Reaxys
PubChem
eMolecules
Reactions (55)
Yield
Substances (11)
Citations (45)
Conditions
References
1
Synthesize Find similar With ammonia; hydrogen; nickel
T=135°C;
2
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Rx-ID: 130700 Find similar reactions
I.G.Farbenind. Patent: DE527619 , 1929 ; Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 435 Full Text Show Details
Synthesize Find similar With D-(+)-O,O'-dibenzoyltartaric acid
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Rx-ID: 195597 Find similar reactions
Karrer; Dinkel
Helvetica Chimica Acta, 1953 , vol. 36, p. 122,126 Full Text Show Details
Johnson,R.A. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 4872 - 4880 Full Text View citing articles Show Details
Mazur,R.H.
Journal of Organic Chemistry, 1970 , vol. 35, p. 2050 - 2051 Full Text View citing articles Show Details
3
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Rx-ID: 225902 Find similar reactions
With methanol; nickel
T=85°C; Hydrogenation;
Smith; Adkins
Journal of the American Chemical Society, 1938 , vol. 60, p. 660 Full Text Show Details
With lithium aluminium tetrahydride
Ando,N. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 2369 - 2371 Full Text View citing articles Show Details
With lithium aluminium tetrahydride in tetrahydrofuran
Tzikas; Tamm; Boller; Fuerst
Helvetica chimica acta, 1976 , vol. 59, # 5 p. 1850 - 1850 Title/Abstract Full Text View citing articles Show Details
Hide Details
4
With ethanol; sodium; toluene
Chiang
J. Chin. chem. Soc., 1951 , vol. 18, p. 65,71, 77 Full Text Show Details
With lithium aluminium tetrahydride; diethyl ether
Karrer; Dinkel
Helvetica Chimica Acta, 1953 , vol. 36, p. 122,126 Full Text Show Details
Synthesize Find similar 92%
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Rx-ID: 701691 Find similar reactions
With ammonium formate; palladium on activated charcoal in methanol; water
T=20°C;
Allegretti, Marcello; Berdini, Valerio; Cesta; Curti, Roberto; Nicolini, Luca; Topai, Alessandra
Tetrahedron Letters, 2001 , vol. 42, # 25 p. 4257 - 4259 Title/Abstract Full Text View citing articles Show Details
With methanol; ammonia; hydrogen; nickel
T=150°C; P=110326 Torr;
Schwoegler; Adkins
Journal of the American Chemical Society, 1939 , vol. 61, p. 3499,3500 Full Text Show Details
With methanol; ammonia; hydrogen; nickel
T=90 - 100°C; P=4413.05 Torr;
Bami; Iyer; Guha
Journal of the Indian Institute of Science, Section A, 1947 , vol. 29, p. 12 Current Science, 1947 , vol. 16, p. 254 Full Text Show Details
Hide Details With methanol; platinum(IV) oxide; ammonia; hydrogen; ammonium chloride
P=735.5 - 2206.5 Torr;
Alexander; Misegades
Journal of the American Chemical Society, 1948 , vol. 70, p. 1316 Full Text Show Details
With ammonium hydroxide; hydrogen; nickel
Kuffner,F. et al.
Monatshefte fuer Chemie, 1962 , vol. 93, p. 469 - 475 Full Text View citing articles Show Details
With ammonia; nickel
T=120°C; P=25742.8 Torr; Hydrogenation;
Norton et al.
Journal of Organic Chemistry, 1952 , vol. 19, p. 1054,1055 Full Text Show Details
Balandin; Wasjunina
Doklady Akademii Nauk SSSR, 1955 , vol. 103, p. 831,833 Chem.Abstr., 1956 , p. 9283 Full Text Show Details
Multi-step reaction with 2 steps 1: aqueous-alcoholic NaOH-solution 2: nickel / 180 - 200 °C / Hydrogenation View Scheme
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 692 Bulletin de la Societe Chimique de France, 1921 , vol. <4>29, p. 220 Full Text Show Details
With NADH in aq. buffer T=30°C; pH=9.5;
Chen, Fei-Fei; Liu, You-Yan; Zheng, Gao-Wei; Xu, Jian-He
ChemCatChem, 2015 , vol. 7, # 23 p. 3838 - 3841 Title/Abstract Full Text View citing articles Show Details
5
Synthesize Find similar With hydrogen; nickel in 1,4-dioxane
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Rx-ID: 978152 Find similar reactions
Rubinstein,H. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1973 , p. 2094 - 2097 Full Text View citing articles Show Details
6
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7
A
B
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Rx-ID: 1934193 Find similar reactions
With lithium aluminium tetrahydride; 3-Ocyclohexylmethyl-1,2-O-cyclohexylidene-α-Dglucofuranose in diethyl ether
2.5 h; HeatingLiAlH4 concentration effect on enantiomeric excess; asymmetric reduction of ketones and isoelectronic ketone oximes with LiAlH4-3-Ocyclohexylmethyl-1,2-O-cyclohexylidene-α-Dglucofuranose complex; Product distribution;
Landor, Stephen R.; Chan, Yuet M.; Sonola, Olutunji O.; Tatchell, Austin R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 493 - 496 Title/Abstract Full Text View citing articles Show Details
A
B
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Synthesize Find similar Rx-ID: 4551008 Find similar reactions
Rx-ID: 994101 Find similar reactions
Johnson,R.A. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 4872 - 4880 Full Text View citing articles Show Details
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8
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With hydrogen; palladium on activated charcoal
Title compound not separated from byproducts;
Andres, Celia; Nieto, Javier; Pedrosa, Rafael; Villamanan, Nieves
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 4130 - 4135
9
Title/Abstract Full Text View citing articles Show Details
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Rx-ID: 5803465 Find similar reactions
P=735.5 - 2206.5 Torr; Hydrogenation;
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Alexander; Misegades
Journal of the American Chemical Society, 1948 , vol. 70, p. 1316 Full Text Show Details
10
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T=150°C; P=110326 Torr; Hydrogenation;
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Rx-ID: 5803466 Find similar reactions
Schwoegler; Adkins
Journal of the American Chemical Society, 1939 , vol. 61, p. 3499,3500 Full Text Show Details
11
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Rx-ID: 6672479 Find similar reactions
T=135°C;
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I.G. Farbenind.
Patent: DE527619 , 1929 ; Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 345 Full Text Show Details
12
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Rx-ID: 6932553 Find similar reactions
Isobutylmethylketon, Ni, wss. NaOH, elektrokatalyt. red. Aminierung (Wasserbad);
Mirzoyan et al.
Trudy Khimiko-Metallurgicheskogo Instituta, Akademiya Nauk Kazakhskoi SSR, 1973 , vol. 20, p. 75,77 Chem.Abstr., vol. 80, # 132742e Full Text Show Details
aus Isobutyl-methyl-keton-oxim, LiAlH4-GlucoseKomplex, stereospezif. Red.;
Landor et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 1902 Full Text Show Details
Hide Experimental Procedure
Sutton, Scott C.; Hannah, Amy L.; Chen, Yuewu; Zhu, Shirong
Patent: US2002/161028 A1, 2002 ; Title/Abstract Full Text Show Details
The amines added were as follows: ... ETHYL 4-AMINO-1-PIPERIDINECARBOXYLATE 4-AMINO-1-BENZYLPIPERIDINE 1-(2-AMINOETHYL)PIPERIDINE P-ANISIDINE 1,3-DIMETHYLBUTYLAMINE 1-METHYL-3-PHENYLPROPYLAMINE 2-AMINO-5-DIETHYLAMINOPENTANE BENZYLAMINE ... Hide Details
Hide Experimental Procedure
Petrolite Corporation
Patent: US4026946 A1, 1977 ; Title/Abstract Full Text Show Details
Petrolite Corporation
Patent: US4026807 A1, 1977 ; Title/Abstract Full Text Show Details
The following are representative examples. ... Dodecylamine Monoethanolamine N-Amylamine Sec-amylamine 2-amino-4-methylpentane 4-amino-2-butanol 5-isopropylamino-1-pentanol
Hide Experimental Procedure
Petrolite Corporation
Patent: US4206233 A1, 1980 ; Title/Abstract Full Text Show Details
Petrolite Corporation
Patent: US4248796 A1, 1981 ;
Title/Abstract Full Text Show Details
The following are representative examples. ... Dodecylamine Monoethanolamine n-Amylamine Sec-amylamine 2-amino-4-methylpentane 4-amino-2-butanol 5-isopropylamino-1-pentanol
13
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With ethanol; sodium
Rx-ID: 6932554 Find similar reactions
Gulewitsch; Wasmus
Chemische Berichte, 1906 , vol. 39, p. 1192 Full Text Show Details
14
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Rx-ID: 6932555 Find similar reactions
T=85°C; Hydrogenation;
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Smith; Adkins
Journal of the American Chemical Society, 1938 , vol. 60, p. 660 Full Text Show Details
A
15
B
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Rx-ID: 7053321 Find similar reactions
Gulewitsch; Wasmus
Chemische Berichte, 1906 , vol. 39, p. 1192 Full Text Show Details
16
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Multi-step reaction with 2 steps 1: lithium alanate; diethyl ether 2: O2,O3-dibenzoyl-Dg-tartaric acid
View Scheme
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Rx-ID: 22158691 Find similar reactions
Karrer; Dinkel
Helvetica Chimica Acta, 1953 , vol. 36, p. 122,126 Full Text Show Details
17
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With water; sodium hydroxide in triethanolamine
T=120°C; 6 h; optical yield given as percent ee;
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Rx-ID: 29817086 Find similar reactions
Sun, Jian-Hua; Dai, Rong-Ji; Meng, Wei-Wei; Deng, Yu-Lin
Catalysis Communications, 2010 , vol. 11, # 11 p. 987 - 991 Title/Abstract Full Text View citing articles Show Details
18
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Rx-ID: 31786696 Find similar reactions
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With D-glucopyranose; (R)-alanine; Neosartorya fischeri (R)-selective amine transaminase; pyridoxal 5'phosphate; Reduced nicotinamide-adenine dinucleotide in water
T=30°C; pH=7.5; aq. sodium phosphate bufferEnzymatic reaction;
Schaetzle, Sebastian; Steffen-Munsberg, Fabian; Thontowi, Ahmad; Hoehne, Matthias; Robins, Karen; Bornscheuer, Uwe T.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 13 p. 2439 - 2445 Title/Abstract Full Text View citing articles Show Details
A
B
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19
Synthesize Find similar Rx-ID: 32093034 Find similar reactions
With potassium hydroxide
Inert atmosphere;
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
20
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With Reduced nicotinamide-adenine dinucleotide in aq. buffer T=25°C; pH=9.6; Kinetics;
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Rx-ID: 35688192 Find similar reactions
Abrahamson, Michael J.; Wong, John W.; Bommarius, Andreas S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1780 - 1786 Title/Abstract Full Text View citing articles Show Details
21
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With pyridoxal 5'-phosphate; ω-transaminases from ochrobactrum anthropi mutant
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Rx-ID: 40295149 Find similar reactions
Han, Sang-Woo; Park, Eul-Soo; Dong, Joo-Young; Shin, Jong-Shik
Advanced Synthesis and Catalysis, 2015 , vol. 357, # 8 p. 1732 - 1740
W58A; isopropylamine in aq. phosphate buffer; dimethyl sulfoxide
T=37°C; P=300 Torr; pH=7; Enzymatic reaction; Kinetics; Reagent/catalyst; enantioselective reaction;
Title/Abstract Full Text View citing articles Show Details
22
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With aminedehydrogenase; ammonia; ammonium chloride
T=30°C; pH=8.7; 48 h; Enzymatic reaction; enantioselective reaction;
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Rx-ID: 41148571 Find similar reactions
Mutti, Francesco G.; Knaus, Tanja; Scrutton, Nigel S.; Breuer, Michael; Turner, Nicholas J.
Science, 2015 , vol. 349, # 6255 p. 1525 - 1529 Title/Abstract Full Text View citing articles Show Details
23
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With aminedehydrogenase; ammonia; ammonium chloride
T=30°C; pH=8.7; 48 h; Enzymatic reaction; enantioselective reaction;
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Rx-ID: 41148578 Find similar reactions
Mutti, Francesco G.; Knaus, Tanja; Scrutton, Nigel S.; Breuer, Michael; Turner, Nicholas J.
Science, 2015 , vol. 349, # 6255 p. 1525 - 1529 Title/Abstract Full Text View citing articles Show Details
24
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With aminedehydrogenase; ammonia; ammonium chloride
T=30°C; pH=8.7; 48 h; Enzymatic reaction; enantioselective reaction;
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Rx-ID: 41148586 Find similar reactions
Mutti, Francesco G.; Knaus, Tanja; Scrutton, Nigel S.; Breuer, Michael; Turner, Nicholas J.
Science, 2015 , vol. 349, # 6255 p. 1525 - 1529 Title/Abstract Full Text View citing articles Show Details
73 %Chromat.
With alcohol dehydrogenase from Streptomyces coelicolor; leucine dehydrogenase from Exiguobactertium sibiricum K77S/N270L double mutant; NADH in aq. buffer T=30°C; pH=9.5; 24 h; Enzymatic reaction; stereoselective reaction;
Chen, Fei-Fei; Liu, You-Yan; Zheng, Gao-Wei; Xu, Jian-He
ChemCatChem, 2015 , vol. 7, # 23 p. 3838 - 3841 Title/Abstract Full Text View citing articles Show Details
25
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85 %Spectr.
With [(η6-p-MeC6H4Pri)2Ru2Cl2(μ-Cl)2]; 1,2bis(dimethylphosphanyl)ethane; potassium tertbutylate; hydrazine hydrate; dimethyl sulfoxide in tert-butyl alcohol
T=100°C; 12 h; Inert atmosphereSealed tube;
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Rx-ID: 42534803 Find similar reactions
Dai, Xi-Jie; Li, Chao-Jun
Journal of the American Chemical Society, 2016 , vol. 138, # 16 p. 5433 - 5440 Title/Abstract Full Text View citing articles Show Details
26
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85 %Spectr.
With [(η6-p-MeC6H4Pri)2Ru2Cl2(μ-Cl)2]; 1,2bis(dimethylphosphanyl)ethane; potassium tertbutylate; hydrazine hydrate; dimethyl sulfoxide in tert-butyl alcohol
T=100°C; 12 h; Inert atmosphereSealed tube;
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Dai, Xi-Jie; Li, Chao-Jun
Journal of the American Chemical Society, 2016 , vol. 138, # 16 p. 5433 - 5440 Title/Abstract Full Text View citing articles Show Details
A
27
Synthesize
Rx-ID: 42534804 Find similar reactions
B
C
Find similar Rx-ID: 39607731 Find similar reactions
A: 6% B: 12% C: 7%
With ammonia; hydrogen in o-xylene
T=150°C; 20 h; Autoclave;
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Nakamura, Yoichi; Kon, Kenichi; Touchy, Abeda Sultana; Shimizu, Ken-Ichi; Ueda, Wataru
ChemCatChem, 2015 , vol. 7, # 6 p. 921 - 924 Title/Abstract Full Text View citing articles Show Details
28
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73%
With hydrazine hydrate in methanol; water
amination; 5 h; Heating;
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Rx-ID: 5344787 Find similar reactions
Hoffmann, Reinhard W.; Stenkamp, Dirk; Trieselmann, Thomas; Goettlich, Richard
European Journal of Organic Chemistry, 1999 , # 11 p. 2915 - 2927 Title/Abstract Full Text View citing articles Show Details
29
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30
Multi-step reaction with 3 steps 1.1: BF3*Et2O; NaBD4 / diethyl ether / -78 - 20 °C 1.2: 15 percent / H2O2; NaOH / H2O; diethyl ether / 2 h / 20 °C 2.1: triphenylphosphane; diethyl azodicarboxylate / tetrahydrofuran / 12 h / 20 °C 3.1: 73 percent / hydrazine hydrate / methanol; H2O / 5 h / Heating View Scheme
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Rx-ID: 16041042 Find similar reactions
Hoffmann, Reinhard W.; Stenkamp, Dirk; Trieselmann, Thomas; Goettlich, Richard
European Journal of Organic Chemistry, 1999 , # 11 p. 2915 - 2927 Title/Abstract Full Text View citing articles Show Details
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Multi-step reaction with 2 steps 1: triphenylphosphane; diethyl azodicarboxylate / tetrahydrofuran / 12 h / 20 °C 2: 73 percent / hydrazine hydrate / methanol; H2O / 5 h / Heating View Scheme
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Rx-ID: 16065695 Find similar reactions
Hoffmann, Reinhard W.; Stenkamp, Dirk; Trieselmann, Thomas; Goettlich, Richard
European Journal of Organic Chemistry, 1999 , # 11 p. 2915 - 2927 Title/Abstract Full Text View citing articles Show Details
A
B
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31
Synthesize Find similar Rx-ID: 198411 Find similar reactions
With ethanol; sodium
Kerp
Justus Liebigs Annalen der Chemie, 1896 , vol. 290, p. 148 Full Text Show Details
A
B
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32
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Rx-ID: 6949373 Find similar reactions
33
isomer(ic) II;
Harries; Gley
Chemische Berichte, 1899 , vol. 32, p. 1331 Full Text Show Details
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With sodium in various solvent(s)
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Rx-ID: 2195216 Find similar reactions
Braconnier, M.F.; Braekman, J.C.; Daloze, D.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 8 p. 605 - 614 Title/Abstract Full Text Show Details
34
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With hydrogenchloride; water
Hydrolysis; 1 h; Heating;
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Rx-ID: 5069970 Find similar reactions
Gajda, Tadeusz; Napieraj, Anna; Osowska-Pacewicka, Krystyna; Zawadzki, Stefan; Zwierzak, Andrzej
Tetrahedron, 1997 , vol. 53, # 13 p. 4935 - 4946 Title/Abstract Full Text View citing articles Show Details
35
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With hydrogenchloride
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Rx-ID: 9992568 Find similar reactions
Xiao, Xue; Wang, Haowei; Huang, Zhiyan; Yang, Jun; Bian, Xiaoxia; Qin, Yong
Organic Letters, 2006 , vol. 8, # 1 p. 139 - 142 Title/Abstract Full Text View citing articles Show Details
36
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With hydrogenchloride in methanol
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Rx-ID: 10548107 Find similar reactions
Tanuwidjaja, Jessica; Peltier, Hillary M.; Ellman, Jonathan A.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 626 - 629
Title/Abstract Full Text View citing articles Show Details
37
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Multi-step reaction with 3 steps 1: titanium(IV) ethoxide / tetrahydrofuran / 10 h / 60 °C 2: L-Selectride(R) / tetrahydrofuran / -48 - 20 °C 3: HCl / methanol View Scheme
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Rx-ID: 11874209 Find similar reactions
Tanuwidjaja, Jessica; Peltier, Hillary M.; Ellman, Jonathan A.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 626 - 629 Title/Abstract Full Text View citing articles Show Details
38
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Multi-step reaction with 2 steps 1: L-Selectride(R) / tetrahydrofuran / -48 - 20 °C 2: HCl / methanol View Scheme
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Rx-ID: 11879665 Find similar reactions
Tanuwidjaja, Jessica; Peltier, Hillary M.; Ellman, Jonathan A.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 626 - 629 Title/Abstract Full Text View citing articles Show Details
39
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Multi-step reaction with 2 steps 1: diethylzinc; Ni(acac)2 / dioxane; toluene / 20 °C 2: HCl View Scheme
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Rx-ID: 12846196 Find similar reactions
Xiao, Xue; Wang, Haowei; Huang, Zhiyan; Yang, Jun; Bian, Xiaoxia; Qin, Yong
Organic Letters, 2006 , vol. 8, # 1 p. 139 - 142 Title/Abstract Full Text View citing articles Show Details
40
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Multi-step reaction with 3 steps 1: pyridine 2: LAH / tetrahydrofuran 3: Na / various solvent(s) View Scheme
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Rx-ID: 20049442 Find similar reactions
Braconnier, M.F.; Braekman, J.C.; Daloze, D.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 8 p. 605 - 614 Title/Abstract Full Text Show Details
41
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Multi-step reaction with 5 steps 1: SOCl2
2: LAH 3: pyridine 4: LAH / tetrahydrofuran 5: Na / various solvent(s) View Scheme
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Rx-ID: 20049482 Find similar reactions
Braconnier, M.F.; Braekman, J.C.; Daloze, D.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 8 p. 605 - 614 Title/Abstract Full Text Show Details
42
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Multi-step reaction with 4 steps 1: LAH 2: pyridine 3: LAH / tetrahydrofuran 4: Na / various solvent(s) View Scheme
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Rx-ID: 20049508 Find similar reactions
Braconnier, M.F.; Braekman, J.C.; Daloze, D.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 8 p. 605 - 614 Title/Abstract Full Text Show Details
43
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Multi-step reaction with 2 steps 1: LAH / tetrahydrofuran 2: Na / various solvent(s) View Scheme
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Rx-ID: 20054844 Find similar reactions
Braconnier, M.F.; Braekman, J.C.; Daloze, D.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 8 p. 605 - 614 Title/Abstract Full Text Show Details
A
B
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44
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Rx-ID: 29817089 Find similar reactions
With lipase B from Candida antarctica in diethyl ether
T=20°C; 8 h; Enzymatic reaction; optical yield given as percent ee;
Sun, Jian-Hua; Dai, Rong-Ji; Meng, Wei-Wei; Deng, Yu-Lin
Catalysis Communications, 2010 , vol. 11, # 11 p. 987 - 991 Title/Abstract Full Text View citing articles Show Details
A
B
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45
Synthesize Find similar Rx-ID: 29908328 Find similar reactions
With lithium hydroxide hydrate in N,N-dimethylformamide
T=20°C; Inert atmosphere;
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Bornholdt, Jan; Felding, Jakob; Clausen, Rasmus P.; Kristensen, Jesper L.
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12474 - 12480 Title/Abstract Full Text View citing articles Show Details
A
B
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46
Synthesize Find similar Rx-ID: 183460 Find similar reactions
With nickel
T=180 - 200°C; Hydrogenation;
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 692 Bulletin de la Societe Chimique de France, 1921 , vol. <4>29, p. 220 Full Text Show Details
A
B
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47
Synthesize Find similar Rx-ID: 6934090 Find similar reactions
T=180 - 200°C; Hydrogenation;
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 692 Bulletin de la Societe Chimique de France, 1921 , vol. <4>29, p. 220 Full Text Show Details
A
B
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Synthesize Find similar
48
Synthesize Find similar Rx-ID: 32092998 Find similar reactions
Multi-step reaction with 3 steps 1.1: ethanol; water / Resolution of racemate; Inert
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448
atmosphere 2.1: potassium hydroxide / Inert atmosphere 2.2: pH 1 / Inert atmosphere 3.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Title/Abstract Full Text View citing articles Show Details
A
B
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49
Synthesize Find similar Rx-ID: 32093010 Find similar reactions
Multi-step reaction with 4 steps 1.1: potassium hydroxide / Inert atmosphere 1.2: pH 1 / Inert atmosphere 2.1: ethanol; water / Resolution of racemate; Inert atmosphere 3.1: potassium hydroxide / Inert atmosphere 3.2: pH 1 / Inert atmosphere 4.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
B
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50
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Rx-ID: 32093016 Find similar reactions
in hexane; ethyl acetate
T=20°C; Resolution of racemateInert atmosphereHeating; optical yield given as percent de;
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
B
51
Synthesize Find similar Rx-ID: 32093025 Find similar reactions
Multi-step reaction with 2 steps 1.1: potassium hydroxide / Inert atmosphere 1.2: pH 1 / Inert atmosphere 2.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
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Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
B
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52
Synthesize Find similar Rx-ID: 32093043 Find similar reactions
Multi-step reaction with 6 steps 1.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere 2.1: sodium isopropylthiolate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere 2.2: Inert atmosphere 3.1: potassium hydroxide / Inert atmosphere 3.2: pH 1 / Inert atmosphere 4.1: ethanol; water / Resolution of racemate; Inert atmosphere 5.1: potassium hydroxide / Inert atmosphere 5.2: pH 1 / Inert atmosphere 6.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
53
B
Synthesize Find similar Rx-ID: 32093054 Find similar reactions
Multi-step reaction with 5 steps 1.1: sodium isopropylthiolate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere 1.2: Inert atmosphere 2.1: potassium hydroxide / Inert atmosphere 2.2: pH 1 / Inert atmosphere 3.1: ethanol; water / Resolution of racemate; Inert atmosphere 4.1: potassium hydroxide / Inert atmosphere 4.2: pH 1 / Inert atmosphere 5.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Synthesize Find similar
Synthesize Find similar
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
B
Synthesize Find similar
Synthesize Find similar
54
Synthesize Find similar Rx-ID: 32093067 Find similar reactions
Multi-step reaction with 7 steps 1.1: n-butyllithium / diethyl ether; hexane / 16 h / 20 °C / Inert atmosphere 1.2: Inert atmosphere; Reflux 2.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere 3.1: sodium isopropylthiolate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere 3.2: Inert atmosphere 4.1: potassium hydroxide / Inert atmosphere 4.2: pH 1 / Inert atmosphere 5.1: ethanol; water / Resolution of racemate; Inert atmosphere 6.1: potassium hydroxide / Inert atmosphere 6.2: pH 1 / Inert atmosphere 7.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details
A
B
55
Synthesize Find similar Rx-ID: 32093082 Find similar reactions
Multi-step reaction with 8 steps 1.1: tetrahydrofuran / 3.75 h / 0 - 20 °C / Inert atmosphere 2.1: n-butyllithium / diethyl ether; hexane / 16 h / 20 °C / Inert atmosphere 2.2: Inert atmosphere; Reflux 3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C / Inert atmosphere 4.1: sodium isopropylthiolate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere 4.2: Inert atmosphere 5.1: potassium hydroxide / Inert atmosphere 5.2: pH 1 / Inert atmosphere 6.1: ethanol; water / Resolution of racemate; Inert atmosphere 7.1: potassium hydroxide / Inert atmosphere 7.2: pH 1 / Inert atmosphere 8.1: hexane; ethyl acetate / 20 °C / Resolution of racemate; Inert atmosphere; Heating View Scheme
Synthesize Find similar
Synthesize Find similar
Ribeiro, Nigel; Kobayashi, Yuka; Maeda, Jin; Saigo, Kazuhiko
Chirality, 2011 , vol. 23, # 6 p. 438 - 448 Title/Abstract Full Text View citing articles Show Details