Hbm 2016 exoprep

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EXO-Prep Isolate successfully exosomes from body fluids and cell media Exosomes one step isolation from a wide range of biofluids or cell culture media

Isolate exosome from your sample by EXO-Prep

Applications

EXO-Prep is a new and efficient method for exosome isolation from biofluids and from cell culture media. Exosomes are quicky isolated from your sample by an incubation step with EXO-Prep precipitation reagent. Exosome pellet is subsequently collected by one-step centrifugation and can be easily resuspended in PBS 1X. Solubilized exosomes are suitable for different downstream analyses such as proteomic or nucleic acids marker profiling, NTA, FACS etc.

Single step isolation of exosomes from biofluids and cell supernatants.

Isolate the overall exosome population in a sample.

Isolated exosomes can be used for NTA analysis.

Isolated exosomes are suitable for protein profiling (WB, ELISA, FACS).

Isolated exosomes are suitable for nucleic acid extraction and profiling.

Cat. Code

Volume

Reactions

EXO-Prep for Exosome Isolation from Plasma and Serum HBM-EXP-B5

5 ml

180 reactions Plasma, 80 reactions Serum

HBM-EXP-B10

10 ml

350 reactions Plasma, 160 reactions Serum

HBM-EXP-B20

20 ml

700 reactions Plasma, 320 reactions Serum

HBM-EXP-C25

25 ml

HBM-EXP-C50

50 ml

EXO-Prep for Exosome Isolation from Cell Media 25 reactions 50 reactions EXO-Prep for Exosome Isolation from Urine HBM-EXP-U25

30 ml

25 reactions

HBM-EXP-U50

60 ml

50 reactions

EXO-Prep: working procedure and potential applications 12 10

Plasma

8

4 2

Serum

0

110 kDa> 100 ul

250 ul Plasma volumes used for exosome isolation

Urine

Sample video

Exosome pellet

NTA performed on exosomes isolated by EXO-Prep and resuspended in 100 ul of PBS 1X. Size of particles is in according to the size of exosome vesicles (50-120 nm)

Western blotting: Detection of Exosome marker Alix in protein lysates (30 ug) from exosomes isolated with EXO-Prep from 100 ul and 500 ul of plasma/serum and 10 and 20 ml of whole urine. Protein lysates (30 ug) from exosomes purified by ultracentrifugation (UC) were used as control.

Nucleic acids extraction and analysis: Exosomes previously isolated by EXO-Prep or ultracentrifugation (UC) from 100 ul or 500 ul of plasma were used for total RNA extraction and profiling of four exosomal miRNAs. Exosome isolated with EXO-Prep are enriched in miRNAs compared to those purified by ultracentrifugation from the same amount of plasma. 22,00 24,00

miR16

26,00

CT

Exosome isolated from 100 ul of plasma

Alix

110 kDa>

Spin to collect exosome pellet

Nano Tracking Analysis (NTA)

Particle Size/Concentration

Alix

500 ul

Cell Supernatants

69

Alix

110 kDa>

6

Add the appropriate volume of EXO-Prep and incubate in ice for 1 h

Biofluids

EXO-Prep isolation

CD9 expression in exosomes isolated from different volumes of plasma

Ratio to background

ELISA assay: Exosomes isolated by EXOPrep are suitable for protein profiling using ELISA assay. ELISA performed on HBM immunoplate for overall exosome capture from human plasma (HBM-POF)

miR21

28,00

miR223 miR451

30,00 32,00 34,00

100ul

500ul UC

www.hansabiomed.eu info@hansabiomed.eu

100ul 500ul EXO-Prep


EXO-Prep isolate the overall exosome population in your sample in one single step Particle size/ Concentration

Sample and particles number

Sample Video Frame

Particle size/ Concentration

Sample Video Frame

A

C

Whole human plasma

Sample and particles number

Plasma post EXO-Prep treatment

Particles/ml: 8.92x10^11

Particles/ml: 0.91x10^11

B Exosomes isolate by EXO-Prep from 100 ul of plasma

NTA analysis performed on the same plasma sample before and after EXO-Prep treatment shows that EXO-Prep is able to isolate almost the entire exosome population in the sample. Indeed the number of particles in Exosome isolated by EXO-Prep ( 8.67x10^11) corresponds to that present in whole plasma (8.92x10^11). Viceversa plasma after EXOPrep treatment remains depleted of microvesicles (0.91x10^11).

Particles/ml: 8.67x10^11

1. NTA and exosome detection in whole plasma (A), EXO-Prep isolated exosomes resuspended in 100 ul of PBS 1x (B) and plasma post EXO-Prep treatment (C).

EXO-Prep guarantees exosome isolation form complex biofluids, high performances and cheaper price than competitor products Isolation from 100 ul of human plasma 12

9 8

Ratio to background

Ratio to background

2. CD9 expression of plasma exosomes from two healthy individuals (100 μl and 250 μl) using EXO-Prep (EP) isolation reagent compared to a competitor reagent (Comp) and exosomes purified by ultracentrifugation (UC).

Isolation from 250 ul of human plasma

10

7 6 5 4 3 2

10

1 0

I1 EP

I2 EP

I1 Comp I2 Comp

UC 1

8 6 4 2 0

UC 2

I1 EP

I2 EP

I1 Comp I2 Comp

UC 1

UC 2

miRNA Analysis

Total RNA yield

20,00

50 45

22,00

40

24,00

30

CT Values

RNA yield (ng)

35

25 20 15

miR16

26,00

miR21 miR223

28,00

miR451

30,00

3. RNA extraction and profiling of 4 exosome miRNA from exosomes isolated by EXOPrep, a Competitor reagent and ultracentrifugation (UC). 100 μl of plasma sample have been used.

10

32,00

5 0

UC

Competitor

Characteristics Exosome isolation from cell supernatants Exosome isolation from complex biofluids (plasma, serum, urine) Plasma exosome isolation

34,00

EXO-Prep

Thrombin pretreatment Pellet solubility

EXO-Prep

UC

Competitor

Yes

Yes

Yes

Yes, but pellet is hard to solubilize

Not required

Necessary

Easy

Very hard

100 μl

250 μl

Isolated exosome are intact and suitable for ELISA assay

Yes

No suitable for ELISA quantification

Suitable for nucleic acids extraction and analysis

Yes

Yes

Price (for 5 ml of reagent)

●●

●●●

Minimum sample amount

HansaBioMed LLC Email: info@hansabiomed.eu Tel: +372 620 43 48 Fax: +372 620 43 58

Competitor

EXO-Prep

EXO-Prep is a fast and efficient method for exosome isolation from biofluids or cell culture media. In particular, when compared to a competitor product on the market, EXO-Prep allows exosome isolation from a smaller volume (100 ul) of complex biofluids as plasma, without thrombin pretreatment or difficult solubilization of exosome pellet. EXO-Prep-isolated exosomes are suitable for different analyses: protein profiling via western blotting or ELISA (Fig 2), nucleic acids extraction and miRNA/mRNA profiling (Fig 3), FACS.

US Contact Email: info@galenlabsupplies.com Tel: 860-704-9058 Fax: 888-260-6091 www.galenlabsupplies.com


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