International Journal for Research in Applied Science & Engineering Technology (IJRASET)

ISSN: 2321-9653; IC Value: 45.98; SJ Impact Factor: 7.538

Volume 11 Issue IV Apr 2023- Available at www.ijraset.com

3c 419 (80%, M+), 421 (66%, M++2), 418 (48%, M+-1), 388 (25%, M+-OCH3), 387 (20%, M+CH3OH), 356 (18%, M+-2OCH3), 336 (25%), 315(5%), 273(12%), 260 (18%, M+(312)2CO), 245 (16%, M+(260)-NH), 228 (15%, M+(260) -CH3OH), 209 (14%, M+(245)-HCl), 178 (18%, M+(356) -symm. rDA fragment), 152 (30%, M+(178)-CO), 120 (35%), 107 (58%,

C7H7O+), 76 (22%, C6H4 +).

3d 395 (40%,

IV. CONCLUSION

Microwave-assisted synthesis is a convenient way toward the goal of green chemistry. Highly substituted, 2, 5-Dianilino-3, 6Dichloro-1, 4-Benzoquinones (3a-d), have been synthesized .Mass fragmentation of the title compounds along with m/z values and relative intensity of the fragment and 13C NMR characterize the derivatives of 2, 5-Dianilino-3, 6-Dichloro-1, 4-Benzoquinones.

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