Elastomeric & new materials, recycling / dental implant courses by Indian dental academy

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Elastomeric and newer materials Recycling of materials Biodegradation of materials Hypersensitivity reactions Disinfection procedures

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INDIAN DENTAL ACADEMY Leader in continuing dental education www.indiandentalacademy.com

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DISINFECTION PROCEDURES Objective of sterilization –Removal of microorganisms or destroy them from materials or from areas since they cause contamination, infection and decay. In microbiology Surgery Drug & food

- to prevent contamination - to maintain asepsis -for ensuring the safety

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 Sterilization

– The process by which an

article, surface, or medium is freed of all living microorganisms either in the vegetative or spore state  Disinfection – The destruction or removal of all pathogenic organisms, or organisms capable of giving rise to infection

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 Antisepsis

– used to indicate the prevention of infection, usually by inhibiting the growth of bacteria in wounds or tissues SEPS ( A Greek word ) – PUTRID

 Bactericidal agents  Bacteriostatic agents www.indiandentalacademy.com

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Elastomerics  Elastomer

is a material that after substantial deformation rapidly returns to its original dimensions.  Natural rubber- ancient Incan & Mayan civilization- 1st known elastomer  Charles goodyear- 1839vulcanization www.indiandentalacademy.com

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Elastomerics  Natural rubber latex elastics- Baker, Case,

Angle- early advocates  Polymer rubbers – developed from petrochemicals – 1920

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Structure  Primary + secondary bonds- weak

molecular attraction  At rest – folded linear molecule  On extension – unfold- expense of secondary bonds

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Elastomerics  If primary bonds are broken- permanent

deformation  Synthetic polymers – sensitive to free radical generating systems ozone uv light  Decrease in flexibility & tensile strength  Addition of antioxidants & anti ozonates www.indiandentalacademy.com

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Elastomerics 

Introduced to dental profession – 1960’s

Generate light continuous forces Uses – canine retraction diastema closure rotational correction space closure Advinexpensive relatively hygienic easily applied ptn co operation

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Elastomerics ďƒ˜ Disadv –

absorb water & saliva stain permanently permanent deformation rapid loss of force temperature sensitive www.indiandentalacademy.com

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Elastomerics

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Elastomerics

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Elastomerics

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Elastomerics Force degradation and force delivery of elastomeric chains ďƒ˜ Inability to deliver a continuous force level ďƒ˜ Bishara & Anderson-1970- compared latex & unitek alastik modules ďƒ˜ After 24 hrs alastiks 74 % force decay latex elastics 42 % loss www.indiandentalacademy.com

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Force Decay

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Elastomerics  After 1st

day- force decay relatively stable  Hershey & Reynolds- 1975 – compared chains – framework- simulating tooth movement  Conclusion 1st day- 50% force loss 4 wks – 40% original force remains more consistent force- by stamping manufacture – than injection molded www.indiandentalacademy.com

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Elastomerics  Wong1976 – compared two commercial chains  Chains distracted & maintained at 17 mm in water at 37 C  Result – 1st 3 hrs – greatest amount of force lost  Kovach et al – evaluated initial force values of unitek alastiks stretched to 30 % of their original length at rates of .2 , 2 & 20” / min www.indiandentalacademy.com

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 Conclusion –

rapidly extended chains – greater initial force levels At 1 wk the chain stretched at slow rateexhibited less force decay Recommended slow stretching

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 Ash & Nikolai-1978 – compared force

decay of chains – stored in air , water and vivo  In vivo environment – significantly more force decay after 30 mins than those kept in air  After 3 wks – chains in vivo – greater force loss than those stored in water  Both maintained force levels of more than 160 gms www.indiandentalacademy.com

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Due to effects of mastication oral hygiene , salivary enzymes & temp variations

 Genova et al – 1985 – investigated force degradation of chains - artificial saliva  Conclusion chains subjected to tooth movement retained 913 % less force than held at constant length short filament chains – higher initial force levels & retain higher % of remaining force

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 Rock et al – tested 13 commercially

available elastics  Regardless of the no. of loops , the force values at 100% extension were constant  Short filament chains – higher initial force level at 100 % extension-403 to 625gms  Recommended 50 – 75 % extensiondesired force of 300 gms

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 Killiany et al – 1986 – force delivery and

decay characteristics of RMO – ENERGY chain – compared with short loop chain from American orthodontics  After 4 wks – simulated oral environment – ENERGY chain – retained 66 % of initial force short loop chain retained 33 % of original force

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 Kuster etal 1986- compared chains of 2

companies stored in air & in vivo  At 100% extension force levels

315gm 279gm  Initial extension of 50 -75% not supported

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 Storie & Fraunhofer – compared gray

chain & fluoride releasing chain from ortho arch  conclusion fluoride releasing chain – higher initial force level at 100 % extension gray chain – retain 38 % of its initial force fluoride releasing chain – 14 % of initial force after 1 wk in 37 C distilled water

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 Baty & Fraunhofer- compared 3

colour of elastomeric chains with std gray chains  Conclusion 

Colouring had little effect on initial force delivery of chains

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Pre- stretching effects  Purpose – to improve the large initial force

degradation & the constancy of force delivery  Wong – 1976 – pre stretching the elastic chains 1/3 of their original length – improve the strength  Brooks & Hershey – combination of pre - stretching and heat app n – reduced the amount of force degradation by 50 % at 1 hr and 31 % at 4 wks www.indiandentalacademy.com

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 Heat appln alone – increased rate of force

decay  Storie et al – pre stretched gray and

fluoride releasing chains – 50 % for 5 secs Immersed in 3 fluid environments  Reported no clinical benefit

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Environmental effects  Ferriter – 1990 – effect of ph extremes of

plaque (4.95) & saliva (7.26)  Chains – basic soln – exhibited more force decay  Jefferies et al – simulated disinfection 30

mins & sterilization (10 hrs & 1 wk ) using gluteraldehyde soln  Use of gluteraldehyde – no deleterious effect on properties www.indiandentalacademy.com

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 Coffelt et al – subjected chains to

31 % APF 4 % SNF 0.4 % Kcl soln  Concluded 31% APF had some effect on the force delivery & decay rate

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summary 

 

E chains lose 50- 70 % of their initial force during the first day and at 3 wks retain only 30 -40 % of the original force Force guage should be used to determine the desired initial force Longer filament chains deliver a lower initial force at the same extension than the closed loop chain Pre stretching of these chains – means of reducing the rapid force decay rate & a constant force www.indiandentalacademy.com

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summary  Environmental factors – associated with

deformation & force degradation  The synthetic elastomeric chains – protected from direct light  E chains – convenient , inexpensive method – continuous force system over a 3-4 wk period

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White spot lesion Enamel de mineralization ďƒ˜ Prevention 1. Effective plaque control 2. Fluoride release a. fluoride varnishes b. fluoride containing composites c. fluoride releasing GIC d. fluoride relesing elastomers ďƒ˜

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 Enamel sealants – minimal benefit (Banks

& Richmond)  Fluoride releasing composites – ineffective in preventing enamel damage ( Mitchel , Turner – 1993 )  GIC – provides greater fluoride release  Inadequate bond strength  Featherstone – 1985 – long duration low dose fluoride release – reduces demineralization www.indiandentalacademy.com

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 Fluoride releasing elastomeric modules –

provide such conditions  Joseph & Gobler – 1993 – study on the

rate and amount of SNF release from a fluoride impregnated elastic power chain  Material 5 experimental groups & 1 control group 12 unit length of F power chain (CFRD) studied 37 C in a incubator & 100 rpm agitation www.indiandentalacademy.com

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Conclusion fluoride release initially high – very low levels – after 1 wk Minimum continuous level of 0.25 mg of fluoride – necessary for remineralization Bactericidal effect at low levels of fluoride 

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 Protection

only temporary  Max benefit – elastics to be replaced at wkly intervals  Regular topical appln of fluoride still necessary

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 William wiltshire – 1996 – measured

release of fluoride from fluoride releasing elastomeric modules ( fluor-I ties) in vitro  Results initial burst of fluoride during the 1 st and 2nd day foll by a logarithmic decrease  35 % - total fluoride at day 1  63 % - 1st wk  83 % - 1st month  88 % - 2nd month  At 6 months – 0.19 +/- 0.03 micro gms www.indiandentalacademy.com

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 For optimal clinical benefit – replace

fluoride releasing ligature monthly  Banks , Chadwik, Asher

prospective controlled clinical trial To evaluate the effectiveness of SNF releasing modules & chain

Materials 49 ptns, 782 teeth- exptl group 45 ptns, 740 teeth – control group, non fluoride releasing elastomerics www.indiandentalacademy.com

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 After bonding excess composite removed  Etching confined  Standardized dietary & hygiene

instructions  Ptns scored by EDI ( Enamel

Decalcification Index) – Banks & Richmond – 1994 www.indiandentalacademy.com

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EDI

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 Conclusion 

 

The use of fluoride releasing elastomeric modules – reduced enamel decalcification per tooth by 49 % Enamel decalcification control group – 26 % of teeth & 73 % ptns exptl group – 16 % of teeth & 63 % ptns Occlusal zones showed no difference Fluoride releasing elastomerics – effective in reducing enamel decalcification

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Fibre reinforced composite  Poly( ethylene tere phthalate glycol) &

poly (1,4 cyclohexylene dimethylene tere phthalate glycol) reinforced with continuous glass fibres  FRC contained -43-45 vol% fiber  Flexural strength -565 MPa  Requisites proper wetting of glass fibres proper orientation of glass fibres www.indiandentalacademy.com

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pultrusion  Fibre bundles – pulled through an extruder

simultaneously with the extrusion of the polymer.  Fibre bundles impregnated by the polymer  Exiting dies determine cross section shape and size

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Electro micrograph

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Fibre reinforced composite   

Burstone & Gunther 2001 Enhanced mech. properties A metal attachment pad- FRC strip – exhibited superior bonding strength

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Highest failure – with loadings parallel to the tooth surface Less shear strength

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Charles Burstone& Kuhlberg ďƒ˜ Pre impregnated material – PREG

partially polymerised fibre matrix complex

Applications 1. Bonded cuspid to cuspid retainers 2. Bridges

active applications - adjuncts for active tooth movements www.indiandentalacademy.com

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 Matrix – light cured thermoset Bisgma  Splint it – long fibre reinforced composite  S glass fiber-

bar more esthetic

 Two stages of polymerization  Initial polymerization- matrix flexible

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Properties  ME – 70 % > highly filled composite  YS – 6 times >  Resiliency – 24 times >

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ďƒ˜

Clinical use - 3 configurations rope wide strip woven pattern

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 Technique    

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FRC rope cut to length Transparent foil removed Tooth prepared for bonding FRC placed & contoured to tooth Attachments are directly bonded to FRC Low viscosity adhesive – protective layer Indirect or direct bonding

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Active application FRC full arch

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Attachments

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Intermaxillary elastics

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Vertical elastics- open bite

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Extrusion of maxillary incisor segment

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Space closure

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Space closure

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Molar uprighting

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Uprighting posterior segment with tip back spring

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Anterior lingual root torquing spring combination with stainless steel arch wire

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Maxillary incisor intrusion TMA intrusion arch

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Mandibular incisor intrusion arch

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Replacement connectors

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Maxillary lingual bonded FRC retainer

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Connecting FRC framework

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summary  Long fibre reinforced materials have the

potential to replace metals in clinical orthodontics  Biocompatibility not a concern  FRC materials are superior to polymers  Increased rigidity and strength  Highly formable – fabricated in complex shapes www.indiandentalacademy.com

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 Layers can be added to change the shape

- improve rigidity  Precise contour to the teeth  Potential to alter some of the current

methods of active treatment  Esthetic alternative to lingual orthodontics

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 Ptns who need only partial or

compromised treatment are good candidates for FRC appliances  Mixed dentition cases  FRC bars- alternative to bands

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ďƒ˜ Disadvantage

weakest in shear Shear loads to be minimized as much as possible Requires good bonding conditions eg – bridges and retainers

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Biodegradation Orthodontic materials – Universally austentic SS - 18% chromium - 8% nickel NiTi – 1970s Oral environment – ionic properties thermal properties microbiologic enzymatic Ideal for biodegradation 

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ďƒ˜ Human exposure to Ni

- diet - atmosphere - jewelry - water - clothing - fasteners www.indiandentalacademy.com

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 Dietary intake

- Ni – 200 -300 microgms / day - Cr – 280 microgms / day - Ti – 300 – 2000 microgms/day Water – 20 microgms / l – Ni - 0.43 microgms/l- Cr www.indiandentalacademy.com

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 Iatrogenic exposure

Joint prosthesis Dental implants Orthopedic plates Surgical clips Pace maker leads Prosthetic heart valves orthodontic appliances Ni release – dental alloy – 4.2 www.indiandentalacademy.com microgms/cm/day

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 36micgms/day – Cr  Full mouth ortho appliances –

40micgms/day – Ni  Heat treated-SS arch wire-

0.26micgms/cm/day www.indiandentalacademy.com

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 Bishara , Barret – 1993 : Purpose – Compare in vitro corrosion rate for std orthodontic appliances Appliance immersed – prepared artificial saliva at 37c

Materials 10 sets of bands and brackets Both SS & NiTi archwires

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-Type 305 – SS – bands AISI -Type 316 – SS – brackets and tubes AISI -Bands not covered from inner surface -17- 25 wires -5 sets – rectangular SS wires -5 sets – Ni Ti – Unitek Polyethylene tubes – 100 ml Artificial saliva – pH – 6.75 www.indiandentalacademy.com

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Analyzed – 1,7,14,21,28 days

 Results –  

Ni – peak level – day 7th Park and Shearer similar findings

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Cr – peak level 14th day

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Conclusion    

Orthodontic appliances -reasonable amts of Ni & Cr when placed in a artificial saliva medium Ni release reaches max after 1 week then diminishes Cr release increases during the first 2 weeks and levels off during subsequent 2 weeks Release rates of Ni & Cr from SS or NiTi wire – not significantly different.

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Conclusion ďƒ˜ For both archwire types the release rate

for Ni averaged 37 times greater than that for Cr. ďƒ˜ The release rates for full mouth orthodontic appliances are less than 10% of the reported average daily dietary intake for Ni & .25% of those reported for Cr. www.indiandentalacademy.com

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 Changes in the blood level of nickel

Bishara,Barret Purpose: to determine whether orthodontic patients accumulate measurable concentrations of Ni in blood. Materials: 31 subjects – 18 females & 13 males. Blood samples collected 1 – before placement of orthodontic appliance 2 – 2 months after placement 3 – 4-5 months after placement www.indiandentalacademy.com

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Blood analyzed – atomic absorption spectro photometry

Nickel and Chromium carcinogenicity Ni – risk inversely proportional to solubility in aqueous media Cr – hexavalent oxidation state

Normal Ni & Cr conc in blood Ni – 2.4 +/- 0.5 ng/ml & 30 +/- 19 ng/ml Cr – 0.371 ng/ml www.indiandentalacademy.com

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 

Hexavalant Cr – readily absorbed Elimination – urine.

Results – 

Ni levels in blood

All blood levels below normal

17.2% of blood samples – above detection limit of .4 ppb

never exceeded 1.3ppb www.indiandentalacademy.com

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 16 patients no detectable Ni levels  5 patients reduction in blood level

Higher values –  Contamination from venipuncture needle  Diet

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SUMMARY ďƒ˜ Patients with fully banded & bonded

appliances did not show a significant increase in the Ni blood level during the 1 st 4-5 mnts of orthodontic therapy ďƒ˜ Orthodontic therapy using appliances made of alloys containing Ni-Ti did not result in significant increase in the blood levels of Ni. www.indiandentalacademy.com

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Grimsdottir 1992  Facebows,archwires,brackets& molar

bands analyzed  Most appliances – variable amount –Ag solder  14days in 0.9Nacl  Facebows – highest amount of NI &Cr  Archwires- least

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Park & Shearer  Ni &Cr release-simulated ortho appliance  incubated in 0.05%Nacl  Ni-40micgms/day  Cr-36 micgms/day  below the daily dietary intake  may sensitize patients www.indiandentalacademy.com

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Metal release from simulated fixed orthodontic appliances – AJO 2001 Hwang etal

Method Simulated fixed orthodontic appliances ---soaked in 50 ml of artificial saliva pH – 6.75 +/- .15 at 37 C Time period – 3 months 4 groups ( 16 – 22) 2 SS wires 2 Ni-Ti arch wires www.indiandentalacademy.com

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Composition of artificial saliva

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320 polyethylene tubes – 50 ml artificial saliva

Method Metal release – plasma mass spectrometry Analyzed on 1st, 3rd days, 1st 2nd 3rd 4th 8th &12th weeks

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Results Cr release – no increase after 4 weeks – gp A -- 2 weeks in gp B -- 3 weeks in gp C -- 8 weeks in gp D

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Ni release – no increase after 2 weeks – gp A -- 3 days in gp B -- 7 days in gp C -- 3 weeks in gp D

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Iron Release – no increase after 2 weeks – gp A -- 3 days in gp B -- 1 day in gp C & gp D

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CONCLUSION The daily amount of Cr & Ni released – insignificant when compared with – daily dietary intake of these metals Such a small amount of release might produce sensitivity when the orthodontic appliance are in place for 2-3 years For an allergic reaction in the oral mucosa an antigen must be 5 – 12 times greater than that needed for a skin allergy www.indiandentalacademy.com

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Leaching of Ni Cr and Be ions from base metal alloy in an artificial oral environment --Yong Tai, Ralf D Long, J PROST DENT 1992 Method Artificial oral environment – 3D force movement cycles of mastication 12 pairs of crowns articulated Metal vs metal Metal vs enamel Metal vs procelain Metal vs metal without chewing as a control www.indiandentalacademy.com

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1 year simulated – period of mastication Results In vitro analysis in artificial environment – release of Ni & Be from base metal alloy Dissolution & Occlusal wear are both factors in the release of Ni & Be metals Occlusal wear increases the concs 2-3 times more – than with dissolution alone.

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Hypersensitivity Refers to the injurious consequences in the sensitized host following contact with specific antigens. Incidence of Ni sensitivity Greg, Dulap, Moffa – allergic response to Ni containing dental alloys. www.indiandentalacademy.com

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 Ni toxicity – moderately cytotoxic  Cr toxicity – little

Grimsdotir & Hansten – saliva -connecting medium – discharge of ions & metal compounds – combine with chemically corroded metal – attach to mucosa.

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Alan & Smith – incidence rate of hypersensitivity – 10%

Blane & Peltonon – estimated that 4.5 – 28.5 of popln – have sensitivity to Ni Higher prevalence in females  Janson & Park – hypersensitivity in

females – related to environmental exposure – contact with detergents jewellery & other metallic objects

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 Factors affecting development of

sensitization

 Raitt and Brostoff –  Mechanical irritation  Skin laceration  Increased environmental temperature  Increased intensity and duration of

exposure  Genetic factors

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Dietary intake    

Ni - 200 – 300 micgms / day Cr – 250 micgms / day Drinking water – 20 micgms / l – Ni (Bencho ) Amount of Ni release

 Grims Dottar – largest amount of Ni – released

from facebow – silver solder Brackets -- .3-.9 micgms/day SS archwire -- .26 micgms/cm.sq/day www.indiandentalacademy.com

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 Form

of release - Ni – soluble  Cr – insoluble  Allergy more common in extra oral -- intra oral appliances – 6 times 5-12 times higher conc needed – oral mucosa www.indiandentalacademy.com

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Lack of intra oral response due to Salivary glycoproteins -- barrier difference of permeability Cellular hypersensitivity btn skin & mucosa difference in Langerhans distribution

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 No

increase in blood level of Ni – 5 months of Ortho t/t - Bishara

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Hypersensitivity reactions       

Dental Alloys Symptoms of allergic reactions – dental alloys Inflammed hyperplastic gingival tissue Alveolar bone loss -- crowns Edema of throat, palate, gums Osteomyelitis – SS bone fixation wires Orthodontic appliances – face bows & neck straps, Ni-Ti arch wires , www.indiandentalacademy.com

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Symptoms  Contact dermatitis,  Contact stomatitis,  Loss of taste,  Numbness, burning sensn,  Angular chelitis  Severe gingivitis,  Mild erythema with or without edema www.indiandentalacademy.com

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Immunologic mechanism Ni – common cause – contact dermatitis Delayed hypersensitivity reaction Induction phase Elucidation phase Diagnosis – ptn history clinical findings patch testing

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Different corrosion resistant materials – used in Hypersensitivity ptns AISI 316 L steel – most corrosion resistant AISI 304 L steel PIA 17 – 4 Bio force ion guard wire – 3 micron nitrogen coating Pyramid manufacturers – steel -- hypo allergic www.indiandentalacademy.com

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Conclusions The daily amount of Cr & Ni released – insignificant when compared with – daily dietary intake of these metals Such a small amount of release might produce sensitivity when the orthodontic appliance are in place for 2-3 years For an allergic reaction in the oral mucosa an antigen must be 5 – 12 times greater than that needed for a skin allergy www.indiandentalacademy.com

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ďƒ˜ Patients with fully banded & bonded

appliances did not show a significant increase in the Ni blood level during the 1 st 4-5 mnts of orthodontic therapy ďƒ˜ Orthodontic therapy using appliances made of alloys containing Ni-Ti did not result in significant increase in the blood levels of Ni. www.indiandentalacademy.com

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ďƒ˜ The release rates for full mouth

orthodontic appliances are less than 10% of the reported average daily dietary intake for Ni & .25% of those reported for Cr.

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Orthodontic appliances Strong biologic sensitizers

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Janson & Prystousky -- age range 10-20 years

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 Raitt and Brostoff – several factors for the development of sensitization  Mechanical irritation  Skin laceration  Increased environmental temperature  Increased intensity and duration of exposure  Genetic factors

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Kawahara & Yamakawa – Ni – moderately cytotoxic & Cr – little toxicity.

Grandjsan et al – avg dietary intake Ni – 200 -300 micgms./day Cr – 250 micgms/day

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Benco – Ni concs – drinking water below 20 micgm/ltr. -- below the normal dietary intake-not clinically significant

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Majjer & Smith – Ni released – soluble compound Cr – insoluble form

Greg & Temovari – reaction – use of facebow – Ni-Ti arch wires

Moffa et al – allergic response to Ni containing dental alloys

Dulap et al – allergic reaction – insertion of Ni-Ti wire in sensitive patient www.indiandentalacademy.com

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Jacobson & Hensten –

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Park & Shearer -- Ni from orthodontic bands – sensitized ptns. – cause hypersensitivity reactions in ptns with prior h/o hs.

James et al – no relationship betwn a +ve recn to Ni & a clinical response to Ni containing dental alloy

Stearh Jear et al – no risk involved for Ni sensitive ptns www.indiandentalacademy.com

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Bishara, Barrete – no increase in blood level of Ni – 5 months of orthodontic treatment.

Magnuson & Neilson – higher level of Ni conc – needed to elicit – intra oral response

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Fischer – sensitivity test – not to be used indiscriminately

Vijayabasava, Surendra Shetty –

decrease in pH – increase in Ni Highest – pH 5.8 Ni release – less than 5-10% daily dietary intake Ross Levy et al – orthodontic appliance – induce sensitivity – little or no effect on the gingiva of the ptn. www.indiandentalacademy.com

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Recycling “ Involves repeated exposure of the appliance for several wks to mechanical stresses or elements of the oral environment as well as sterilization b/w uses. May result in corrosion and biodegradation of the wire Alteration in properties www.indiandentalacademy.com

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Recycling  Niti – desirable mechanical prop  

 

Relatively high cost Buckthal et al – 52% orthodontists recycle Ni ti wires 80% cold methods – disinfection Cold & heat sterilization – don’t affect mechanical properties Harris et al – simulated oral environment 0.016 Nitinol wires www.indiandentalacademy.com

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 Concluded – significant decrease in YS –

4 month period

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Effects of clinical recycling on mechanical properties of Niti alloy wires -sunil kapila-1991  Materials and methods

60 wires – Nitinol & Niti wires 3 point bending test – mechanical properties SEM – surface characteristics

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 Wires

To – as received condition T1 – 8 wks of clinical exposure ( 1 cycle) T2 – 2 cycles Cold recycled after one clinical cycleisopropyl alcohol Results Nitinol wires subjected to 1 or 2 recycles demonstrated statistically significant differences during loading then control To www.indiandentalacademy.com

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ďƒ˜ SEM of both Nitinol and Niti wires

demonstrated increased pitting of wires after clinical exposure

ďƒ˜ Some smoothening of Nitinol wires were

also observed in localised regions of the wire

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Surface characteristics

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Recycling of orthodontic brackets  British survey – 47.5 % of clinicians recycle metal brackets 

recycled brackets – accelerates corrosion process

wheeler and Ackermann – reduction in mesh diameter – recycling – no significant change in bond strength www.indiandentalacademy.com

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 Mascia and chen – decrease in shear

bond strength  Hixon et al – studied change in bracket

slot tolerance after recycling of brackets  concluded – no statistically significant change in the tolerance through two successive recycles  Chapman – bracket slot - increase in

width – proportionate to no. of times it is recycled www.indiandentalacademy.com

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comparison of iron release from new and recycled orthodontic brackets-Huang & Yen- AJO2001 purpose – compare release of ions

Ni, Mn , Fe 

materials and methods – 12 wk

period recycle brackets – coated with adhesive and heat treated atomic absorption – detection of ions www.indiandentalacademy.com

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 surface characteristics – energy dispersive

radiographic analysis  Results – recycled brackets released

more ions than new brackets  Both new and recycled brackets can degrade in solns  Greater amounts of Ni, Mn and Fe ions were released in the artificial saliva soln than in other buffer solns

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 The brackets release greater amounts of

ions in a ph 4 buffer than in ph 7 or 10 buffer  As the immersion time increased so did the ion release  After 12 wk immersion the total amount of ion release was less than the cumulative daily intake-

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Effect of recycling on the mechanical properties and surface topography of Niti alloy wires Sung ho lee & Chang – AJO 2001 Parameters – mechanical properties surface topography frictional forces

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Materials 3 types of Niti wires – 60 wires 16. 22 rectangular wires 1. As received condition – To - control group 2. Treated in artificial saliva for 4 wks – T1 3. Treated in artificial saliva & autoclaved – T2 Method – maintained in a incubator at 37 C 

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 Results – Niti wires demonstrated no

statistically significant differences in max tensile strength , ME and bending fatigue

 Niti and Optimalloy demonstrated

increased pitting and corrosion on recycling , Sent alloy did not

 Recycled NIti and Optimalloy

demonstrated greater surface roughness , Sent alloy did not . www.indiandentalacademy.com

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 Recycled Niti and Optimalloy

demonstrated significantly greater max frictional co.eff s than did the control group.

 Sent alloy showed no difference.  Surface roughness and frictional co.eff of

recycled Niti and Optimalloy were not more than those of Sent alloy control group www.indiandentalacademy.com

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changes in bracket slot tolerence following recycling of direct bond metallic orthodontic appliances -Mark Hixson Materials and methods – Stainless steel – direct bond brackets – 3 different companies Evaluated for changes in ability to be torqued by rectangular arch wire after being recycled 75 0.022 * 0.028 brackets www.indiandentalacademy.com

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ďƒ˜ Torque meter assembly

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 conclusion – recycling of brackets results in no significant change in the tolerance through two successive recycles  The max increase in tolerance after 2 recycles was approximately 3 degrees

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Effect of recycling on shear bond strength – D N Kapoor, Pradeep Tandon – JIOS sep 03  Purpose – compare the reconditioning

methods like flaming ,sand blasting and solvent disolution  Bond strength – universal instron testing machine

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Results ďƒ˜ New brackets bonded to freshly extracted

teeth produce higher shear bond strength when compared to re-bonded brackets bonded to freshly extracted teeth and/or reconditioned enamel surface ďƒ˜ Flaming and sand blasting method for re conditioning of brackets demonstrates highest shear bond strength www.indiandentalacademy.com

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Results ďƒ˜ Rebonded brackets after re conditioning

by solvent disolution method exhibit more than optimum shear bond strength and can be an effective chemical method for reconditioning ďƒ˜ Lowest value of shear bond strength was seen when the bracket - reconditioned by flaming was bonded to reconditioned enamel surface www.indiandentalacademy.com

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results ďƒ˜ Significant alteration In the enamel surface

was not observed due to repeated bonding - SEM

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Thank you www.indiandentalacademy.com Leader in continuing dental education

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