Query 1. Query
Query
Results
Date
IDE.XRN=2958662
12 reactions in Reaxys
2016-06-02 17h:00m:52s (EST)
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O
O
O
Cl
O
O
O
Cl
O
O
O
O
O
O
Rx-ID: 1745828 View in Reaxys 1/12 Yield
Conditions & References
49 %
With titanium tetrachloride in dichloromethane, Time= 3h, T= 20 °C , Title compound not separated from byproducts Daukshas, V.K.; Udrenaite, E.B.; Kuleshyus, V.A.; Chemistry of Heterocyclic Compounds (New York, NY, United States); vol. 18; nb. 12; (1982); p. 1243 - 1246; Khimiya Geterotsiklicheskikh Soedinenii; vol. 18; nb. 12; (1982); p. 1614 - 1617 View in Reaxys
49 %
With titanium tetrachloride in dichloromethane, Time= 3h, T= 20 °C Daukshas, V.K.; Udrenaite, E.B.; Kuleshyus, V.A.; Chemistry of Heterocyclic Compounds (New York, NY, United States); vol. 18; nb. 12; (1982); p. 1243 - 1246; Khimiya Geterotsiklicheskikh Soedinenii; vol. 18; nb. 12; (1982); p. 1614 - 1617 View in Reaxys
O
O
Cl
O Cl
Rx-ID: 1930231 View in Reaxys 2/12 Yield
Conditions & References
95 %
With phosphorus pentachloride, Time= 0.5h, T= 60 - 80 °C Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys O O
Cl
O
O Cl
O
O
O
O
Rx-ID: 2184963 View in Reaxys 3/12 Yield 43 %
Conditions & References With titanium tetrachloride in dichloromethane, Time= 3h, T= 20 °C Daukshas, V.K.; Udrenaite, E.B.; Kuleshyus, V.A.; Chemistry of Heterocyclic Compounds (New York, NY, United States); vol. 18; nb. 12; (1982); p. 1243 - 1246; Khimiya Geterotsiklicheskikh Soedinenii; vol. 18; nb. 12; (1982); p. 1614 - 1617 View in Reaxys HO
Cl
N
O Cl
Rx-ID: 2033404 View in Reaxys 4/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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HO
Cl
N
O Cl
Rx-ID: 2036096 View in Reaxys 5/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
HO
Cl
N
O Cl
Rx-ID: 2067329 View in Reaxys 6/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys HO
Cl
N
O Cl
Rx-ID: 2084747 View in Reaxys 7/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys HO
Cl
N
O Cl
Rx-ID: 2086533 View in Reaxys 8/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
Cl
O Cl HO
N
Rx-ID: 2152990 View in Reaxys 9/12
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Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
Cl
HO
O
N
Cl
Rx-ID: 2184961 View in Reaxys 10/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
Cl
O Cl HO
N
Rx-ID: 2184962 View in Reaxys 11/12 Yield
Conditions & References With pyridine, hydroxylamine hydrochloride, titanium tetrachloride, 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h, Yield given. Multistep reaction Ruolene, Yu. I.; Adomenas, P. V.; Sirutkaitis, R. A.; Denis, G. I.; Journal of Organic Chemistry USSR (English Translation); vol. 20; (1984); p. 1187 - 1191; Zhurnal Organicheskoi Khimii; vol. 20; nb. 6; (1984); p. 1305 - 1310 View in Reaxys
Cl
O Cl
Rx-ID: 7533083 View in Reaxys 12/12 Yield
Conditions & References Rk. mit Aziridin (NaOH in Ether) -> Bis-aziridino-(3-methyl-butoxy)-methan Funke; Justus Liebigs Annalen der Chemie; vol. 725; (1969); p. 15 View in Reaxys
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