Ethyl trifluoroacetate [C4H5F3O2] by Asch

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CAS Registry Number: 383-63-1 Chemical Name: ethyl trifluoroacetate,; trifluoroacetic acid ethyl ester Linear Structure Formula: CH3CH2OCOCF3 Molecular Formula: C4H5F3O2 Molecular Weight: 142.078 Type of Substance: acyclic InChI Key: STSCVKRWJPWALQ-UHFFFAOYSA-N Note:

O F O

Substance Label (73) Label References 2

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CF3COOEt

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EtOCOCF3

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14h

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CF&3%COOEt

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CF&3%CO&2%Et

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EtTFA

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S7A

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Intermediate 62

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F3CCOOEt

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2a; CF&3%COOEt

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ETFA

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K-0

Patent; GRUeNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; FRORMANN, Sven; LESCH, Bernhard; LEE, Jeewoo; KIM, Yong-Soo; KIM, Myeong-Seop; WO2010/127855; (2010); (A1) English, View in Reaxys; Patent; GRUeNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; FRORMANN, Sven; LESCH, Bernhard; LEE, Jeewoo; KIM, Yong-Soo; KIM, Myeon-Seop; WO2010/127856; (2010); (A1) English, View in Reaxys; Patent; Gruenenthal GmbH; US2012/46301; (2012); (A1) English, View in Reaxys; Patent; Gruenenthal GmbH; US2012/115893; (2012); (A1) English, View in Reaxys; Patent; Gruenenthal GmbH; US2012/115903; (2012); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; WO2013/13815; (2013); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo; WO2013/68461; (2013); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo; WO2013/68462; (2013); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo; WO2013/68467; (2013); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek, John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo; WO2013/68463; (2013); (A1) English, View in Reaxys; Patent; GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; DAMANN, Nils; LESCH, Bernhard; BAHRENBERG, Gregor; SAUNDERS, Derek John; STOCKHAUSEN, Hannelore; KIM, Yong-Soo; KIM, Myeong-Seop; LEE, Jeewoo; WO2013/68464; (2013); (A1) English, View in Reaxys

CF&3%COOC&2 %H&5%

Kinoshita, Yusuke; Kunieda, Michio; Mikata, Yuji; Tamiaki, Hitoshi; Tetrahedron Letters; vol. 54; nb. 10; (2013); p. 1243 - 1246, View in Reaxys

A; K-0

Patent; Gruenenthal GmbH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo; US2013/29962; (2013); (A1) English, View in Reaxys

for 57

Nack, William A.; He, Gang; Zhang, Shu-Yu; Lu, Chengxi; Chen, Gong; Organic Letters; vol. 15; nb. 13; (2013); p. 3440 - 3443, View in Reaxys

Park, Hea Jung; Kim, Ji Na; Yoo, Hyun-Ji; Wee, Kyung-Ryang; Kang, Sang Ook; Cho, Dae Won; Yoon, Ung Chan; Journal of Organic Chemistry; vol. 78; nb. 16; (2013); p. 8054 - 8064, View in Reaxys

A-4

Patent; Boivin, Roch; Carlson, Eric; Endo, Atsushi; Hansen, Hans; Hawkins, Lynn D.; Ishizaka, Sally; Mackey, Matthew; Narayan, Sridhar; Satoh, Takashi; Schiller, Shawn; US2013/324547; (2013); (A1) English, View in Reaxys

Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi; Chemistry - A European Journal; vol. 19; nb. 52; (2013); p. 17692 - 17697, View in Reaxys

18b

Patent; Connolly, Peter J.; Macielag, Mark J.; Zhu, Bin; US2012/58986; (2012); (A1) English, View in Reaxys; Patent; Connolly, Peter J.; Macielag, Mark J.; McDonnell, Mark E.; Zhu, Bin; US2012/77797; (2012); (A1) English, View in Reaxys

Patent; ENZON PHARMACEUTICALS, INC.; Zhao, Hong; Yan, Weili; Shi, Lianjun; Royzen, Maksim; WU, Dechun; WO2010/57155; (2010); (A1) English, View in Reaxys

III

Patent; AUROBINDO PHARMA LIMITED; AMBATI, V Raghava Reddy; GARAGA, Srinivas; MALLELA, Sambhu Prasad Sarma; MEENAKSHISUNDERAM, Sivakumaran; WO2010/95024; (2010); (A2) English, View in Reaxys

Patent; APATH, LLC; SLOMCZYNSKA, Urszula; OLIVO, Paul; BEATTIE, Jodi; STARKEY, Gale; NOUEIRY, Amine; ROTH, Robert; WO2010/96115; (2010); (A1) English, View in Reaxys

educt to 10

Zhao, Peng; Yang, Zhen-Jun; Zhang, Liang-Ren; Zhang, Li-He; Tetrahedron Letters; vol. 49; nb. 18; (2008); p. 2951 - 2955, View in Reaxys

F3CCO2Et

Bobkov, Georgii V.; Mikhailov, Sergey N.; Van Aerschot, Arthur; Herdewijn, Piet; Tetrahedron; vol. 64; nb. 27; (2008); p. 6238 - 6251, View in Reaxys

CF3CO2Et

Brown-Proctor; Sherman; Kilbourn; Journal of Labelled Compounds and Radiopharmaceuticals; vol. 42; nb. SUPPL. 1; (1999); p. S632-S634, View in Reaxys; Sakai, Atsushi; Bakke, Mikio; Ohta, Hiromichi; Kosugi, Hiroshi; Sugai, Takeshi; Chemistry Letters; nb. 11; (1999); p. 1255 - 1256, View in Reaxys; Gruselle, Michel; Malezieux, Bernard; Andres, Roman; Amouri, Hani; Vaissermann, Jacqueline; Melikyan, Gagik G.; European Journal of Inorganic Chemistry; nb. 2; (2000); p. 359 - 368, View in Reaxys; Miura, Katsukiyo; Hondo, Takeshi; Nakagawa, Takahiro; Takahashi, Tatsuyuki; Hosomi, Akira; Organic Letters; vol. 2; nb. 3; (2000); p. 385 - 388, View in Reaxys; Maxwell,

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ed. to 1. interm. to 6

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CF3COOC2H5

Haiss, Peter; Zeller, Klaus-Peter; Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences; vol. 58; nb. 6; (2003); p. 595 - 605, View in Reaxys; Azam, A. T. M. Zafrul; Moriguchi, Tomohisa; Shinozuka, Kazuo; Chemical Communications; nb. 3; (2006); p. 335 - 337, View in Reaxys

Hickey, Matthew R.; Nelson, Todd D.; Secord, Elizabeth A.; Allwein, Shawn P.; Kress, Michael H.; Synlett; nb. 2; (2005); p. 255 - 258; Art.No: S09004ST, View in Reaxys

R1CO2R4 for Hpz4 Montoya, Vanessa; Pons, Josefina; Branchadell, Vicenc; Ros, Josep; Tetrahedron; vol. 61; nb. 52; (2005); p. 12377 12385, View in Reaxys CF3-CO2Et

Sosnovskikh; Usachev; Blinov; Kodess; Mendeleev Communications; vol. 11; nb. 1; (2001); p. 36 - 38, View in Reaxys; Usachev, Boris I.; Sosnovskikh, Vyacheslav Ya.; Journal of Fluorine Chemistry; vol. 125; nb. 9; (2004); p. 1393 - 1395, View in Reaxys

EtOTFA

Yang, Wen; Giandomenico, Christen M.; Sartori, Michael; Moore, Dennis A.; Tetrahedron Letters; vol. 44; nb. 12; (2003); p. 2481 - 2483, View in Reaxys; Allwein, Shawn P.; Secord, Elizabeth A.; Martins, Andrew; Mitten, Jeffrey V.; Nelson, Todd D.; Kress, Michael H.; Dolling, Ulf H.; Synlett; nb. 14; (2004); p. 2489 - 2492, View in Reaxys

IIe

Vasil'eva; Sevenard; Khomutov; Kuznetsova; Russian Journal of Organic Chemistry; vol. 40; nb. 6; (2004); p. 874 878, View in Reaxys

2, R=CF3

Singh, Sunil Kumar; Vobbalareddy, Saibaba; Kalleda, Srinivasa Rao; Rajjak, Shaikh Abdul; Casturi, Seshagiri Rao; Datla, Srinivasa Raju; Mamidi, Rao N.V.S.; Mullangi, Ramesh; Bhamidipati, Ravikanth; Ramanujam, Rajagopalan; Akella, Venkateswarlu; Yeleswarapu, Koteswar Rao; Organic and Biomolecular Chemistry; vol. 2; nb. 17; (2004); p. 2442 - 2450, View in Reaxys

Copyright ÂŠ 2018 Elsevier Life Sciences IP Limited except certain content provided by third parties. Reaxys is a trademark of Elsevier Life Sciences IP Limited.

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CF3C(O)OEt

Andre, Joao P.; Geraldes, Carlos F. G. C.; Martins, Jose A.; Merbach, Andre E.; Prata, Maria I. M.; Santos, Ana C.; De Lima, Joao J. P.; Toth, Eva; Chemistry - A European Journal; vol. 10; nb. 22; (2004); p. 5804 - 5816, View in Reaxys

CF2CO2Et

Kojima; Bruice; Organic letters; vol. 2; nb. 1; (2000); p. 81 - 84, View in Reaxys; Jaunzems, Janis; Oelze, Benjamin; Kirschning, Andreas; Organic and Biomolecular Chemistry; vol. 2; nb. 23; (2004); p. 3448 - 3456, View in Reaxys

CF3COEt

Croxtal, Ben; Fawcett, John; Hope, Eric G.; Journal of Fluorine Chemistry; vol. 119; nb. 1; (2003); p. 65 - 73, View in Reaxys

Asseline, Ulysse; Chassignol, Marcel; Draus, Jolanta; Durand, Maurice; Maurizot, Jean-Claude; Bioorganic and Medicinal Chemistry; vol. 11; nb. 16; (2003); p. 3499 - 3511, View in Reaxys

ester for 6d

Reznikov; Skuridin; Khromovskikh; Khramtsov; Russian Chemical Bulletin; vol. 52; nb. 9; (2003); p. 2052 - 2056, View in Reaxys

Rf1CO2Et, Rf1=CF3

Legros, Julien; Crousse, Benoit; Bonnet-Delpon, Daniele; Begue, Jean-Pierre; Tetrahedron; vol. 58; nb. 20; (2002); p. 3993 - 3998, View in Reaxys

Krasutsky, Pavel A.; Kolomitsyn, Igor V.; Botov, Evgenij M.; Carlson, Robert M.; Semenova, Irina G.; Fokin, Andrey A.; Tetrahedron Letters; vol. 43; nb. 48; (2002); p. 8687 - 8691, View in Reaxys

R(F)CO2Et, a R=CF3

Sosnovskikh; Usachev; Sizov; Russian Chemical Bulletin; vol. 51; nb. 11; (2002); p. 2109 - 2115, View in Reaxys

table 2, entry 6

Liu, Andrew Man Fai; Somers, Neil A.; Kazlauskas, Romas J.; Brush, Terry S.; Zocher, Frank; Enzelberger, Markus M.; Bornscheuer, Uwe T.; Horsman, Geoff P.; Mezzetti, Alessandra; Schmidt-Dannert, Claudia; Schmid, Rolf D.; Tetrahedron Asymmetry; vol. 12; nb. 4; (2001); p. 545 - 556, View in Reaxys

EtO2CCF3

Singh, Shiv P.; Kumar, Dalip; Jones, Brian G.; Threadgill, Michael D.; Journal of Fluorine Chemistry; vol. 94; nb. 2; (1999); p. 199 - 203, View in Reaxys; Garrett, Shane W.; Davies, Owen R.; Milroy, David A.; Wood, Pauline J.; Pouton, Colin W.; Threadgill, Michael D.; Bioorganic and Medicinal Chemistry; vol. 8; nb. 7; (2000); p. 1779 - 1797, View in Reaxys; Wender; Jessop; Pattabiraman; Pelkey; VanDeusen; Organic letters; vol. 3; nb. 21; (2001); p. 3229 3232, View in Reaxys

CF3CO2Et (educt to 8)

Morita, Chikanori; Hashimoto, Kimiko; Okuno, Toshikatsu; Shirahama, Haruhisa; Heterocycles; vol. 52; nb. 3; (2000); p. 1163 - 1169, View in Reaxys

educt, row 7

Clavel, Philippe; Biran, Claude; Bordeau, Michel; Roques, Nicolas; Trevinc, Stephane; Tetrahedron Letters; vol. 41; nb. 45; (2000); p. 8763 - 8767, View in Reaxys

Konno; Ishihara; Yamanaka; Tetrahedron Letters; vol. 41; nb. 44; (2000); p. 8467 - 8472, View in Reaxys

educt to 6

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Uneyama, Kenji; Mizutani, Go; Maeda, Kazushige; Kato, Tsuyoshi; Journal of Organic Chemistry; vol. 64; nb. 18; (1999); p. 6717 - 6723, View in Reaxys

Uneyama, Kenji; Mizutani, Go; Chemical Communications; nb. 7; (1999); p. 613 - 614, View in Reaxys

CF3CO2CH2CH3

Wright, Dennis L.; McMills, Mark C.; Organic Letters; vol. 1; nb. 4; (1999); p. 667 - 670, View in Reaxys

Pashkevich; Khomutov; Sevenard; Russian Journal of Organic Chemistry; vol. 34; nb. 12; (1998); p. 1727 - 1730, View in Reaxys

CF3CO2C2H5

Kuhn, David G.; Kamhi, Victor M.; Furch, Joseph A.; Diehl, Robert E.; Lowen, Gregory T.; Kameswaran, Venkataraman; Pesticide Science; vol. 41; nb. 3; (1994); p. 279 - 286, View in Reaxys

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Patent; Hebei Normal University; Liu, Qingbin; Wang, Zheng; Liu, Bo; Zhang, Fujun; (11 pag.); CN105237342; (2016); (A) Chinese, View in Reaxys Page/Page column

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Page/Page column

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Druglikeness (1) 1 of 1

LogP

1.363

H Bond Donors

H Bond Acceptors

Rotatable Bonds

TPSA

26.3

Lipinski Number

Veber Number

Melting Point (1) 1 of 1

Melting Point [°C]

-78.16

Lu, Wei; Xie, Kai; Pan, Yi; Chen, Zhong-Xue; Zheng, Chun-Man; Journal of Fluorine Chemistry; vol. 156; (2013); p. 136 143, View in Reaxys Boiling Point (20) Boiling Point [°C]

Pressure (Boiling Point) [Torr]

References

61.84

Lu, Wei; Xie, Kai; Pan, Yi; Chen, Zhong-Xue; Zheng, Chun-Man; Journal of Fluorine Chemistry; vol. 156; (2013); p. 136 - 143, View in Reaxys

60 - 62

Ishikawa et al.; Nippon Kagaku Kaishi; (1975); p. 1541,1543, View in Reaxys; Yuan, Chengye; Li, Jinfeng; Zhang, Wenchi; Journal of Fluorine Chemistry; vol. 127; nb. 1; (2006); p. 44 - 47, View in Reaxys

53 - 54

Forbus, T. R.; Taylor, S. L.; Martin, J. C.; Journal of Organic Chemistry; vol. 52; nb. 19; (1987); p. 4156 - 4159, View in Reaxys

72 - 74

Konovalova, I. V.; Ofitserov, E. N.; Mironov, V. F.; Kostyuk, V. I.; Pudovik, A. N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 53; nb. 9; (1983); p. 1945 - 1950,1754 - 1758, View in Reaxys

Bock,E. et al.; Canadian Journal of Chemistry; vol. 52; (1974); p. 3113 - 3118, View in Reaxys; Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys; Belen'kii et al.; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); (1968); p. 1541; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; (1968); p. 1631; Chem.Abstr.; vol. 70; nb. 3218h; (1969), View in Reaxys; Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 52; nb. 12; (1982); p. 2724 - 2728,2402 - 2405, View in Reaxys

55 - 57

Hagen, Arnulf P.; Miller, Tammy S.; Bynum, Richard L.; Kapila Ved P.; Journal of Organic Chemistry; vol. 47; nb. 7; (1982); p. 1345 - 1347, View in Reaxys

59 - 62

760

54 82

Downie, Ian M.; Wynne, Neil; Harrison, Stephen; Tetrahedron; vol. 38; nb. 10; (1982); p. 1457 - 1458, View in Reaxys Fokin, A. V.; Studnev, Yu. N.; Ragulin, L. I.; Krotovich, I. N.; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); vol. 31; (1982); p. 1696 1698; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; nb. 8; (1982); p. 1906 - 1907, View in Reaxys

Olah,G.A.; Nishimura,J.; Journal of the American Chemical Society; vol. 96; (1974); p. 2214 2220, View in Reaxys Golovanov et al.; J. Gen. Chem. USSR (Engl. Transl.); vol. 43; (1973); p. 2666,2644,2646, View in Reaxys

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102 - 104 59

Dyatkin,B.L. et al.; Journal of Organometallic Chemistry; vol. 57; (1973); p. 423 - 433, View in Reaxys 760

60 55

Barnes et al.; Canadian Journal of Chemistry; vol. 50; (1972); p. 2175,2176-2178, View in Reaxys Patent; Coll; Luis; DE1966974; (1969); Chem.Abstr.; vol. 85; nb. 5203, View in Reaxys

760

59.5 - 60.5

Ginsburg,V.A.; Vasil'eva,M.N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 37; (1967); p. 2493 2497,2371 - 2374, View in Reaxys Sarubinskii et al.; J. Gen. Chem. USSR (Engl. Transl.); vol. 35; (1965); p. 1620,1624, View in Reaxys

61.6

760

Macey; Journal of Physical Chemistry; vol. 64; (1960); p. 254,255, View in Reaxys

61.3

750

Moffat; Hunt; Journal of the American Chemical Society; vol. 79; (1957); p. 54, View in Reaxys

60.7

740

Gorin et al.; Journal of the American Chemical Society; vol. 75; (1953); p. 5622,5624, View in Reaxys

60.5 61.7

Henne et al.; Journal of the American Chemical Society; vol. 69; (1947); p. 1819, View in Reaxys 761

Swarts; Bulletin de la Classe des Sciences, Academie Royale de Belgique; vol. <5>8; (1922); p. 346; Bulletin des Societes Chimiques Belges; vol. 32; (1923); p. 104; Chem. Zentralbl.; vol. 94; nb. I; (1923); p. 66, View in Reaxys

Refractive Index (15) Refractive Index Wavelength (ReTemperature (Refractive Index) [nm] fractive Index) [°C]

References

1.305

589

Konovalova, I. V.; Ofitserov, E. N.; Mironov, V. F.; Kostyuk, V. I.; Pudovik, A. N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 53; nb. 9; (1983); p. 1945 - 1950,1754 - 1758, View in Reaxys

1.3045

589

Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 52; nb. 12; (1982); p. 2724 - 2728,2402 - 2405, View in Reaxys

1.3083

589

Laato; Acta Chemica Scandinavica (1947-1973); vol. 21; (1967); p. 2119,2123,2129, View in Reaxys

1.3115

589

Ginsburg,V.A.; Vasil'eva,M.N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 37; (1967); p. 2493 - 2497,2371 - 2374, View in Reaxys

1.308

589

Tal'vik; Organic Reactivity (New York, English Translation); vol. 3-4; (1966); p. 101,103, View in Reaxys

1.30657

589

Macey; Journal of Physical Chemistry; vol. 64; (1960); p. 254,255, View in Reaxys

1.30527

646.3

Macey; Journal of Physical Chemistry; vol. 64; (1960); p. 254,255, View in Reaxys

1.31

486.1

Macey; Journal of Physical Chemistry; vol. 64; (1960); p. 254,255, View in Reaxys

1.30725

589

Moffat; Hunt; Journal of the American Chemical Society; vol. 79; (1957); p. 54, View in Reaxys

1.30735

589

Gorin et al.; Journal of the American Chemical Society; vol. 75; (1953); p. 5622,5624, View in Reaxys

1.3072

589

Bender; Journal of the American Chemical Society; vol. 75; (1953); p. 5986,5988, View in Reaxys

1.3093

589

Henne et al.; Journal of the American Chemical Society; vol. 69; (1947); p. 1819, View in Reaxys

1.3078

656.3

16.7

1.3124

486.1

16.7

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1.3153

434

16.7

Density (10) 1 of 10

Density [g·cm-3]

1.1913

Reference Temperature [°C]

Measurement Temperature 20 [°C] Gazizov, T. Kh.; Belyalov, R. U.; Pudovik, A. N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 52; nb. 12; (1982); p. 2724 2728,2402 - 2405, View in Reaxys 2 of 10

Density [g·cm-3]

1.17729

Measurement Temperature 25 [°C] Memmi, Abdelmajid; Piekarski, Salomon; Journal of Chemical Research, Miniprint; nb. 4; (1982); p. 1101 - 1120, View in Reaxys 3 of 10

Density [g·cm-3]

1.1621

Reference Temperature [°C]

Measurement Temperature 20 [°C] Ginsburg,V.A.; Vasil'eva,M.N.; J. Gen. Chem. USSR (Engl. Transl.); vol. 37; (1967); p. 2493 - 2497,2371 - 2374, View in Reaxys 4 of 10

Density [g·cm-3]

1.1852

Reference Temperature [°C]

Measurement Temperature 20 [°C] Tal'vik; Organic Reactivity (New York, English Translation); vol. 3-4; (1966); p. 101,103, View in Reaxys 5 of 10

Density [g·cm-3]

1.1908

Reference Temperature [°C]

Measurement Temperature 20 [°C] Macey; Journal of Physical Chemistry; vol. 64; (1960); p. 254,255, View in Reaxys 6 of 10

Density [g·cm-3]

1.167

Reference Temperature [°C]

Measurement Temperature 30 [°C] Rutledge; Smith; Journal of the American Chemical Society; vol. 75; (1953); p. 5762, View in Reaxys 7 of 10

Density [g·cm-3]

1.1466

Reference Temperature [°C]

Measurement Temperature 40 [°C] Rutledge; Smith; Journal of the American Chemical Society; vol. 75; (1953); p. 5762, View in Reaxys 8 of 10

Density [g·cm-3]

1.126

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Reference Temperature [°C]

Measurement Temperature 50 [°C] Rutledge; Smith; Journal of the American Chemical Society; vol. 75; (1953); p. 5762, View in Reaxys 9 of 10

Density [g·cm-3]

1.1905

Reference Temperature [°C]

Measurement Temperature 20 [°C] Desreux; Bulletin des Societes Chimiques Belges; vol. 44; (1935); p. 258, View in Reaxys 10 of 10

Density [g·cm-3]

1.1953

Measurement Temperature 16.7 [°C] Swarts; Bulletin de la Classe des Sciences, Academie Royale de Belgique; vol. <5>8; (1922); p. 346; Bulletin des Societes Chimiques Belges; vol. 32; (1923); p. 104; Chem. Zentralbl.; vol. 94; nb. I; (1923); p. 66, View in Reaxys Association (MCS) (11) 1 of 11

Description (Association (MCS))

Stability constant of the complex with ...

Solvent (Association (MCS))

cyclohexane

Temperature (Association (MCS)) [°C]

19.9

Partner (Association (MCS))

3-(biphenyl-4-yl)-2H-azirine

Naito, Ikuo; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Ishida, Akito; Takamuku, Setsuo; Bulletin of the Chemical Society of Japan; vol. 68; nb. 10; (1995); p. 2905 - 2908, View in Reaxys 2 of 11

Description (Association (MCS))

Stability constant of the complex with ...

Solvent (Association (MCS))

CCl4

Temperature (Association (MCS)) [°C]

Partner (Association (MCS))

4-Fluorophenol

Besseau, Francois; Laurence, Christian; Berthelot, Michel; Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999); nb. 3; (1994); p. 485 - 490, View in Reaxys 3 of 11

Description (Association (MCS))

Association with compound

Solvent (Association (MCS))

CCl4

Temperature (Association (MCS)) [°C]

Partner (Association (MCS))

diisopropyl-2,6-nitro-4-phenol-d1

Laurence, Christian; Berthelot, Michel; Helbert, Maryvonne; Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy; vol. 41; nb. 7; (1985); p. 883 - 892, View in Reaxys 4 of 11

Description (Association (MCS))

Enthalpy of association

Partner (Association (MCS))

methylammonium cation

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Meot-Ner (Mautner), Michael; Journal of the American Chemical Society; vol. 106; nb. 5; (1984); p. 1257 - 1264, View in Reaxys 5 of 11

Description (Association (MCS))

Further physical properties of the complex

Temperature (Association (MCS)) [°C]

Partner (Association (MCS))

cyclohexane

Memmi, Abdelmajid; Piekarski, Salomon; Journal of Chemical Research, Miniprint; nb. 4; (1982); p. 1101 - 1120, View in Reaxys 6 of 11

Description (Association (MCS))

Spectrum of the complex

Smolyanskii et al.; J. Gen. Chem. USSR (Engl. Transl.); vol. 49; (1979); p. 675,586,587, View in Reaxys 7 of 11

Description (Association (MCS))

Stability constant of the complex with ...

Marek et al.; Journal of Applied Spectroscopy; vol. 19; (1973); p. 926; ; p. 130, View in Reaxys 8 of 11

Description (Association (MCS))

Association with compound

Solvent (Association (MCS))

dibutyl ether

Partner (Association (MCS))

lithium butylate

Moffat; Hunt; Journal of the American Chemical Society; vol. 81; (1959); p. 2082,2084, View in Reaxys 9 of 11

Description (Association (MCS))

Association with compound

Solvent (Association (MCS))

dibutyl ether

Partner (Association (MCS))

lithium ethylate

Bender; Journal of the American Chemical Society; vol. 75; (1953); p. 5986,5988, View in Reaxys; Moffat; Hunt; Journal of the American Chemical Society; vol. 81; (1959); p. 2082,2084, View in Reaxys 10 of 11

Description (Association (MCS))

Association with compound

Solvent (Association (MCS))

dibutyl ether

Partner (Association (MCS))

sodium methylate

Bender; Journal of the American Chemical Society; vol. 75; (1953); p. 5986,5988, View in Reaxys 11 of 11

Description (Association (MCS))

Association with compound

Solvent (Association (MCS))

dibutyl ether

Partner (Association (MCS))

sodium ethanolate

Bender; Journal of the American Chemical Society; vol. 75; (1953); p. 5986,5988, View in Reaxys Azeotropes (MCS) (2) 1 of 2

Temperature (Azeotropes (MCS)) [°C]

Azeotropes

ethanol; water

Reid; Journal of the American Chemical Society; vol. 69; (1947); p. 2069, View in Reaxys

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2 of 2

Temperature (Azeotropes (MCS)) [°C]

Azeotropes

ethanol

Fukuhara; Bigelow; Journal of the American Chemical Society; vol. 63; (1941); p. 789, View in Reaxys Conformation (1) Object of Investiga- References tion Conformation

True; Bohn; Journal of the American Chemical Society; vol. 98; (1976); p. 1188,1189-1194, View in Reaxys

Crystal Property Description (1) Colour & Other References Properties yellow

Patent; PFIZER LIMITED; WO2006/64332; (2006); (A1) English, View in Reaxys

Dynamic Viscosity (1) Dynamic Viscosity Temperature (Dy[P] namic Viscosity) [°C] 0.00282 - 0.004342

20 - 60.2

References

Swarts; Journal de Chimie Physique et de Physico-Chimie Biologique; vol. 28; (1931); p. 628, View in Reaxys

Electrical Data (2) 1 of 2

Description (Electrical Da- Relaxation frequency ta) Purokit et al.; Bulletin of the Chemical Society of Japan; vol. 48; (1975); p. 2785, View in Reaxys

2 of 2

Description (Electrical Da- Electrical properties ta) Purohit et al.; Indian Journal of Pure and Applied Physics; vol. 12; (1974); p. 701, View in Reaxys

Electrical Moment (1) 1 of 1

Description (Electrical Moment)

Dipole moment

Bock,E. et al.; Canadian Journal of Chemistry; vol. 52; (1974); p. 3113 - 3118, View in Reaxys; Purokit et al.; Bulletin of the Chemical Society of Japan; vol. 48; (1975); p. 2785, View in Reaxys Electrochemical Behaviour (2) Description (Elec- References trochemical Behaviour) Proton affinity

Wolf,J.F. et al.; Journal of the American Chemical Society; vol. 99; (1977); p. 5417 - 5429, View in Reaxys

Polarography

Gawargious et al.; Analytical Chemistry; vol. 47; (1975); p. 502,503-505, View in Reaxys

Electrochemical Characteristics (2) 1 of 2

Description (Electrochemical Characteristics)

Electrochemical characteristics given

Maekawa, Hirofumi; Ozaki, Taro; Nishiguchi, Ikuzo; Tetrahedron Letters; vol. 51; nb. 5; (2010); p. 796 - 799, View in Reaxys; Maekawa, Hirofumi; Ozaki, Taro; Zulkeflee, Dayana; Murakami, Taro; Kihara, Shin; Nishiguchi, Ikuzo; Synlett; nb. 3; (2012); p. 401 - 404, View in Reaxys 2 of 2

Description (Electrochemical Characteristics)

redox potential

Solvent (Electrochemical Characteristics)

acetonitrile

Comment (Electrochemical Characteristics)

Potential: -2.58 V. No. of transm. electrons: 2. Method: voltammetry. Description: glassy carbon vs SCE

Product

ethyl difluorocarboxylate

Stepanov, Andrei A.; Minyaeva, Tatyana V.; Martynov, Boris I.; Tetrahedron Letters; vol. 40; nb. 11; (1999); p. 2203 - 2204, View in Reaxys Electron Binding (1) Description (Elec- References tron Binding)

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Electronic states

Lu, Wei; Xie, Kai; Pan, Yi; Chen, Zhong-Xue; Zheng, Chun-Man; Journal of Fluorine Chemistry; vol. 156; (2013); p. 136 - 143, View in Reaxys

Further Information (2) Description (FurReferences ther Information) Further information Manatt,S.L.; Journal of the American Chemical Society; vol. 88; (1966); p. 1323 - 1324, View in Reaxys Further information Bellamy,L.J.; Pace,R.J.; Spectrochimica Acta; vol. 19; (1963); p. 1831 - 1839, View in Reaxys Ionization Potential (1) References Sweigart; Turner; Journal of the American Chemical Society; vol. 94; (1972); p. 5599, View in Reaxys; Gelius et al.; Physica Scripta; vol. 2; (1970); p. 70,73, View in Reaxys; Smith; Thomas; Journal of the American Chemical Society; vol. 100; (1978); p. 5459,5461, View in Reaxys Liquid/Liquid Systems (MCS) (1) 1 of 1

Description (Liquid/Liquid Distribution between solvent 1 + 2 Systems (MCS)) Comment (Liquid/Liquid Systems (MCS))

equation

Partner (Liquid/Liquid Systems (MCS))

chloroform

Abraham, Michael H.; Platts, James A.; Hersey, Anne; Leo, Albert J.; Taft, Robert W.; Journal of Pharmaceutical Sciences; vol. 88; nb. 7; (1999); p. 670 - 679, View in Reaxys Other Thermochemical Data (3) Description (Other References Thermochemical Data) Entropy

Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys

Enthalpy

Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys

Thermodynamic properties

Barnes et al.; Canadian Journal of Chemistry; vol. 50; (1972); p. 2175,2176-2178, View in Reaxys

Surface Tension (1) Surface Tension Temperature (Sur[g·s-2] face Tension) [°C]

References

16.76

Desreux; Bulletin des Societes Chimiques Belges; vol. 44; (1935); p. 258, View in Reaxys

Transport Phenomena (MCS) (1) 1 of 1

Description (Transport Phenomena (MCS))

Viscosity

Temperature (Transport Phenomena (MCS)) [°C]

Partner (Transport Phenomena (MCS))

cyclohexane

Memmi, Abdelmajid; Piekarski, Salomon; Journal of Chemical Research, Miniprint; nb. 4; (1982); p. 1101 - 1120, View in Reaxys NMR Spectroscopy (23) 1 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

trifluoroacetic acid

Location

supporting information

Kalman, Steven E.; Munz, Dominik; Fortman, George C.; Boaz, Nicholas C.; Groves, John T.; Gunnoe, T. Brent; Dalton Transactions; vol. 44; nb. 12; (2015); p. 5294 - 5298, View in Reaxys 2 of 23

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

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Nucleus (NMR Spectroscopy)

Coupling Nuclei

Fortman, George C.; Boaz, Nicholas C.; Munz, Dominik; Konnick, Michael M.; Periana, Roy A.; Groves, John T.; Brent Gunnoe; Journal of the American Chemical Society; vol. 136; nb. 23; (2014); p. 8393 - 8401, View in Reaxys 3 of 23

Description (NMR Spectroscopy)

Chemical shifts; Spectrum

Nucleus (NMR Spectroscopy)

Frequency (NMR Spectro- 400.2 scopy) [MHz] Location

supporting information

Maricich, Tom J.; Allan, Matthew J.; Kislin, Brett S.; Chen, Andrea I-T.; Meng, Fan-Chun; Bradford, Christine; Kuan, Nai-Chia; Wood, Jeremy; Aisagbonhi, Omonigho; Poste, Alethea; Wride, Dustin; Kim, Sylvia; Santos, Therese; Fimbres, Michael; Choi, Dianne; Elia, Haydi; Kaladjian, Joseph; Abou-Zahr, Ali; Mejia, Arturo; Synthesis (Germany); vol. 45; nb. 24; (2013); p. 3361 - 3368; Art.No: SS-2013-M0543-OP, View in Reaxys 4 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

chloroform-d1

Li, Wei; Li, Jianchang; Wu, Yuchuan; Fuller, Nathan; Markus, Michelle A.; Journal of Organic Chemistry; vol. 75; nb. 4; (2010); p. 1077 - 1086, View in Reaxys 5 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

19F

Solvents (NMR Spectroscopy)

chloroform-d1

Frequency (NMR Spectro- 282 scopy) [MHz] Hugenberg, Verena; Haufe, Guenter; Journal of Fluorine Chemistry; vol. 131; nb. 9; (2010); p. 942 - 950, View in Reaxys 6 of 23

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

19F

Solvents (NMR Spectroscopy)

hexane

Wang, Fang; Wenslow Jr., Robert M.; Dowling, Thomas M.; Mueller, Karl T.; Santos, Ivan; Wyvratt, Jean M.; Analytical Chemistry; vol. 75; nb. 21; (2003); p. 5877 - 5885, View in Reaxys 7 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Hogan, Terrence; Sen, Ayusman; Journal of the American Chemical Society; vol. 119; nb. 11; (1997); p. 2642 - 2646, View in Reaxys 8 of 23

Nucleus (NMR Spectroscopy)

Coupling Nuclei

Hogan, Terrence; Sen, Ayusman; Journal of the American Chemical Society; vol. 119; nb. 11; (1997); p. 2642 - 2646, View in Reaxys

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9 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Hogan, Terrence; Sen, Ayusman; Journal of the American Chemical Society; vol. 119; nb. 11; (1997); p. 2642 - 2646, View in Reaxys 10 of 23

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CD2Cl2; CCl4

Temperature (NMR Spectroscopy) [°C]

-78

Katayama, Hiroshi; Kamigaito, Masami; Sawamoto, Mitsuo; Higashimura, Toshinobu; Journal of Physical Organic Chemistry; vol. 8; nb. 4; (1995); p. 282 - 292, View in Reaxys 11 of 23

Description (NMR Spectroscopy)

Spectrum

Nucleus (NMR Spectroscopy)

19F

Solvents (NMR Spectroscopy)

CD2Cl2; CCl4

Temperature (NMR Spectroscopy) [°C]

-78

Katayama, Hiroshi; Kamigaito, Masami; Sawamoto, Mitsuo; Higashimura, Toshinobu; Journal of Physical Organic Chemistry; vol. 8; nb. 4; (1995); p. 282 - 292, View in Reaxys 12 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CDCl3

Nordlander, J. Eric; Catalane, David B.; Kotian, Kirtivan D.; Stevens, Randall M.; Haky, Jerome E.; Journal of Organic Chemistry; vol. 46; (1981); p. 778 - 782, View in Reaxys; Sugiyama, Tomohito; Nojima, Masatomo; Krieger-Beck, Petra; Kim, Woo-Sun; Griesbaum, Karl; Journal of Organic Chemistry; vol. 57; nb. 12; (1992); p. 3487 - 3490, View in Reaxys; Wasiak, J.; Helinski, J.; Dabkowski, W.; Skrzypczynski, Z.; Michalski, J.; Polish Journal of Chemistry; vol. 69; nb. 7; (1995); p. 1027 - 1032, View in Reaxys 13 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

19F

Solvents (NMR Spectroscopy)

CDCl3

Nordlander, J. Eric; Catalane, David B.; Kotian, Kirtivan D.; Stevens, Randall M.; Haky, Jerome E.; Journal of Organic Chemistry; vol. 46; (1981); p. 778 - 782, View in Reaxys; Takeuchi, Yoshio; Itoh, Noriaki; Koizumi, Toru; Yamagami, Chisako; Takeuchi, Yoshito; Magnetic Resonance in Chemistry; vol. 30; nb. 1; (1992); p. 58 - 64, View in Reaxys; Wasiak, J.; Helinski, J.; Dabkowski, W.; Skrzypczynski, Z.; Michalski, J.; Polish Journal of Chemistry; vol. 69; nb. 7; (1995); p. 1027 1032, View in Reaxys 14 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

13C

Solvents (NMR Spectroscopy)

CDCl3

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Takeuchi, Yoshio; Itoh, Noriaki; Koizumi, Toru; Yamagami, Chisako; Takeuchi, Yoshito; Magnetic Resonance in Chemistry; vol. 30; nb. 1; (1992); p. 58 - 64, View in Reaxys; Wasiak, J.; Helinski, J.; Dabkowski, W.; Skrzypczynski, Z.; Michalski, J.; Polish Journal of Chemistry; vol. 69; nb. 7; (1995); p. 1027 - 1032, View in Reaxys 15 of 23

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CDCl3

Comment (NMR Spectroscopy)

1H-1H

Sugiyama, Tomohito; Nojima, Masatomo; Krieger-Beck, Petra; Kim, Woo-Sun; Griesbaum, Karl; Journal of Organic Chemistry; vol. 57; nb. 12; (1992); p. 3487 - 3490, View in Reaxys; Wasiak, J.; Helinski, J.; Dabkowski, W.; Skrzypczynski, Z.; Michalski, J.; Polish Journal of Chemistry; vol. 69; nb. 7; (1995); p. 1027 - 1032, View in Reaxys 16 of 23

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CDCl3

Comment (NMR Spectroscopy)

19F-13C.

Wasiak, J.; Helinski, J.; Dabkowski, W.; Skrzypczynski, Z.; Michalski, J.; Polish Journal of Chemistry; vol. 69; nb. 7; (1995); p. 1027 - 1032, View in Reaxys 17 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

Solvents (NMR Spectroscopy)

CCl4

Forbus, T. R.; Taylor, S. L.; Martin, J. C.; Journal of Organic Chemistry; vol. 52; nb. 19; (1987); p. 4156 - 4159, View in Reaxys 18 of 23

Description (NMR Spectroscopy)

Chemical shifts

Nucleus (NMR Spectroscopy)

19F

Solvents (NMR Spectroscopy)

CCl4

Forbus, T. R.; Taylor, S. L.; Martin, J. C.; Journal of Organic Chemistry; vol. 52; nb. 19; (1987); p. 4156 - 4159, View in Reaxys 19 of 23

Description (NMR Spectroscopy)

Spin-spin coupling constants

Solvents (NMR Spectroscopy)

CCl4

Comment (NMR Spectroscopy)

1H-1H

Forbus, T. R.; Taylor, S. L.; Martin, J. C.; Journal of Organic Chemistry; vol. 52; nb. 19; (1987); p. 4156 - 4159, View in Reaxys 20 of 23

Description (NMR Spectroscopy)

NMR

Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys; Dyatkin,B.L. et al.; Journal of Organometallic Chemistry; vol. 57; (1973); p. 423 - 433, View in Reaxys; Muller; Carr; Journal of Physical Chemistry; vol. 67; (1963); p. 112, View in Reaxys; Barnes et al.; Canadian Journal of Chemistry; vol. 50; (1972); p. 2175,2176-2178, View in Reaxys; Golovanov et al.; J. Gen. Chem. USSR (Engl. Transl.); vol. 43; (1973); p. 2666,2644,2646, View in Reaxys; Sleevi et al.; Analytical Chemistry; vol. 51; (1979); p. 1931,1934, View in Reaxys; Olah et al.; Journal of the American Chemical Society; vol. 97; (1975); p. 5477,5479, View in Reaxys 21 of 23

Description (NMR Spectroscopy)

Spin-spin coupling constants

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Muller; Carr; Journal of Physical Chemistry; vol. 67; (1963); p. 112, View in Reaxys; Winter; Scott; Canadian Journal of Chemistry; vol. 46; (1968); p. 2887,2890, View in Reaxys 22 of 23

Description (NMR Spectroscopy)

Chemical shifts

Comment (NMR Spectroscopy)

Chem. Verschieb. der Protonen am sek. C-Atom in CCl4, Trifluoressigsaeure u. Trifluoressigsaeure-H2SO4 (Lsgm.-Effekt)

Peterson; Journal of Organic Chemistry; vol. 31; (1966); p. 439, View in Reaxys 23 of 23

Description (NMR Spectroscopy)

Chemical shifts

Comment (NMR Spectroscopy)

Chem. Verschieb. der Methylgruppen in CCl4, Trifluoressigsaeure u. Trifluoressigsaeure-H2SO4 (Lsgm.-Effekt)

Peterson; Journal of Organic Chemistry; vol. 31; (1966); p. 439, View in Reaxys IR Spectroscopy (18) 1 of 18

Description (IR Spectroscopy)

Bands; Spectrum

Comment (IR Spectroscopy)

neat (no solvent, gas phase)

Lestard, Maria Eliana Defonsi; Tuttolomondo, Maria Eugenia; Wann, Derek A.; Robertson, Heather E.; Rankin, David W. H.; Ben Altabef, Aida; Journal of Raman Spectroscopy; vol. 41; nb. 10; (2010); p. 1357 - 1368, View in Reaxys 2 of 18

Description (IR Spectroscopy)

Bands; Spectrum

Comment (IR Spectroscopy)

neat (no solvent, solid phase)

Description (IR Spectroscopy)

Bands; Spectrum

Comment (IR Spectroscopy)

neat liquid

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

1788 1/cm

Takayama, Shuichi; Lee, Shelly T.; Hung, Shang-Cheng; Wong, Chi-Huey; Chemical Communications; nb. 2; (1999); p. 127 - 128, View in Reaxys 5 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

hexane

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 6 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

acetonitrile

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 7 of 18

Description (IR Spectroscopy)

Spectrum

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Solvent (IR Spectroscopy)

CHCl3

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 8 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

CCl4

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 9 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

cyclohexane

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 10 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

1,2-dichloro-ethane

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 11 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

tetrachloroethene

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 12 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

CS2

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 13 of 18

Description (IR Spectroscopy)

Spectrum

Solvent (IR Spectroscopy)

dibutyl ether

Comment (IR Spectroscopy)

1820 - 1760 cm**(-1)

Hernanz, A.; Troitino, D.; Morcillo, J.; Journal of Molecular Structure; vol. 142; (1986); p. 255 - 258, View in Reaxys 14 of 18

Description (IR Spectroscopy)

Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys; Pierce; Joullie; Journal of Organic Chemistry; vol. 28; (1963); p. 658,660, View in Reaxys; Winter; Scott; Canadian Journal of Chemistry; vol. 46; (1968); p. 2887,2890, View in Reaxys; Dvorak; Dedek; Collection of Czechoslovak Chemical Communications; vol. 31; (1966); p. 2727,2734, View in Reaxys; Laurence et al.; Journal of the American Chemical Society; vol. 101; (1979); p. 4793,4795, View in Reaxys; Zhukov; Gubanov; Journal of Molecular Structure; vol. 41; (1977); p. 281,284, 285, View in Reaxys; Smolyanskii et al.; J. Gen. Chem. USSR (Engl. Transl.); vol. 49; (1979); p. 675,586,587, View in Reaxys; Crowder; Journal of Fluorine Chemistry; vol. 1; (1971); p. 219,221, View in Reaxys 15 of 18

Description (IR Spectroscopy)

Bands

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Kagarise; Whetsel; Spectrochimica Acta; vol. 18; (1962); p. 341, View in Reaxys; Horak; Moravec; Collection of Czechoslovak Chemical Communications; vol. 36; (1971); p. 2757,2761,2763, View in Reaxys; Ishikawa et al.; Nippon Kagaku Kaishi; (1975); p. 1541,1543, View in Reaxys 16 of 18

Description (IR Spectroscopy)

Intensity of IR bands

Brown; Spectrochimica Acta; vol. 18; (1962); p. 1615,1616, View in Reaxys; Marek et al.; Journal of Applied Spectroscopy; vol. 19; (1973); p. 926; ; p. 130, View in Reaxys 17 of 18

Description (IR Spectroscopy)

Spectrum

Bellamy,L.J.; Pace,R.J.; Spectrochimica Acta; vol. 19; (1963); p. 1831 - 1839, View in Reaxys; Laato; Acta Chemica Scandinavica (1947-1973); vol. 21; (1967); p. 2119,2123,2129, View in Reaxys 18 of 18

Description (IR Spectroscopy)

Bands

Comment (IR Spectroscopy)

1800 - 1000 cm**(-1); dampffoermig und fluessig.

Fuson et al.; Journal of Chemical Physics; vol. 20; (1952); p. 1627,1628,1629,1633, View in Reaxys Mass Spectrometry (3) Description (Mass References Spectrometry) spectrum; electron impact (EI)

Chiang, Chao-Ming; Miller, Timothy M.; Dubois, Lawrence H.; Journal of Physical Chemistry; vol. 97; nb. 45; (1993); p. 11781 - 11786, View in Reaxys

spectrum

Kagramanov, N. D.; Kutin, A. A.; Peschanskii, N. V.; Zapevalov, A. Ya.; German, L. S.; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); vol. 40; nb. 7; (1991); p. 1321 - 1325; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; nb. 7; (1991); p. 1497 - 1502, View in Reaxys; Akhrem, I. S.; Vartanyan, R. S.; Afanas'eva, L. V.; Vol'pin, M. E.; Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation); vol. 32; (1983); p. 1217 - 1220; Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya; nb. 6; (1983); p. 1346 - 1350, View in Reaxys Majid,A.; Shreeve,J.M.; Journal of Organic Chemistry; vol. 38; nb. 23; (1973); p. 4028 - 4031, View in Reaxys

Rotational Spectroscopy (1) Description (Rota- References tional Spectroscopy) Microwave spectrum

True; Bohn; Journal of the American Chemical Society; vol. 98; (1976); p. 1188,1189-1194, View in Reaxys

Raman Spectroscopy (1) Description (Ram- References an Spectroscopy) Raman

Luminescence Spectroscopy (1) Description (Lumi- References nescence Spectroscopy) Luminescence quenching

Carroll et al.; Journal of the American Chemical Society; vol. 95; (1973); p. 315, View in Reaxys

Other Spectroscopic Methods (2) Description (Other References Spectroscopic Methods) ESCA

Nordling; Angewandte Chemie; vol. 84; (1972); p. 144,148, View in Reaxys; Nordling; Journal de Physique, Colloque; vol. 32; (1971); p. C4-254,261, View in Reaxys; Gelius et al.; Physica Scripta; vol. 2; (1970); p. 70,73, View in Reaxys; Gelius et al.; Journal of Electron Spectroscopy and Related Phenomena; vol. 2; (1973); p. 405,423, View in Reaxys; Siegbahn; Philosophical Transactions of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences; vol. 268; (1970); p. 33,48,49, View in Reaxys; Travnikova, Oksana; Borve, Knut J.; Patanen, Minna; Soederstroem, Johan; Miron, Catalin; Saethre, Leif J.; Martensson, Nils; Svensson, Svante; Journal of Electron Spectroscopy and Related Phenomena; vol. 185; nb. 8-9; (2012); p. 191 - 197, View in Reaxys

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Photoelectron spec- Sweigart; Turner; Journal of the American Chemical Society; vol. 94; (1972); p. 5599, View in Reaxys; Smith; Thotrum mas; Journal of the American Chemical Society; vol. 100; (1978); p. 5459,5461, View in Reaxys Use (8) Use Pattern

Location

References

Agricultural use

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

Engineering

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

Pharmaceuticals

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

Printing/ coating/dye

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

synthesis of fluorine-containing dyes

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

synthesis of fluorine-containing liquid crystal

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

synthesis of fluorine-containing medicine

Page/Page column title page

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

synthesis of fluoPage/Page column rine-containing pes- title page ticides

Patent; Sinochem Lantian Co., Ltd.; Li, Hua; Xu, Weiguo; Jiang, Qiang; Dai, Jialiang; Yang, Wangsong; (7 pag.); CN103864615; (2016); (B) Chinese, View in Reaxys

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