-Duo; Liu, Chuan; Dai, Li-Xin; Zhang, Wei; You, Shu-Li; Organic Letters; vol. 16; nb. 15; (2014); p. 3919 - 3921 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
3/4
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NH
2-(3-indolyl)ethylbis(dimethylglyoximato)pyridinecobalt(III) I
Rx-ID: 8420164 View in Reaxys 7/7 Yield
Conditions & References With toluene-4-sulfonyl iodide in dichloromethane, 40 deg C, 20-30 s then allowed to stand for 10-30 min Ashcroft, Martyn R.; Bougeard, Peter; Bury, Adrian; Cooksey, Christopher J.; Johnson, Michael D.; Journal of Organometallic Chemistry; vol. 289; (1985); p. 403 - 416 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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