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6 reactions in Reaxys
2016-06-01 21h:06m:33s (EST)
N
1. Query
O
NH
Search as: As drawn
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NH
NH O
O
O
N
HN
Rx-ID: 1823016 View in Reaxys 1/6 Yield
Conditions & References With hydrogen, palladium on activated charcoal in ethanol, Time= 15h, p= 2585.7Torr , Yield given Repke, David B.; Grotjahn, Douglas B.; Shulgin, Alexander T.; Journal of Medicinal Chemistry; vol. 28; nb. 7; (1985); p. 892 - 896 View in Reaxys
NH
NH
O
O N
Rx-ID: 19395975 View in Reaxys 2/6 Yield
Conditions & References Reaction Steps: 5 1: 85 percent / tert-butylcatechol / xylene / 3 h / Heating 2: H2 / 10 percent Pd/C / ethanol / 12 h / 2585.7 Torr 3: K2CO3 / H2O; toluene / 15 h / Ambient temperature 4: lithium aluminum hydride / tetrahydrofuran / 0.5 h / Heating 5: H2 / 10 percent Pd/C / ethanol / 15 h / 2585.7 Torr With lithium aluminium tetrahydride, tert-butyl-pyrocatechol, hydrogen, potassium carbonate, palladium on activated charcoal in tetrahydrofuran, ethanol, water, toluene, xylene Repke, David B.; Grotjahn, Douglas B.; Shulgin, Alexander T.; Journal of Medicinal Chemistry; vol. 28; nb. 7; (1985); p. 892 - 896 View in Reaxys
NH NH
O
O
NH 2
N
Rx-ID: 19397559 View in Reaxys 3/6 Yield
Conditions & References Reaction Steps: 3 1: K2CO3 / H2O; toluene / 15 h / Ambient temperature 2: lithium aluminum hydride / tetrahydrofuran / 0.5 h / Heating 3: H2 / 10 percent Pd/C / ethanol / 15 h / 2585.7 Torr With lithium aluminium tetrahydride, hydrogen, potassium carbonate, palladium on activated charcoal in tetrahydrofuran, ethanol, water, toluene Repke, David B.; Grotjahn, Douglas B.; Shulgin, Alexander T.; Journal of Medicinal Chemistry; vol. 28; nb. 7; (1985); p. 892 - 896 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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NH
NH
O
O
N O
N
O
Rx-ID: 19397702 View in Reaxys 4/6 Yield
Conditions & References Reaction Steps: 4 1: H2 / 10 percent Pd/C / ethanol / 12 h / 2585.7 Torr 2: K2CO3 / H2O; toluene / 15 h / Ambient temperature 3: lithium aluminum hydride / tetrahydrofuran / 0.5 h / Heating 4: H2 / 10 percent Pd/C / ethanol / 15 h / 2585.7 Torr With lithium aluminium tetrahydride, hydrogen, potassium carbonate, palladium on activated charcoal in tetrahydrofuran, ethanol, water, toluene Repke, David B.; Grotjahn, Douglas B.; Shulgin, Alexander T.; Journal of Medicinal Chemistry; vol. 28; nb. 7; (1985); p. 892 - 896 View in Reaxys
NH NH
O O
HN
O
O
N
Rx-ID: 19426049 View in Reaxys 5/6 Yield
Conditions & References Reaction Steps: 2 1: lithium aluminum hydride / tetrahydrofuran / 0.5 h / Heating 2: H2 / 10 percent Pd/C / ethanol / 15 h / 2585.7 Torr With lithium aluminium tetrahydride, hydrogen, palladium on activated charcoal in tetrahydrofuran, ethanol Repke, David B.; Grotjahn, Douglas B.; Shulgin, Alexander T.; Journal of Medicinal Chemistry; vol. 28; nb. 7; (1985); p. 892 - 896 View in Reaxys
O O
N O
NH
2H
2H
O
N 2
H
2H
NH
Rx-ID: 28198057 View in Reaxys 6/6 Yield 76 %
Conditions & References With lithium aluminium deuteride in tetrahydrofuran, Inert atmosphere, Microwave irradiation Brandt, Simon D.; Tirunarayanapuram, Sri Subha; Freeman, Sally; Dempster, Nicola; Barker, Steven A.; Daley, Paul F.; Cozzi, Nicholas V.; Martins, Claudia P. B.; Journal of Labelled Compounds and Radiopharmaceuticals; vol. 51; nb. 14; (2008); p. 423 - 429 View in Reaxys
Copyright © 2016 Reed Elsevier Properties SA. All rights reserved. Authorized use only. Reaxys® and the Reaxys® trademark are owned and protected by Reed Elsevier Properties SA and used under license.
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