Cyclohexanone by Asch

Reaxys

PubChem

eMolecules

Reactions (1470)

Yield

Substances (2)

Citations (3478)

Conditions

References

892 Synthesize Find similar

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Rx-ID: 2101280 Find similar reactions

With oxygen O2, singlet; rose bengal disodium salt in methanol; dichloromethane

91 h; Irradiation;

13%

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Chawla, H. Mohindra; Hassner, Alfred

Tetrahedron Letters, 1986 , vol. 27, # 38 p. 4619 - 4622 Title/Abstract Full Text View citing articles Show Details

893 Synthesize Find similar A: 33% B: 26%

Rx-ID: 2114072 Find similar reactions

With oxygen; anhydrous cobalt diacetate

T=90°C; P=750.06 Torr; other oxygen pressure; MechanismRate constant;

Vcelak, Jaroslav; Klimova, Miroslava; Chvalovsky, Vaclav

Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 4 p. 847 - 866 Title/Abstract Full Text Show Details

894 Synthesize Find similar A: 20 % Chromat. B: 54 % Chromat. C: 14 % Chromat.

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Rx-ID: 2530490 Find similar reactions

With dichloro bis(acetonitrile) palladium(II) in dichloromethane

2 h; Ambient temperature;

Baan, J. L. van der; Bickelhaupt, F.

Tetrahedron Letters, 1986 , vol. 27, # 51 p. 6267 - 6270 Title/Abstract Full Text View citing articles Show Details

With dichloro bis(acetonitrile) palladium(II)

2 h; Ambient temperaturevarious solvents; Product distribution;

Baan, J. L. van der; Bickelhaupt, F.

Tetrahedron Letters, 1986 , vol. 27, # 51 p. 6267 - 6270 Title/Abstract Full Text View citing articles Show Details

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895 Synthesize Find similar

Rx-ID: 2530491 Find similar reactions

A: 71 % Chromat. B: 20 % Chromat.

With dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran

2 h; Ambient temperature;

Baan, J. L. van der; Bickelhaupt, F.

Tetrahedron Letters, 1986 , vol. 27, # 51 p. 6267 - 6270 Title/Abstract Full Text View citing articles Show Details

A: 71 % Chromat. B: 20 % Chromat.

With dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran

2 h; Ambient temperature;

Baan, J. L. van der; Bickelhaupt, F.

Tetrahedron Letters, 1986 , vol. 27, # 51 p. 6267 - 6270 Title/Abstract Full Text View citing articles Show Details

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896 Synthesize Find similar

Rx-ID: 2531176 Find similar reactions

With titanium tetrachloride

Hatanaka, Yasuo; Kuwajima, Isao

Tetrahedron Letters, 1986 , vol. 27, # 6 p. 719 - 722 Title/Abstract Full Text Show Details

Synthesize

897 Synthesize

Rx-ID: 2531963

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With titanium tetrachloride in dichloromethane

T=0°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

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Sato, Tadashi; Watanabe, Masami; Murayama, Eigoro

Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1621 - 1624 Title/Abstract Full Text View citing articles Show Details

898 Synthesize Find similar

Rx-ID: 2553476 Find similar reactions

Quinga, E. M. Y.; Mendenhall, G. D.

Journal of the American Chemical Society, 1986 , vol. 108, # 3 p. 474 - 478 Title/Abstract Full Text View citing articles Show Details

With 9,10-Dibromoanthracene in various solvent(s) T=43.7°C; investigation the chemiluminescent thermolysis; activation energy and ΔH0 investigated; Product distributionQuantum yieldThermodynamic data;

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899 Synthesize Find similar

B: 79%

Rx-ID: 2772454 Find similar reactions

With triethylamine in dichloromethane

T=20 - 25°C; 60 h;

Jefford, Charles W.; Rossier, Jean-Claude; Boukouvalas, John

Journal of the Chemical Society, Chemical Communications, 1986 , # 23 p. 1701 - 1702 Title/Abstract Full Text View citing articles Show Details

900 Synthesize Find similar

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T=180°C; P=10 Torr; Yield given;

Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.

Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 5219 Title/Abstract Full Text View citing articles Show Details

95 % Spectr.

With lithium bromide

T=60°C;

Robinson, Philip L.; Kelly, Jeffery W.; Evans, Slayton A.

Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 15 - 24 Title/Abstract Full Text Show Details

901

Rx-ID: 3056579 Find similar reactions

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A: 0.6% B: 2.7% C: 2.9%

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With hydrogen; magnesium oxide; ruthenium in water

T=99.9°C; P=15001.2 Torr; Product distribution;

Rx-ID: 3387765 Find similar reactions

Sokol'skii, D. V.; Ualikhanova, A.; Temirbulatova, A. E.; Mailyubaev, B. T.

Journal of Organic Chemistry USSR (English Translation), 1986 , p. 1520 - 1524 Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 8 p. 1693 - 1697 Title/Abstract Full Text Show Details

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902 Synthesize Find similar

A: 97%

Rx-ID: 3662683 Find similar reactions

With triethylamine in dichloromethane

T=20 - 25°C; 16 h;

Jefford, Charles W.; Rossier, Jean-Claude; Boukouvalas, John

Journal of the Chemical Society, Chemical Communications, 1986 , # 23 p. 1701 - 1702 Title/Abstract Full Text View citing articles Show Details

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903 Synthesize Find similar

A: 95%

Rx-ID: 3663320 Find similar reactions

With triethylamine in dichloromethane

T=20 - 25°C; 58 h;

Jefford, Charles W.; Rossier, Jean-Claude; Boukouvalas, John

Journal of the Chemical Society, Chemical Communications, 1986 , # 23 p. 1701 - 1702 Title/Abstract Full Text View citing articles Show Details

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904 Synthesize Find similar

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Rx-ID: 3737833 Find similar reactions

With iodosylbenzene; [(5,5'-H2Salen)MnIII]+PF6-

T=25°C; investigation of the oxidation catalyzed by different cationic (salen)MnIII complexes; Product distribution; A

905

Srinivasan, K.; Michaud, P.; Kochi, J. K.

Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2309 2320 Title/Abstract Full Text View citing articles Show Details

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A: 13.9% B: 5.1% C: 17.8% D: 4.8% E: 11.9%

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With aluminium trichloride; palladium/alumina; sodium chloride

T=160°C; 3 h; various reaction temperatures; effect of the amount of the fused salt; Product distribution;

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Kamiyama, Tsutomu; Enomoto, Saburo; Inoue, Masami

Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 2 p. 450 - 454 Title/Abstract Full Text Show Details

906 Synthesize Find similar

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Rx-ID: 8491911 Find similar reactions

With styrene; meta-diisopropyl benzene; sulfuric acid

multistep reaction; 1.) acetonitrile, 2.) MeOH/H2O;

Shea, K. J.; Dougherty, T. K.

Journal of the American Chemical Society, 1986 , vol. 108, # 5 p. 1091 1093 Title/Abstract Full Text View citing articles Show Details

With 1,2-bis-(ethylene)-benzene; sulfuric acid

multistep reaction; 1.) acetonitrile, 2.) MeOH/H2O;

Shea, K. J.; Dougherty, T. K.

Journal of the American Chemical Society, 1986 , vol. 108, # 5 p. 1091 1093 Title/Abstract Full Text View citing articles Show Details

907 Synthesize Find similar

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Rx-ID: 11736391 Find similar reactions

Multi-step reaction with 2 steps 1: 90.2 percent Chromat. / H2 / 5percent Ru/MgO / H2O / 99.9 °C / 45003.6 Torr 2: 0.3 percent / H2 / 5percent Ru/MgO / H2O / 99.9 °C / 15001.2 Torr View Scheme

Sokol'skii, D. V.; Ualikhanova, A.; Temirbulatova, A. E.; Mailyubaev, B. T.

Journal of Organic Chemistry USSR (English Translation), 1986 , p. 1520 - 1524 Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 8 p. 1693 - 1697 Title/Abstract Full Text Show Details

Multi-step reaction with 3 steps 1: 9.8 percent Chromat. / H2 / 5percent Ru/MgO / H2O / 99.9 °C / 45003.6 Torr 2: 1.4 percent / H2, NH4OH / 5percent Ru/MgO / H2O / 99.9 °C / 15001.2 Torr 3: 0.3 percent / H2 / 5percent Ru/MgO / H2O / 99.9 °C / 15001.2 Torr View Scheme

Sokol'skii, D. V.; Ualikhanova, A.; Temirbulatova, A. E.; Mailyubaev, B. T.

Journal of Organic Chemistry USSR (English Translation), 1986 , p. 1520 - 1524 Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 8 p. 1693 - 1697 Title/Abstract Full Text Show Details

908 Synthesize Find similar

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Rx-ID: 11742512 Find similar reactions

Multi-step reaction with 2 steps 1: 1.4 percent / H2, NH4OH / 5percent Ru/MgO / H2O / 99.9 °C / 15001.2 Torr 2: 0.3 percent / H / 5percent Ru/MgO / H O / 99.9 °C / 15001.2 Torr

Sokol'skii, D. V.; Ualikhanova, A.; Temirbulatova, A. E.; Mailyubaev, B. T.

Journal of Organic Chemistry USSR (English Translation), 1986 , p. 1520 - 1524

View Scheme

Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 8 p. 1693 - 1697 Title/Abstract Full Text Show Details

909 Synthesize Find similar

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Rx-ID: 19187048 Find similar reactions

Multi-step reaction with 2 steps 1: CH2Cl2 / Ambient temperature 2: CH2Cl2 / Ambient temperature View Scheme

Moriarty, Robert M.; Prakash, Om; Vavilikolanu, Pushra R.

Synthetic Communications, 1986 , vol. 16, # 10 p. 1247 - 1254 Title/Abstract Full Text Show Details

910 Synthesize Find similar

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Rx-ID: 21491782 Find similar reactions

Multi-step reaction with 2 steps 1: 10 percent / Rose Bengal (10-5 M), singlet oxygen / CH2Cl2 / 72 h / Irradiation

2: 10 percent / Rose Bengal (10-5 M), singlet oxygen / methanol; CH2Cl2 / 115 h / Irradiation View Scheme

Chawla, H. Mohindra; Hassner, Alfred

Tetrahedron Letters, 1986 , vol. 27, # 38 p. 4619 - 4622 Title/Abstract Full Text View citing articles Show Details

911 Synthesize Find similar

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Rx-ID: 21491786 Find similar reactions

Multi-step reaction with 2 steps 1: 11 percent / Rose Bengal (10-5 M), singlet oxygen / 93 h / Irradiation 2: 10 percent / Rose Bengal (10-5 M), singlet oxygen / methanol; CH2Cl2 / 115 h / Irradiation View Scheme

Chawla, H. Mohindra; Hassner, Alfred

Tetrahedron Letters, 1986 , vol. 27, # 38 p. 4619 - 4622 Title/Abstract Full Text View citing articles Show Details

912 Synthesize Find similar

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Rx-ID: 21492421 Find similar reactions

Multi-step reaction with 2 steps 1: 9 percent / Rose Bengal (10-5 M), singlet oxygen / 68 h / Irradiation 2: 10 percent / Rose Bengal (10-5 M), singlet oxygen / methanol; CH2Cl2 / 115 h / Irradiation View Scheme

Chawla, H. Mohindra; Hassner, Alfred

Tetrahedron Letters, 1986 , vol. 27, # 38 p. 4619 - 4622 Title/Abstract Full Text View citing articles Show Details

913 Synthesize Find similar

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Rx-ID: 24960042 Find similar reactions

With hydrogenchloride; sodium chloride; sodium carbonate in butan-1-ol

International Flavors and Fragrances Inc.

Patent: US4585582 A1, 1986 ;

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Title/Abstract Full Text Show Details

II.C:EXAMPLE II-C STR23

EXAMPLE II-C STR23 Into a 250 ml reaction flask equipped with mechanical stirrer, immersion thermometer, water-cooled condenser and heating mantle is placed 0.23 moles of the aldol condensation product of cyclohexanone and n-valeraldehyde produced according to Example II-A and 176.4 ml of 5percent hydrogen chloride in n-butanol (8.4 ml of 38percent HCl in 168 ml n-butanol). The reaction mass is heated with stirring to reflux and refluxed until a ratio of endo:exo isomer is about 13:1 monitored on a 6'*1/4" SE-30 glass packed GLC column. The time of reaction of 170 minutes. At the end of the 170-minute period the reaction apparatus is shut down and the reaction mass is washed with 1 volume of saturated sodium chloride solution followed by 1 volume of 10percent sodium carbonate solution and 3 volumes of saturated sodium chloride solution. The product is then dried over anhydrous sodium sulfate to yield 230 grams of crude. The crude material is distilled under vacuum using a rush-over head. The yield of product is 140 grams.

With hydrogenchloride; sodium chloride; sodium carbonate in butan-1-ol

International Flavors and Fragrances Inc.

Patent: US4310701 A1, 1982 ;

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Title/Abstract Full Text Show Details

VI.C:EXAMPLE VI-C STR68

EXAMPLE VI-C STR68 Into a 250 ml reaction flask equipped with mechanical stirrer, immersion thermometer, water-cooled condenser and heating mantle is placed 0.23 moles of the aldol condensation product of cyclohexanone and n-valeraldehyde produced according to Example VI-A and 176.4 ml of 5percent hydrogen chloride in n-butanol (8.4 ml of 38percent HCl in 168 ml n-butanol). The reaction mass is heated with stirring to reflux and refluxed until a ratio of endo:exo isomer is about 13:1 monitored on a 6'*1/4" SE-30 glass packed GLC column. The time of reaction of 170 minutes. At the end of the 170-minute period the reaction apparatus is shut down and the reaction mass is washed with 1 volume of saturated sodium chloride solution followed by 1 volume of 10percent sodium carbonate solution and 3 volumes of saturated sodium chloride solution. The product is then dried over anhydrous sodium sulfate to yield 230 grams of crude. The crude material is distilled under vacuum using a rush-over head. The yield of product is 140 grams. A

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914 Synthesize Find similar

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Rx-ID: 1504816 Find similar reactions

A: 1.6% B: 0.6% C: 17.5% D: 0.7%

With oxygen; zinc; iron in water; acetic acid

T=20°C; isotope effect, competitive oxidation; Mechanism;

Barton, Derek H. R.; Boivin, Jean; Ozbalik, Nubar; Schwartzentruber, Kathy M.; Jankowski, Krzysztof

Tetrahedron Letters, 1985 , vol. 26, # 4 p. 447 - 450 Title/Abstract Full Text View citing articles Show Details

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915 Synthesize

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Rx-ID: 1590644

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B: 10 % Chromat.

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With hydrogenchloride; sodium periodate

1.) 20-25 deg C, 1 h; Yield given. Multistep reaction;

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Uemura, Sakae; Fukuzawa, Shin-ichi

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 471 - 480 Title/Abstract Full Text View citing articles Show Details

916 Synthesize Find similar

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Rx-ID: 1818322 Find similar reactions

With pyridine; 2-hydroxy-1,3-isoindolinedione; lithium perchlorate in acetonitrile

Ambient temperatureelectrolysis: 0.85 V vs. s.c.e.;

90%

Masui, Masaichiro; Kawaguchi, Tetsuo; Ozaki, Shigeko

Journal of the Chemical Society, Chemical Communications, 1985 , # 21 p. 1484 - 1485 Title/Abstract Full Text View citing articles Show Details

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917 Synthesize Find similar

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Rx-ID: 1856474 Find similar reactions

Sharma, S. N.; Sonawane, H. R.; Dev, Sukh

Tetrahedron, 1985 , vol. 41, # 12 p. 2483 - 2492 Title/Abstract Full Text View citing articles Show Details

in ethyl acetate

10 h; Irradiation; Yield given. Yields of byproduct given;

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918 Synthesize Find similar Rx-ID: 1999529 Find similar reactions

B: 18% C: 24% D: 18%

With Co(III)(BPI)(OAc)(OO-tBu)

T=60°C; 2 h; stoichiometric oxidation by various cobalt(III)alkylperoxy complexes, solvents; Product distribution;

Saussine, Lucien; Brazi, Eric; Robine, Alain; Mimoun, Hubert; Fischer, Jean; Weiss, Raymond

Journal of the American Chemical Society, 1985 , vol. 107, # 12 p. 3534 3540 Title/Abstract Full Text View citing articles Show Details

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919 Synthesize

Find similar Rx-ID: 2027396 Find similar reactions

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in cyclohexane

T=80°C; 1 h; other cyclohexyloxy radical sources, var. temperature; the effect of the number of atoms separating potential CyO radicals, the effect of O2; Product distributionMechanism; A

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Druliner, J. D.; Krusic, P. J.; Lehr, G. F.; Tolman, C. A.

Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5838 - 5845 Title/Abstract Full Text View citing articles Show Details

920 Synthesize Find similar

With triphenylbismuthine in toluene

T=25°C; 48 h; Yield given. Yields of byproduct given;

Rx-ID: 2027398 Find similar reactions

Dodonov, V. A.; Gushchin, A. V.; Brilkina, T. G.

J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 73 - 80,63 - 68 Title/Abstract Full Text Show Details

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921 Synthesize Find similar

A: 70% B: 6 % Chromat.

Rx-ID: 2328782 Find similar reactions

With boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide in dichloromethane

T=25°C; 4 h;

Mandal, Arun K.; Soni, N. R.; Ratnam, K. R.

Synthesis, 1985 , # 3 p. 274 - 275 Title/Abstract Full Text Show Details

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922 Synthesize Find similar

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Rx-ID: 2429480 Find similar reactions

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Yield given. Yields of byproduct given;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

923 Synthesize Find similar

Synthesize Find similar

Rx-ID: 2429483 Find similar reactions

A: 70%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

A: 70%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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924 Synthesize Find similar

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Rx-ID: 2429486 Find similar reactions

B: 78%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

B: 78%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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925 Synthesize Find similar

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Rx-ID: 2429487 Find similar reactions

B: 86%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

B: 86%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

926 Synthesize Find similar

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Rx-ID: 2429497 Find similar reactions

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B: 30%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Yield given;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

B: 30%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Yields of byproduct given;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

B: 30%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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927 Synthesize Find similar

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Rx-ID: 2429498 Find similar reactions

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Yield given. Yields of byproduct given;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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928 Synthesize Find similar

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Rx-ID: 2429503 Find similar reactions

A: 7% B: 88%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

A: 7% B: 88%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

A: 7% B: 88%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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929 Synthesize Find similar

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Rx-ID: 2429504 Find similar reactions

B: 83%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

B: 83%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

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930 Synthesize Find similar

With Ph3BiCl2 in toluene

T=19°C; 200 h; Yield given. Yields of byproduct given;

Rx-ID: 2443578 Find similar reactions

Dodonov, V. A.; Gushchin, A. V.; Brilkina, T. G.

J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 73 - 80,63 - 68 Title/Abstract Full Text Show Details

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931 Synthesize Find similar

With nickel boride

Ambient temperature; Yield given;

Rx-ID: 2526226 Find similar reactions

Barton, Derek H. R.; Fekih, Abdelwaheb; Lusinchi, Xavier

Tetrahedron Letters, 1985 , vol. 26, # 50 p. 6197 - 6200 Title/Abstract Full Text View citing articles Show Details

932 Synthesize Find similar

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Rx-ID: 2531927 Find similar reactions

A: 5 % Chromat. B: 15 % Chromat.

With n-butyllithium in tetrahydrofuran

T=-78°C; Title compound not separated from byproducts;

Cooke, Manning P.; Houpis, Ioannis N.

Tetrahedron Letters, 1985 , vol. 26, # 41 p. 4987 - 4990 Title/Abstract Full Text View citing articles Show Details

A: 5 % Chromat. B: 15 % Chromat.

With n-butyllithium in tetrahydrofuran

T=-78°C; Title compound not separated from byproducts;

Cooke, Manning P.; Houpis, Ioannis N.

Tetrahedron Letters, 1985 , vol. 26, # 41 p. 4987 - 4990 Title/Abstract Full Text View citing articles Show Details

933 Synthesize Find similar

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Rx-ID: 2568006 Find similar reactions

95%

With hydrogenchloride in methanol

Heating;

Ogura, Katsuyuki; Yahata, Nobuhiro; Hashizume, Kimitoshi; Tsuyama, Koichi; Takahashi, Kazumasa; Iida, Hirotada

Chemistry Letters, 1983 , p. 767 - 770 Title/Abstract Full Text Show Details

67%

With sodium hydrogencarbonate in 1,4-dioxane; water

Irradiation;

Ogura, Katsuyuki; Ohtsuki, Kazuo; Nakamura, Masami; Yahata, Nobuhiro; Takahashi, Kazumasa; Iida, Hirotada

Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2455 - 2458 Title/Abstract Full Text View citing articles Show Details

With hydrogenchloride in methanol

3 h; Heating; Yield given;

Ogura, Katsuyuki; Ohtsuki, Kazuo; Nakamura, Masami; Yahata, Nobuhiro; Takahashi, Kazumasa; Iida, Hirotada

Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2455 - 2458 Title/Abstract Full Text View citing articles Show Details

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With different reagents

different conditions; Product distributionMechanism;

Ogura, Katsuyuki; Ohtsuki, Kazuo; Nakamura, Masami; Yahata, Nobuhiro; Takahashi, Kazumasa; Iida, Hirotada

Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2455 - 2458 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

934 Synthesize Find similar

A: 0.2 g

With hydrogenchloride in chloroform

T=25°C; 24 h;

Rx-ID: 2586269 Find similar reactions

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688

Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

935 Synthesize Find similar

A: 0.4 g

Rx-ID: 2588662 Find similar reactions

With hydrogenchloride in chloroform

T=10°C; 7 h;

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

936 Synthesize Find similar

A: 0.2 g

Rx-ID: 2595314 Find similar reactions

With trifluoroacetic acid in chloroform

T=23°C; overnight;

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

937 Synthesize Find similar

A: 90 % Chromat. B: 90 % Chromat.

Rx-ID: 2646547 Find similar reactions

With ammonium cerium(IV) nitrate in water; acetonitrile

T=25°C;

Wilson, Stephen R.; Zucker, Paul A.; Kim, Chong-wan; Villa, Carmine A. Tetrahedron Letters, 1985 , vol. 26, # 16 p. 1969 - 1972 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

938 Synthesize Find similar Rx-ID: 2899083 Find similar reactions

Synthesize Find similar

With peroxyformic acid

10 h; Irradiation; Yield given. Yields of byproduct given;

Sharma, S. N.; Sonawane, H. R.; Dev, Sukh

Tetrahedron, 1985 , vol. 41, # 12 p. 2483 - 2492 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

939 Synthesize Find similar

Rx-ID: 3123563 Find similar reactions

With potassium carbonate in water-d2

T=34°C; Equilibrium constant;

Burkey, Theodore J.; Fahey, Robert C.

Journal of Organic Chemistry, 1985 , vol. 50, # 8 p. 1304 - 1306 Title/Abstract Full Text View citing articles Show Details

With potassium carbonate in 1,4-dioxane

T=34°C; Equilibrium constant;

Burkey, Theodore J.; Fahey, Robert C.

Journal of Organic Chemistry, 1985 , vol. 50, # 8 p. 1304 - 1306 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

940 Synthesize Find similar

C: 53%

Rx-ID: 3579453 Find similar reactions

Kerr, Bernadette; McCullough, Kevin J.

Journal of the Chemical Society, Chemical Communications, 1985 , # 9 p. 590 - 592 Title/Abstract Full Text View citing articles Show Details

in decane

T=190°C; 8 h;

941 Synthesize Find similar

95 % Spectr.

Synthesize Find similar

Rx-ID: 3590815 Find similar reactions

Gravel, Denis; Murray, Stevens; Ladouceur, Gaetan

Journal of the Chemical Society, Chemical Communications, 1985 , # 24 p. 1828 - 1829 Title/Abstract Full Text View citing articles Show Details

in benzene

2 h; Irradiation;

Synthesize Find similar

942 Synthesize Find similar Rx-ID: 3856103 Find similar reactions

A: 2.7% B: 12.4% C: 8.9% D: 65%

With oxygen

T=120°C; 4.33333 h; Further byproducts given;

Perkel'; Freidin; Neginskaya; Stolyankova; Ivanova

Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 2 p. 1444 1449 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

943 Synthesize Find similar Rx-ID: 3856106 Find similar reactions

A: 2.9% B: 12.4% C: 8.9% D: 65%

With oxygen

T=120°C; 4.33333 h; Further byproducts given;

Perkel'; Freidin; Neginskaya; Stolyankova; Ivanova

Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 2 p. 1444 1449 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

944 Synthesize Find similar Rx-ID: 3856126 Find similar reactions

A: 3.1% B: 12.4% C: 8.9% D: 65%

With oxygen

T=120°C; 4.33333 h; Further byproducts given;

Perkel'; Freidin; Neginskaya; Stolyankova; Ivanova

Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 2 p. 1444 1449 Title/Abstract Full Text View citing articles Show Details

A: 3.1% B: 12.4% C: 8.9% D: 65%

With oxygen

T=120°C; 4.33333 h; Further byproducts given;

Perkel'; Freidin; Neginskaya; Stolyankova; Ivanova

Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 2 p. 1444 1449 Title/Abstract Full Text View citing articles Show Details

A: 3.1% B: 12.4% C: 8.9% D: 65%

With oxygen

T=120°C; 4.33333 h; Further byproducts given;

Perkel'; Freidin; Neginskaya; Stolyankova; Ivanova

Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 2 p. 1444 1449 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

945 Synthesize Find similar

Synthesize Find similar

Rx-ID: 3867821 Find similar reactions

A: 85%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating; Mechanism;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

A: 85%

With methyloxirane in 1,2-dichloro-ethane

0.75 h; Heating;

Nakayama, Juzo; Sugiura, Hidetoshi; Shiotsuki, Atsuko; Hoshino, Masamatsu

Tetrahedron Letters, 1985 , vol. 26, # 18 p. 2195 - 2198 Title/Abstract Full Text View citing articles Show Details

946 Synthesize Find similar

Synthesize Find similar

Rx-ID: 21322701 Find similar reactions

Multi-step reaction with 2 steps 1: 11 percent / toluene / 1.5 h / Heating 2: HCl(g) / CHCl3 / 24 h / 25 °C View Scheme

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688 Title/Abstract Full Text View citing articles Show Details

Multi-step reaction with 2 steps 1: 10.5 percent / toluene / 1.5 h / Heating 2: Trifluoroacetic acid / CHCl3 / 23 °C / overnight View Scheme

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688 Title/Abstract Full Text View citing articles Show Details

947 Synthesize Find similar

Synthesize Find similar

Rx-ID: 21325640 Find similar reactions

Multi-step reaction with 2 steps 1: 9 percent / toluene / 2 h / Heating 2: HCl(g) / CHCl3 / 7 h / 10 °C View Scheme

Bobowski; Shavel Jr.

Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 6 p. 1679 - 1688 Title/Abstract Full Text View citing articles Show Details

948 Synthesize Find similar

Synthesize Find similar

Rx-ID: 21618659 Find similar reactions

Multi-step reaction with 2 steps 1: nickel boride / Ambient temperature 2: pyridine dichromate View Scheme

Barton, Derek H. R.; Fekih, Abdelwaheb; Lusinchi, Xavier

Tetrahedron Letters, 1985 , vol. 26, # 50 p. 6197 - 6200 Title/Abstract Full Text View citing articles Show Details

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949 Synthesize Find similar

B: 88%

in acetonitrile

Irradiation;

Synthesize Find similar

Rx-ID: 1510601 Find similar reactions

Smith, David W.; Pienta, Norbert J.

Tetrahedron Letters, 1984 , vol. 25, # 9 p. 915 - 918

Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

950 Synthesize Find similar

B: 79 % Spectr.

Rx-ID: 1716454 Find similar reactions

With sulfuric acid in diethyl ether

Ambient temperature;

Ogura, K.; Yamashita, M.; Suzuki, M.; Furukawa, S.; Tsuchinashi, G.

Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 6 p. 1637 - 1642 Title/Abstract Full Text Show Details

Synthesize Find similar

951 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Synthesize Find similar

Rx-ID: 1716926 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

952 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Synthesize Find similar

Rx-ID: 1716927 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

953 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Rx-ID: 1716929 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

954 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Synthesize Find similar

Rx-ID: 1716930 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

955 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnigth; Yield given. Multistep reaction;

Synthesize Find similar

Rx-ID: 1716931 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

956 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Synthesize Find similar

Rx-ID: 1716932 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

957 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Rx-ID: 1716933 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545

Title/Abstract Full Text View citing articles Show Details

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958 Synthesize Find similar

A: 67 % Turnov.

Synthesize Find similar

in acetonitrile

T=5 - 10°C; electrolyses at 11.0 A/dm-2; Further byproducts given. Yields of byproduct given;

Synthesize Find similar

Rx-ID: 1731074 Find similar reactions

Harada; Sakakibara; Kunai; Sasaki

Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 611 - 612 Title/Abstract Full Text View citing articles Show Details

959 Synthesize Find similar

B: 88%

Rx-ID: 1731929 Find similar reactions

With 1,4-diaza-bicyclo[2.2.2]octane in acetonitrile

Irradiationdifferent amount of DABCO; MechanismProduct distribution;

Smith, David W.; Pienta, Norbert J.

Tetrahedron Letters, 1984 , vol. 25, # 9 p. 915 - 918 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

960 Synthesize Find similar

Synthesize Find similar

Rx-ID: 1914146 Find similar reactions

A: 30 % Chromat. B: 60 % Chromat. C: 10 % Chromat.

With tetraethylammonium bromide; triethylamine

T=135°C; 360 h; Product distributionMechanism;

Collins, Clair J.; Martinez, Antonio Garcia; Alvarez, Roberto Martinez; Aguirre, Juan Arranz

Chemische Berichte, 1984 , vol. 117, # 9 p. 2815 - 2824 Title/Abstract Full Text Show Details

Synthesize Find similar

961 Synthesize Find similar

Synthesize Find similar

Gas phase. Determ. by ICR spect.; Equilibrium constantThermodynamic data;

Rx-ID: 1927526 Find similar reactions

Bouchoux, G.; Houriet, R.

Tetrahedron Letters, 1984 , vol. 25, # 50 p. 5755 - 5758 Title/Abstract Full Text View citing articles Show Details

962 Synthesize Find similar

67 % Chromat.

Synthesize Find similar

Rx-ID: 1970554 Find similar reactions

With ozone in dichloromethane

T=0 - 25°C; 2.5 h;

Sponsler, Michael B.; Dougherty, Dennis A.

Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4978 - 4984 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

963 Synthesize Find similar

A: 2.5% B: 75 % Turnov. C: 5 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Synthesize Find similar

Rx-ID: 1970555 Find similar reactions

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2490 - 2497 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2721 2729 Title/Abstract Full Text View citing articles Show Details

964 Synthesize Find similar

A: 32.0 % Turnov. B: 61.5 % Turnov.

Rx-ID: 1980361 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

965 Synthesize Find similar

B: 87.5 % Turnov. C: 3.5 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h; further alkylcycloalkanols, relative rates for the elimination of alkyl radicals; Product distribution;

Rx-ID: 2004445 Find similar reactions

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

966 Synthesize Find similar

A: 87.5 % Turnov. B: 3.5 % Turnov.

Rx-ID: 2004446 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Synthesize Find similar

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

967 Synthesize Find similar

Rx-ID: 2016000 Find similar reactions

With aluminium trichloride in dichloromethane

ice-cooling;

Lub, J.; Boer, Th. J. de

Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 11 p. 328 - 332 Title/Abstract Full Text Show Details

Synthesize Find similar

968 Synthesize Find similar

in acetonitrile

T=50.1°C; P=4410350 Torr; 0.333333 h; other solvents: toluene, benzene, other pressures, volume effect of activation; Thermodynamic dataRate constantMechanism;

Synthesize Find similar

Rx-ID: 2027397 Find similar reactions

Zhulin, V.M.; Lipovich, T.V.; Antonovskii, V.L.

Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2262 - 2264 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2473 2476 Title/Abstract Full Text View citing articles Show Details

969 Synthesize Find similar

A: 94.0 % Turnov. B: 1.5 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Rx-ID: 2029238 Find similar reactions

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

2729 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

970 Synthesize Find similar

Rx-ID: 2030092 Find similar reactions

A: 53% B: 4.5 % Turnov. C: 40.5%

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

A: 53.0 % Turnov. B: 4.5 % Turnov. C: 40.5%

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

971 Synthesize Find similar

A: 54 % Chromat. B: 86%

Rx-ID: 2030153 Find similar reactions

With sodium perchlorate in water; acetonitrile

anodic oxidation;

Porter, Quentin N.; Utley, James H. P.; Machion, Pedro D.; Pardini, Vera L.; Schumacher, Paolo R.; Viertler, Hans

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 5 p. 973 - 979 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

972 Synthesize Find similar

A: 10 % Chromat. B: 90 % Chromat.

With dihydrogen peroxide

1.) MeOH, RT, 4 h, 2.) 170-180 deg C, 20 torr; other temperature; Product distribution;

973

Rx-ID: 2039782 Find similar reactions

Mitra, R. B.; Muljiani, Z.; Deshmukh, A. R. A. S.; Joshi, V. S.; Gadre, S. R.

Synthetic Communications, 1984 , vol. 14, # 2 p. 101 - 112 Title/Abstract Full Text Show Details

Synthesize Find similar

A: 89.5 % Turnov. B: 9.0 % Turnov.

Synthesize Find similar

Rx-ID: 2081495 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Synthesize Find similar

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

974 Synthesize Find similar

A: 17.5 % Turnov. B: 79.5 % Turnov.

Rx-ID: 2081496 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Synthesize Find similar

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

975 Synthesize Find similar

A: 87.5 % Turnov. B: 12.5 % Turnov.

Rx-ID: 2100017 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

976 Synthesize Find similar

A: 39 % Turnov. B: 50.0 % Turnov. C: 5.5 %

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Rx-ID: 2100121 Find similar reactions

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Turnov.

Title/Abstract Full Text View citing articles Show Details

A: 39 % Turnov. B: 50.0 % Turnov. C: 5.5 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

977 Synthesize Find similar

Rx-ID: 2140433 Find similar reactions

A: 3.5 % Turnov. B: 43% C: 50.0 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

A: 3.5% B: 43% C: 50.0 % Turnov.

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

978 Synthesize Find similar

A: 11.5 % Turnov. B: 81.0 % Turnov.

Rx-ID: 2142133 Find similar reactions

With pyridine; lead(IV) acetate; copper diacetate in benzene

T=80°C; 2 h;

Kapustina, N. I.; Spektor, S. S.; Nikishin, G. I.

Synthesize Find similar

979 Synthesize Find similar

Synthesize Find similar

With lithium diisopropyl amide

1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight; Yield given. Multistep reaction;

Rx-ID: 2161997 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1539 - 1545 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

980 Synthesize Find similar

A: 60% B: 20%

Rx-ID: 2328781 Find similar reactions

With jones' reagent in acetone

T=15 - 20°C; 0.5 h;

Krishna, R. R.; Chawla, H. P. S.; Dev, Sukh

Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1190 - 1196 Title/Abstract Full Text Show Details

Synthesize Find similar

981 Synthesize Find similar

Rx-ID: 2328784 Find similar reactions

A: 42% B: 36%

With sodium in tetrahydrofuran

T=25°C; 16 h;

Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.; Srinivas, P.

Tetrahedron, 1984 , vol. 40, # 9 p. 1629 - 1632 Title/Abstract Full Text View citing articles Show Details

A: 42% B: 36%

With sodium in tetrahydrofuran

T=25°C; 16 h;

Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.; Srinivas, P.

Tetrahedron, 1984 , vol. 40, # 9 p. 1629 - 1632 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

982 Synthesize Find similar

Synthesize Find similar

Rx-ID: 2443577 Find similar reactions

in tetrachloromethane

T=19°C; 216 h; hydrolysis of the reaction mixture by 15percent aqueous THF; variation of solvents and reaction time; Product distribution;

Dodonov, V. A.; Gushchin, A. V.; Grishin, D. F.; Brilkina, T. G.

J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 1 p. 100 - 103,87 - 89 Title/Abstract Full Text Show Details

983 Synthesize Find similar

99 % Chromat.

Synthesize Find similar

Rx-ID: 2652140 Find similar reactions

With dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol

T=60°C; 3 h; Mechanism;

Tamao, Kohei; Kumada, Makoto; Maeda, Kimio

Tetrahedron Letters, 1984 , vol. 25, # 3 p. 321 - 324

Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

984 Synthesize Find similar

Synthesize Find similar

Rx-ID: 2676279 Find similar reactions

Irradiationreaction also in presence of biacetyl and benzophenone or O2; MechanismRate constant;

Synthesize Find similar

Sundararajan, K.; Ramakrishnan, V.; Kuriacose J.C.

Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 11 p. 1068 - 1070 Title/Abstract Full Text Show Details

985 Synthesize Find similar

With nitrobenzene

Irradiationalso in presence of biacetyl and benzophenone;

Rx-ID: 2676975 Find similar reactions Sundararajan, K.; Ramakrishnan, V.; Kuriacose J.C.

Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 11 p. 1068 - 1070 Title/Abstract Full Text Show Details

Synthesize Find similar

986 Synthesize Find similar

B: 73%

Rx-ID: 2827391 Find similar reactions

With sodium hydroxide in tetrahydrofuran; water

18 h; Ambient temperature;

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

987 Synthesize Find similar

B: 76%

With sodium hydroxide in tetrahydrofuran; water

18 h; Ambient temperature;

Rx-ID: 2827392 Find similar reactions

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic

Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

988 Synthesize Find similar B: 89%

Rx-ID: 2839330 Find similar reactions

With sodium hydroxide in tetrahydrofuran; water

18 h; Ambient temperature;

Ramage, Robert; Griffiths, Gareth J.; Shutt, Fiona E.; Sweeney, John N. A.

Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1531 - 1537 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

989 Synthesize Find similar

Synthesize Find similar

Rx-ID: 3310071 Find similar reactions

A: 3% B: 55% C: 10%

in acetonitrile

Irradiationdifferent amount of reagent; MechanismProduct distribution;

Smith, David W.; Pienta, Norbert J.

Tetrahedron Letters, 1984 , vol. 25, # 9 p. 915 - 918 Title/Abstract Full Text View citing articles Show Details

A: 3% B: 55% C: 10%

in acetonitrile

Irradiation;

Smith, David W.; Pienta, Norbert J.

Tetrahedron Letters, 1984 , vol. 25, # 9 p. 915 - 918 Title/Abstract Full Text View citing articles Show Details

A: 4% B: 43% C: 15%

in acetonitrile

Irradiation;

Smith, David W.; Pienta, Norbert J.

Tetrahedron Letters, 1984 , vol. 25, # 9 p. 915 - 918 Title/Abstract Full Text View citing articles Show Details

Synthesize Find similar

990 Synthesize Find similar

Synthesize Find similar

Gas phase. Determ. by ICR spect.; Equilibrium constantThermodynamic data;

Rx-ID: 3535140 Find similar reactions

Bouchoux, G.; Houriet, R.

Tetrahedron Letters, 1984 , vol. 25, # 50 p. 5755 - 5758 Title/Abstract Full Text View citing articles Show Details