Reactions (21)
Yield
Substances (29)
Citations (38)
Conditions
References
1
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Rx-ID: 175402
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99%
With borane-ammonia complex in methanol; water
T=20°C; 0.0833333 h;
Goeksu, Haydar; Ho, Sally Fae; Metin, Oender; Korkmaz, Katip; Mendoza Garcia, Adriana; Gueltekin, Mehmet Serdar; Sun, Shouheng
ACS Catalysis, 2014 , vol. 4, # 6 p. 1777 - 1782 Title/Abstract Full Text View citing articles Show Details
99%
With ammonia borane; Pd/MIL-101 in methanol; water
T=20°C; 0.025 h;
Yang, Qihao; Chen, Yu-Zhen; Wang, Zhiyong U.; Xu, Qiang; Jiang, Hai-Long
Chemical Communications, 2015 , vol. 51, # 52 p. 10419 - 10422 Title/Abstract Full Text View citing articles Show Details
99%
With sodium tetrahydroborate in methanol; water
T=20°C; 0.0666667 h; Sealed tubeGreen chemistry;
Göksu, Haydar
New Journal of Chemistry, 2015 , vol. 39, # 11 p. 8498 - 8504 Title/Abstract Full Text View citing articles Show Details
94%
With poly(p-aminostyrene)-palladium(II); hydrogen in N,N-dimethyl-formamide
T=70°C; P=760 Torr; 6 h;
Mukherjee, Debkumar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 2 p. 346 - 352 Title/Abstract Full Text View citing articles Show Details
93%
With Pd2(Bnpy)2(OAc)2; hydrogen in N,N-dimethyl-formamide
Bose, Asish; Saha, C. R.
T=75°C; P=86256.8 Torr; 5 h; var. organic nitro compounds, alkenes, alkynes, aldehydes, ketones, schiff bases and nitriles; other reaction times, temperatures and pressures; MechanismKineticsProduct distribution;
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1990 , vol. 29, # 5 p. 461 - 469 Title/Abstract Full Text Show Details
85%
With formic acid
T=120°C; 0.1 h; Microwave irradiation;
Arya, Kapil; Dandia, Anshu
Journal of the Korean Chemical Society, 2010 , vol. 54, # 1 p. 55 - 58 Title/Abstract Full Text View citing articles Show Details
45%
With ammonium formate; zinc in methanol
T=20°C; 0.0333333 h;
Gowda, D. Channe; Mahesh, B.; Gowda, Shankare
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2001 , vol. 40, # 1 p. 75 - 77 Title/Abstract Full Text Show Details
With hydrogenchloride; iron
T=100°C;
Johnson; Degering
Journal of the American Chemical Society, 1939 , vol. 61, p. 3194 Full Text View citing articles Show Details
With methanol; nickel
T=40 - 50°C; Hydrogenation.unter Druck;
Johnson; Degering
Journal of the American Chemical Society, 1939 , vol. 61, p. 3194 Full Text View citing articles Show Details
With ethanol; nickel
T=40 - 50°C; Hydrogenation.unter Druck;
Johnson; Degering
Journal of the American Chemical Society, 1939 , vol. 61, p. 3194 Full Text View citing articles Show Details
With sodium hydrogensulfite
Aloy; Rabaut
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 654 Full Text Show Details
With tin(ll) chloride
Hoffmann; Meyer,V.
Chemische Berichte, 1891 , vol. 24, p. 3531 Full Text Show Details
With sulfuric acid
T=70 - 75°C; durch elektrolytische Reduktion;
Pierron
Bulletin de la Societe Chimique de France, 1899 , vol. <3>21, p. 783 Full Text Show Details
With hydrogen; nickel
T=320 - 340°C;
Mailhe; Bellegarde
Bulletin de la Societe Chimique de France, 1919 , vol. <4>25, p. 590 Full Text Show Details
With hydrogen; palladium
Saizew
Journal fuer Praktische Chemie (Leipzig), 1872 , vol. <2> 6, p. 131 Full Text Show Details
With sodium hypophosphite; ethanol; copper
Mailhe; Murat
Bulletin de la Societe Chimique de France, 1910 , vol. <4>7, p. 955 Full Text Show Details
durch Einw. von gaerender Hefe;
Neuberg; Welde
Biochemische Zeitschrift, 1914 , vol. 62, p. 480 Full Text Show Details
With hydrogen; nickel
T=150 - 180°C;
Aloy; Rabaut
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 654 Full Text Show Details
With hydrogenchloride; iron
T=50 - 60°C;
Krause
Chemiker-Zeitung, Chemische Apparatur, 1916 , vol. 40, p. 810 Full Text Show Details
Reduktion durch gaerende Hefe;
Neuberg; Welde
Biochemische Zeitschrift, 1914 , vol. 62, p. 480 Full Text Show Details
With hydrazinium monoformate; nickel in methanol
T=20°C; 0.0333333 h;
Gowda, Shankare; Gowda, D.Channe
Tetrahedron, 2002 , vol. 58, # 11 p. 2211 - 2213 Title/Abstract Full Text View citing articles Show Details
With hydrogen in tetrahydrofuran
T=20°C; P=760.051 Torr; 4.5 h;
Kantam, M. Lakshmi; Chakravarti, Rajashree; Pal, Ujjwal; Sreedhar; Bhargava, Suresh
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 6 p. 822 - 827 Title/Abstract Full Text View citing articles Show Details
With nickel; hydrazine in water
T=20°C; 1 h; chemoselective reaction;
Rai, Rohit K.; Mahata, Arup; Mukhopadhyay, Sushobhan; Gupta, Sampa; Li, Pei-Zhou; Nguyen, Kim T.; Zhao, Yanli; Pathak, Biswarup; Singh, Sanjay K.
Inorganic Chemistry, 2014 , vol. 53, # 6 p. 2904 - 2909 Title/Abstract Full Text View citing articles Show Details
100 %Chromat.
With hydrazine hydrate
T=85°C; 1 h;
Li, Yang; Zhou, Yu-Xiao; Ma, Xiao; Jiang, Hai-Long
Chemical Communications, 2016 , vol. 52, # 22 p. 4199 - 4202 Title/Abstract Full Text View citing articles Show Details
95 %Chromat.
With borane-ammonia complex in methanol; water
T=20°C; 2 h; Sonication; chemoselective reaction;
Ma, Xiao; Zhou, Yu-Xiao; Liu, Hang; Li, Yang; Jiang, Hai-Long
Chemical Communications, 2016 , vol. 52, # 49 p. 7719 - 7722 Title/Abstract Full Text View citing articles Show Details
92 %Spectr.
2
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Rx-ID: 233860
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With hydrogenchloride; iron
Foerster; Jungers
Zeitschrift fuer Physikalische Chemie, Abteilung B: Chemie der Elementarprozesse, Aufbau der Materie, 1937 , vol. 36, p. 390 Phys.Z., 1937 , vol. 38, p. 140 Full Text Show Details
Noether
Journal of Chemical Physics, 1942 , vol. 10, p. 664 Full Text View citing articles Show Details
With palladium 10 on activated carbon; hydrogen in methanol
T=20°C; 16 h; Hide Experimental Procedure
Suzhou Zelgen Biopharmaceutical Co., Ltd.; GAO, Xiaoyong; FENG, Weidong; DAI, Xiaojun
Patent: EP2548859 A1, 2013 ; Location in patent: Paragraph 0057; 0059 ; Title/Abstract Full Text Show Details
Deuterated nitromethane (0.64 g, 10.0mmol) was dissolved in methanol (25.0 mL). Pd/C (10percent, 0.1g) was added. H2 replacement was conducted for three times through balloon. At the room temperature, the mixture was stirred for 16 hours. The mixture was acidified by dropping hydrochloric acid, and filtered. The solvent in the filtrate was removed under reduced pressure to afford the title compound (0.60g) as a light yellow product. The result of NMR indicated that (methyl-d3)amine hydrochloride was obtained.
3
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Rx-ID: 34915527
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Stage #1: With palladium 10 on activated carbon; hydrogen in methanol
T=20°C; 16 h; Stage #2: With hydrogenchloride in methanol; water
Suzhou Zelgen Biopharmaceutical Co., Ltd.; GAO, Xiaoyong; FENG, Weidong; DAI, Xiaojun
Patent: EP2548859 A1, 2013 ; Location in patent: Paragraph 0057; 0059 ;
Hide Experimental Procedure
Title/Abstract Full Text Show Details
3.2:2. (Methyl-d3)amine hydrochloride
Deuterated nitromethane (0.64 g, 10.0mmol) was dissolved in methanol (25.0 mL). Pd/C (10percent, 0.1g) was added. H2 replacement was conducted for three times through balloon. At the room temperature, the mixture was stirred for 16 hours. The mixture was acidified by dropping hydrochloric acid, and filtered. The solvent in the filtrate was removed under reduced pressure to afford the title compound (0.60g) as a light yellow product. The result of NMR indicated that (methyl-d3)amine hydrochloride was obtained. 1H NMR (DMSO-d , 400 MHz): δ 8.05 (br, 2H) 6
4
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Rx-ID: 25697997
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With iron; acetic acid in ethanol
Heating / reflux;
THE WALTER AND ELIZA HALL INSTITUTE OF MEDICAL RESEARCH
Patent: US2007/99917 A1, 2007 ; Location in patent: Page/Page column 6 ; Title/Abstract Full Text Show Details
5
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Rx-ID: 24291383
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SCHILL + SEILACHER "STRUKTOL" AKTIENGESELLSCHAFT
Patent: WO2006/84489 A1, 2006 ; Location in patent: Page/Page column 5 ; Title/Abstract Full Text Show Details
6
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Rx-ID: 8551704
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80%
Stage #1: With hydrazine hydrate; zinc in methanol
T=20°C; 0.0666667 h; Stage #2: With hydrogenchloride
Gowda, Shankare; Gowda, D. Channe
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 1 p. 180 - 183 Title/Abstract Full Text View citing articles Show Details
75%
With hydrogenchloride; zinc; hydrazinium monoformate in water
0.0416667 h;
Gowda, Shankare; Gowda, B. K. Kempe; Gowda, D. Channe
Synthetic Communications, 2003 , vol. 33, # 2 p. 281 - 289 Title/Abstract Full Text View citing articles Show Details
45%
Stage #1: With formic acid; nickel in methanol
T=20°C; Reduction; 0.0833333 h; Stage #2: With hydrogenchloride
Addition;
Channe Gowda; Prakasha Gowda; Ramesha Baba; Gowda, Shankare
Synthetic Communications, 2000 , vol. 30, # 16 p. 2889 - 2895 Title/Abstract Full Text View citing articles Show Details
7
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Rx-ID: 22884880
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Warner-Lambert Company
Patent: US6344459 B1, 2002 ; Location in patent: Page column 31 ; Title/Abstract Full Text Show Details
8
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Rx-ID: 27152506
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75%
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Okeya, Seichi; Hashimoto, Masato; Nakamura, Fumiko; Kusuyama, Yoshiaki; Kobayashi, Mako; Arakawa, Ryuichi
Chemistry Letters, 2000 , # 10 p. 1130 - 1131 Title/Abstract Full Text View citing articles Show Details
in nitromethane
Pt complex dissolved in MeNO2; elem. anal.;
9
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Rx-ID: 233861
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With water-d2; deuterium; palladium on activated charcoal
P=4137.2 Torr;
Arduengo III, Anthony J.; Dias, H. V. Rasika; Dixon, David A.; Harlow, Richard L.; Klooster; Koetzle
Journal of the American Chemical Society, 1994 , vol. 116, # 15 p. 6812 - 6822 Title/Abstract Full Text View citing articles Show Details
With water-d2; DCl; palladium; deuterium
Leitch et al.
Canadian Journal of Research, Section B: Chemical Sciences, 1950 , vol. 28, p. 256,262 Org.Synth.Isotopes, 1958 , p. 1418 Full Text Show Details
A
B
C
D
E
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10
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Rx-ID: 1608712
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E: 80%
2 h at -5 deg C, then 5 h at 30 deg C; Product distributionMechanism;
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Voronkov, M. G.; Dubinskaya, E. I.; Sigalov, M. V.; Vitkovskii, V. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 5.1 p. 1055 - 1057,932 - 933
Title/Abstract Full Text Show Details
A
B
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11
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T=10 - 12°C; electroreduction; electrolyte: 2.82N HCl, electrode: copper hydrophobized with 5percent fluororesin 4D, E=-0.8 V (ref. electrode: normal calomel); effect of the hydrophobizer content of the electrode and working potential on the current yields and densi;
Kornienko, G. V.; Kornienko, V. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 8 p. 1771 - 1776,1590 - 1594 Title/Abstract Full Text Show Details
With hydrogenchloride; tin(ll) chloride
Hoffmann; Meyer,V.
Chemische Berichte, 1891 , vol. 24, p. 3531 Full Text Show Details
12
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Rx-ID: 7063888
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Samuelsen et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3872 Full Text View citing articles Show Details
an verschiedenen praeparierten Katalysatoren.Hydrogenation;
A
B
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13
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Rx-ID: 7063909
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Isgaryschew; Petrowa
Zhurnal Fizicheskoi Khimii, 1950 , vol. 24, p. 745 Chem.Abstr., 1950 , p. 10551 Full Text Show Details
T=15 - 80°C; Elektrochemische Reduktion an verschiedenen Metall-Kathoden, verschiedener Stromdichte und verschiedener Konzentration;
A
B
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14
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Rx-ID: 7063910
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T=15 - 80°C; Elektrochemische Reduktion an verschiedenen Metall-Kathoden, verschiedener Stromdichte und verschiedener Konzentration;
A
B
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Isgaryschew; Petrowa
Zhurnal Fizicheskoi Khimii, 1950 , vol. 24, p. 745 Chem.Abstr., 1950 , p. 10551 Full Text Show Details
15
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Melnikow
Zhurnal Obshchei Khimii, 1934 , vol. 4, p. 1057,1058 Chem. Zentralbl., 1936 , vol. 107, # I p. 3131 Full Text Show Details
Produkt5-6:Wasserstoff,Ammoniak;
A
16
B
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Mailhe; Bellegarde
Bulletin de la Societe Chimique de France, 1919 , vol. <4>25, p. 590 Full Text Show Details
T=320 - 340°C;
17
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Rx-ID: 7063873
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Krause
Chemiker-Zeitung, Chemische Apparatur, 1916 , vol. 40, p. 810 Full Text Show Details
18
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Rx-ID: 7063879
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Mailhe; Murat
Bulletin de la Societe Chimique de France, 1910 , vol. <4>7, p. 955 Full Text Show Details
19
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Rx-ID: 7063890
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Aloy; Rabaut
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 654 Full Text Show Details
20
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Rx-ID: 7063883
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Hoffmann; Meyer,V.
Chemische Berichte, 1891 , vol. 24, p. 3531 Full Text Show Details
T=150 - 180°C;
A
B
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21
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Hoffmann; Meyer,V.
Chemische Berichte, 1891 , vol. 24, p. 3531 Full Text Show Details