Report:
OLCC License No. 10087092BDA
SW 2nd Street. Corvallis
Evaluation Summary
For OLCC/OHA Compliance Purposes.
Product Description Evaluation Summary
Client:
Product Name:
#9604
Process Date: 2021-09-19
Retest Date: 2023-09-19
Matrix: Hemp Concentrate
Metrc Source ID: n/a
Metrc Package ID: n/a
License Number: n/a
Date Collected: 2021-09-20
Date Received: 2021-09-20
Total THC
Total CBD
Abrv.
Not Required
Report Date: 2021-09-22 CBDVA
Report ID: A4664-01
Tests Requested: Cannabinoid Potency Analysis Pesticide Analysis
Solvent Analysis
Wt. %Dry Wt. mg/g
LOQ
LOQ
LOQ
LOQ
LOQ
LOQ
LOQ 99.40 %994.0 mg/g
LOQ
LOQ < LOQ
LOQ < LOQ < LOQ < LOQ 0.52 %5.2 mg/g
LOQ
LOQ
LOQ
LOQ
LOQ < LOQ
COA
| ORELAP ID. 4147 545
OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
|
THCA
Δ-9-THC
Δ-8-THC
THCV
. CBDA
CBD
CBGA
CBG
CBDV CBN CBL CBC | Report ID: A4664-01 | Page 1 of 11 | Rev 21.4 09/03/2021 Dry
Test
<
< LOQ
*
*
GVB Oregon
09.20.21 CBD Isolate GBL BCH
Prim - GVB I - CBD Cannabinoid Potency Analysis Moisture Analysis <
< LOQ <
<
No Pesticides Were Detected above Oregon's action limit as stated in OAR 333-007-0400. <
<
<
<
0.00 % 99.40 % <
<
<
<
Residual
<
<
<
0.0 mg/g 994.0 mg/g Pesticide Analysis * moisture compensated & adjusted for the loss of carboxylic acid group - OAR 333-064-0100 Pesticide Status Pass
Report: Case Narrative
OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
This certificate of analysis is prepared for… GVB Oregon
2490 Ewald Ave SE Salem, OR 97302
For OLCC/OHA Compliance Purposes.
This report presents the analytical findings for the sample collected on 2021-09-20 by Skyler Smith using sampling plan A4664 and received by PREE Laboratory on 2021-09-20. The sample was assigned a laboratory ID of A4664-01. The results in this report only apply to sample A4664-01.
This report shall not be reproduced, except in full, without written consent of PREE Laboratory. Report alterations by any other entity beside PREE Laboratory are not allowed. If alterations are made to the original report after the initial release, they will be noted on the case narrative below.
The testing methods used are of sufficient sensitivity to meet the compliance criteria set in OAR 333-007. However, it is the responsibility of the client to utilize the data to comply with standards set in OAR 333-007.
All analyses were performed in accordance with PREE Laboratory’s NELAP/TNI approved quality control system and all quality control data was within the laboratory’s predefined acceptance criteria unless otherwise noted in the case narrative of this report. General comments are also recorded below.
Notes:
The Oregon Department of Agriculture requires hemp products to not contain more than 0.35% total THC, per OAR 603048. Residual solvent analysis was subcontracted. The report from the subcontracting laboratory is attached. Pesticides: The closing calibration verification for the following analytes did not meet the acceptance criteria: Spirofesifen
Sardar, Tamzid M. | Laboratory Director Corvallis, Oregon
If you have any questions regarding the information in this report, please feel free to call 541-257-5002 or email PREE at services@preelab.com.
A4664-01
Report ID:
| Page 2 of 11 | Rev 21.4 09/03/2021
Report: Evaluation Detail
OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
Moisture Analysis
Cannabinoid Potency Analysis
Product Name:
Analysis Date: 2021-09-21
Testing Batch ID: V1768,1767,1766,1765,1758,1756
Testing Method: LSOP #303 Cannabinoid Quantification
Evaluation Detail
Moisture Analysis
Note:
For OLCC/OHA Compliance Purposes.
Evaluation Detail < LOQ
09.20.21 CBD Isolate GBL BCH #9604 Prim Cannabinoid Potency Analysis |Compound Abrv. Total THC * 0.00 % 0.0 mg/g Total CBD * 99.40 % 994.0 mg/g < LOQ
| 99.40 % < LOQ < LOQ < LOQ 0.52 % < LOQ < LOQ
Dry Wt. (mg/g) RL (%) < LOQ
Dry Wt. (%)
Tetrahydro-cannabinolic acidTHCA < LOQ 0.2 % Delta9 Tetrahydro-cannabinolΔ-9-THC < LOQ 0.2 % Delta8 Tetrahydro-cannabinolΔ-8-THC < LOQ 0.2 %
Test Not Requested/Required < LOQ < LOQ < LOQ
TetrahydrocannabivarinTHCV < LOQ 0.2 % Cannabidiolic acid CBDA < LOQ 0.2 % Cannabidiol CBD 994.00.2 % Cannabigerolic acidCBGA < LOQ 0.2 % Cannabigerol CBG < LOQ 0.2 % Cannabidivarinic acidCBDVA < LOQ 0.2 % Cannabidivarin CBDV 5.20.2 % Cannabinol CBN < LOQ 0.2 % Cannabicyclol CBL < LOQ 0.2 % Cannabichromene CBC < LOQ 0.2 %
* moisture compensated & adjusted for the loss of carboxylic acid group - OAR 333-064-0100
Report ID: A4664-01 | Page 3 of 11 | Rev 21.4 09/03/2021
Accreditation for Δ-8-THC, THCV, CBGA,CBG, CBDVA, CBDV, CBL, CBC, CBN is not offered by ORELAP and therefore are not accredited tests.
Report: Evaluation Detail
OLCC License No. 10087092BDA | ORELAP ID.
545 SW 2nd Street. Corvallis OR.
| 541.257.5002 | services@preelab.com | Preelab.com
Pesticide Analysis Evaluation Detail
For OLCC/OHA Compliance Purposes.
09.20.21 CBD Isolate GBL BCH #9604 Prim Pesticide Name|
Testing Batch ID: V1769,1768,1767,1766
LSOP #307 Pesticides by LCMS/MSTesting Method:
Abamectin < LOQ 0.50 Pass
Acephate < LOQ 0.40 Pass
Acequinocyl < LOQ 2.00 Pass
Tested Value (ppm) Pass Criteria (ppm) 0.40 Pass
Azoxystrobin 0.043 0.20 Pass Bifenazate < LOQ 0.20 Pass
Bifenthrin < LOQ 0.20 Pass Boscalid < LOQ 0.40 Pass
Carbaryl < LOQ 0.20 Pass Carbofuran < LOQ 0.20 Pass
Acetamiprid < LOQ 0.20 Pass Aldicarb < LOQ Chlorantraniliprole < LOQ 0.20 Pass
Chlorfenapyr < LOQ 1.00 Pass
Chlorpyrifos < LOQ 0.20 Pass Clofentezine < LOQ 0.20 Pass
Cyfluthrin < LOQ 1.00 Pass Cypermethrin < LOQ 1.00 Pass
Daminozide < LOQ 1.00 Pass Diazinon < LOQ 0.20 Pass
Dichlorvos < LOQ 1.00 Pass Dimethoate < LOQ 0.20 Pass
Ethoprophos < LOQ 0.20 Pass Etofenprox < LOQ 0.40 Pass
Etoxazole < LOQ 0.20 Pass Fenoxycarb < LOQ 0.20 Pass
Fenpyroximate < LOQ 0.40 Pass
Fipronil < LOQ 0.40 Pass
Pass
Fludioxonil < LOQ 0.40 Pass
Hexythiazox < LOQ 1.00
Imazalil < LOQ 0.20
Flonicamid < LOQ 1.00 Imidacloprid < LOQ 0.40 Kresoxim-methyl < LOQ 0.40
LOQ (ppm) Status Pass/Unsatisfactory Pass
Pass
Pass Pass
Product Name: Analysis Date: 2021-09-21 0.20 0.04 0.20 0.04 0.04 0.04 0.04 0.20 0.04 0.04 0.04 0.04 1.00 0.04 0.20 1.00 1.00 0.20 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.20 0.04 0.04 0.04 0.20 Continued on next page…
Report ID: A4664-01 | Page 4 of 11 | Rev 21.4 09/03/2021
4147
97333
Report: Evaluation Detail
OLCC License No.
545 SW 2nd Street.
Pesticide Analysis
| services@preelab.com | Preelab.com
Evaluation Detail
Pesticide Name|
Pass Criteria (ppm) LOQ (ppm) Status Pass/Unsatisfactory Malathion < LOQ 0.20 Pass
Tested Value (ppm)
Metalaxyl < LOQ 0.20 Pass Methiocarb < LOQ 0.20 Pass
Methomyl < LOQ 0.40 Pass
Methyl-Parathion < LOQ 0.20 Pass
MGK-264 < LOQ 0.20 Pass
Myclobutanil < LOQ 0.20 Pass
Paclobutrazol < LOQ 0.40 Pass Permethrins < LOQ 0.20 Pass
0.20 Pass
Pyrethrins < LOQ 1.00 Pass
Pyridaben < LOQ 0.20 Spinosad < LOQ 0.20
Spiromesifen
Propoxur < LOQ 0.20
Naled < LOQ 0.50 Pass Oxamyl < LOQ 1.00 Pass Phosmet < LOQ 0.20 Pass Piperonyl butoxide < LOQ 2.00 Pass < LOQ 0.20
Spirotetramat
Pass Pass Spiroxamine
Pass Pass
Prallethrin < LOQ 0.20 Pass Propiconazole < LOQ 0.40 Pass 0.20 Pass
Thiacloprid < LOQ
For OLCC/OHA Compliance Purposes. 0.04 0.04 0.04 0.04 0.20 0.20 0.20 0.04 0.04 0.04 0.20 0.04 0.04 0.20 0.20 0.04 1.00 0.04 bo 0.20 0.20 0.04 0.04 0.04 0.04 0.04 0.04
Trifloxystrobin
< LOQ
0.40 Pass Tebuconazole < LOQ 0.40 Pass
Thiamethoxam < LOQ 0.20 Pass Pass
< LOQ < LOQ 0.20
ID: A4664-01 |
10087092BDA | ORELAP ID. 4147
Corvallis OR. 97333 | 541.257.5002
Report
Page 5 of 11 | Rev 21.4 09/03/2021
For OLCC/OHA Compliance Purposes.
Quality Control Detail
Moisture Analysis|
Cannabinoid Potency Analysis
Analysis Date: 2021-09-21
Quality Control Detail
Tetrahydro-cannabinolic acid
Delta9 Tetrahydro-cannabinol Cannabidiolic acid
Cannabinoid Potency Analysis |MBLCS Cannabidiol
Tetrahydro-cannabinolic acid
Delta9 Tetrahydro-cannabinol Cannabidiolic acid
Cannabidiol
ID:
< 0.1% < 0.1% < 0.1% < 0.1% < 0.1% < 0.1%
Pass Criteria Tested Value (%) Expected Value (%) < 0.1% < 0.1% < 0.1% < 0.1%
84.3% 84.9% 86.4%
< 0.1% 80-120%
100.0% 80-120% 100.0% 80-120% 100.0% 91.8%
Moisture Analysis < 0.1% 100.0% 80-120%
Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
◦ ◦ ◦ ◦ • • • • Report
A4664-01 | Page 6 of 11 | Rev 21.4 09/03/2021 Testing Batch ID: V1768,1767,1766,1765,1758,1756
OLCC License No.
2nd Street.
Pesticide Analysis
Analysis Date: 2021-09-21
For OLCC/OHA Compliance Purposes.
Quality Control Detail
Pesticide Name |
1 Abamectin
0 Acephate
Acequinocyl
Acetamiprid
Aldicarb
Azoxystrobin
Bifenazate
Bifenthrin
Boscalid
Carbaryl
Carbofuran
Chlorantraniliprole
1 Chlorfenapyr
0 Chlorpyrifos
0 Clofentezine
Cyfluthrin
Cypermethrin
Daminozide
Diazinon
Dichlorvos
Dimethoate
Ethoprophos
Etofenprox
Etoxazole
Fenoxycarb
Fenpyroximate
Fipronil
Flonicamid
Fludioxonil
Hexythiazox
Imazalil
Imidacloprid
Kresoxim-methyl
< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02
Expected Value (ppm) Tested Value (ppm) Pass Criteria (ppm) < 0.02< 0.02< 0.02
< 0.02< 0.02
< 0.02< 0.02< 0.02
< 0.02< 0.02< 0.02
< 0.02 < 0.1< 0.1 < 0.1
< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.5< 0.5 < 0.5
< 0.5< 0.5 < 0.5 < 0.5< 0.5 < 0.5
< 0.02 < 0.1
< 0.02 < 0.02 < 0.1
< 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1 < 0.02 < 0.1
< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02< 0.02 < 0.02
< 0.1 < 0.02 < 0.02 < 0.02
< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.1 < 0.02
< 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.02 < 0.1 < 0.02 < 0.02
< 0.02
< 0.02 < 0.02 < 0.1 < 0.1< 0.1
Continued on next page… Report ID: A4664-01
Page 7 of 11
Rev 21.4 09/03/2021
Report: Quality Check
10087092BDA | ORELAP ID. 4147 545 SW
Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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Testing Batch ID: V1769,1768,1767,1766
MB
For OLCC/OHA Compliance Purposes.
Quality Control Detail
Pesticide Name |MB Expected Value (ppm)
Malathion
Metalaxyl
Methiocarb
Methomyl
Methyl-Parathion
MGK-264 I
MGK-264 II
Myclobutanil
Naled
Oxamyl
Paclobutrazol
Permethrin - trans
Permethrin - cis
Phosmet
Piperonyl butoxide
Prallethrin
Propiconazole
Propoxur
Pyrethrin - Cinerin
Pyrethrin - Jasmolin
Pyrethrin - Pyrethrins
Pyridaben
Spinosyn A
Spinosyn D
Spiromesifen
Spirotetramat
Spiroxamine
Tebuconazole
Thiacloprid
Thiamethoxam
Trifloxystrobin
Tested Value (ppm) Pass Criteria (ppm) < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02
< 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02
< 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1
< 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1
< 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02
< 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1
< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02
< 0.02< 0.02< 0.02 < 0.1< 0.1 < 0.1
< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02
< 0.5< 0.5 < 0.5 < 0.5< 0.5 < 0.5
< 0.5< 0.5 < 0.5 < 0.02< 0.02< 0.02
< 0.1< 0.1 < 0.1 < 0.1< 0.1 < 0.1
< 0.1< 0.1 < 0.1 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02
< 0.02< 0.02< 0.02 < 0.02< 0.02< 0.02
Pesticide Analysis < 0.02< 0.02< 0.02
Continued on next page…
Report ID: A4664-01 | Page 8 of 11 | Rev 21.4 09/03/2021
Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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Check
For OLCC/OHA Compliance Purposes.
Pesticide Analysis Quality Control Detail
Abamectin
Acephate
Acequinocyl
Acetamiprid
Aldicarb
Azoxystrobin
Bifenazate
Bifenthrin
Boscalid
Carbaryl
Carbofuran
Chlorantraniliprole
Chlorfenapyr
Chlorpyrifos
Clofentezine
Cyfluthrin
Cypermethrin
Daminozide
Diazinon
Dichlorvos
Dimethoate
Ethoprophos
Etofenprox
Etoxazole
Fenoxycarb
Fenpyroximate
Fipronil
Flonicamid
Fludioxonil
Hexythiazox
Imazalil
Imidacloprid
Kresoxim-methyl
100.00120.22 100.00112.53
100.00111.13 114.00
Pesticide Name | 100.00136.21
60 - 140
60 - 140
100.00114.4660 - 140
104.06 100.00122.85
100.00104.45
Pass Criteria (%) 60 - 140
60 - 140 60 - 140 60 - 140
LCS Expected Recovery (%) Actual Recovery (%) 100.00 100.00112.3760 - 140
60 - 140
60 - 140 100.00113.1260 - 140
100.00129.4560 - 140
100.00104.52
60 - 140 100.0098.3060 - 140
100.00106.0960 - 140 100.0096.1360 - 140
100.0099.14
60 - 140 100.00112.7960 - 140
100.00120.5860 - 140 100.00123.9860 - 140
100.00116.26
60 - 140 100.00113.8360 - 140
100.00105.1660 - 140 100.00109.9660 - 140
100.00101.62
100.0093.63
60 - 140 100.00112.4160 - 140 60 - 140 100.00118.4360 - 140
100.00119.2860 - 140 100.00116.4760 - 140
100.00 100.00106.8360 - 140 100.00111.3760 - 140 100.00111.2360 - 140
Continued on next page…
Report ID: A4664-01 | Page 9 of 11 | Rev 21.4 09/03/2021
Report: Quality
OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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For OLCC/OHA Compliance Purposes.
Pesticide Analysis
Quality Control Detail
Pesticide Name |
Malathion
Metalaxyl
Methiocarb
Methomyl
Methyl-Parathion
MGK-264 I
MGK-264 II
Myclobutanil
Naled
Oxamyl
Paclobutrazol
Permethrin - trans
Permethrin - cis
Phosmet
Piperonyl butoxide
Prallethrin
Propiconazole
Propoxur
Pyrethrin - Cinerin
Pyrethrin - Jasmolin
Pyrethrin - Pyrethrins
Pyridaben
Spinosyn A
Spinosyn D
Spiromesifen
Spirotetramat
Spiroxamine
Tebuconazole
Thiacloprid
Thiamethoxam
Trifloxystrobin
100.00123.1060 - 140 100.00115.7860 - 140
LCS Expected Recovery (%) 100.00113.2560 - 140 100.00114.0260 - 140 100.00117.9060 - 140 100.0099.7760 - 140 100.00112.1060 - 140 100.00108.4260 - 140
Actual Recovery (%) Pass Criteria (%) 100.00111.0060 - 140 100.00126.1860 - 140
100.00110.9860 - 140 100.00113.8260 - 140 100.00122.0460 - 140 100.0093.0360 - 140
100.0089.2760 - 140 100.0095.5360 - 140 100.00114.5960 - 140 100.00112.1760 - 140 100.00137.6760 - 140
100.0089.8960 - 140 100.00101.5360 - 140 100.00113.2560 - 140 100.00114.5660 - 140
100.00121.0060 - 140 100.00104.2460 - 140 100.00107.0560 - 140 100.0094.4460 - 140 100.00114.4060 - 140
100.00119.7260 - 140 100.00284.02 (Q)60 - 140 100.00102.6261 - 140
Report ID: A4664-01 | Page 10 of 11 | Rev 21.4 09/03/2021
Report: Quality Check OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
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OLCC License No. 10087092BDA | ORELAP ID. 4147 545 SW 2nd Street. Corvallis OR. 97333 | 541.257.5002 | services@preelab.com | Preelab.com
Definitions
For OLCC/OHA Compliance Purposes.
Limit of Quantitation (LOQ) : The minimum level, concentration, or quantity of a target analyte that can be reported with a specific degree of confidence.
Method Blank (MB) : A quality control sample that is free of the analyte being measured.
Laboratory Control Sample (LCS) : A quality control sample with a known amount of the analyte used to demonstrate accuracy.
Field Duplicate : A second sample collected in the field using the same sampling method as the primary sample.
Action Limit : Analyte levels set by the state of Oregon (OAR 333-007) indicating that follow-up action is necessary.
ppm : parts per million, equivalent to 1 μg/g and 1 μg/L or 0.001 mg/g and 0.001 mg/L
COA : Certificate of Analysis.
Report Flag (A) : Compound tested over 100% or 1000 mg/g. The test result is within the method uncertainty and instrument result is not above the upper limit of quantitation. Value will be adjusted down to 100% or 1000 mg/kg in the reporting process.
Report Flag (B) : Blank contamination - The analyte was detected above one-half the reporting limit in an associated blank.
Report Flag (E) : Compound tested above the upper limit of quantitation.
Report Flag (Q) : One or more quality control criteria (for example, LCS recovery, surrogate spike recovery) failed.
Calculations
Cannabinoid Potency : Wet WT% = (Exported concentration ppm) x (Dilution) x (Extraction Vol./Wet wt mg) x 100
Total THC% = (%THCA) x 0.877 + (%THC)
Total CBD% = (%CBDA) x 0.877 + (%CBD)
Total THC (Dry WT)% = % total THC(wet) / [1-(% moisture/100)]
Total CBD (Dry WT)% = % total CBD(wet) / [1-(% moisture/100)]
Percentage Recovery : % Rec. = [(Amount measured) / (Known amount)] * 100
Disclaimers
Disposal : All marijuana and hemp products received by PREE will be disposed of following the OLCC’s rules for Marijuana Waste Management, regardless of product type, unless PREE is given specific disposal instructions for a product based on test results from state regulatory agencies.
Report ID: A4664-01 | Page 11 of 11 |
21.4 09/03/2021
Report: Definition
Rev
Residual Solvents
Analyte LOQAction LevelResult Units
Butanes 250 5000 ppm3 < LOQ
n-Butane 250 5000 ppm< LOQ
iso-Butane 250 5000 ppm< LOQ
Hexanes 174 290 ppm4 < LOQ
n-Hexane 174 290 ppm< LOQ
2-Methylpentane 174 290 ppm< LOQ
3-Methylpentane 174 290 ppm< LOQ
2,2-Dimethylbutane 174 290 ppm< LOQ 2,3-Dimethylbutane 174 290 ppm< LOQ
Pentanes 1400 5000 ppm5 < LOQ
n-Pentane 1400 5000 ppm< LOQ iso-Pentane 1400 5000 ppm< LOQ
Neopentane 250 5000 ppm< LOQ
Xylenes 1302 2170 ppm< LOQ
1,2-Dimethylbenzene 1302 2170 ppm< LOQ
1,3-Dimethylbenzene 1302 2170 ppm< LOQ
1,4-Dimethylbenzene 1302 2170 ppm< LOQ
Xylenes MP 1302 2170 ppm< LOQ
Ethyl benzene 1302 NA ppm< LOQ
2-Propanol (IPA) 1400 5000 ppm< LOQ
Acetone 1400 5000 ppm< LOQ
Acetonitrile 246 410 ppm< LOQ
Benzene 1.2 2 ppm< LOQ
Methanol 1000 3000 ppm< LOQ
Propane 250 5000 ppm< LOQ
Toluene 534 890 ppm< LOQ
Dichloromethane 360 600 ppm< LOQ
1,4-Dioxane 228 380 ppm< LOQ
2-Butanol 1400 5000 ppm< LOQ
2-Ethoxyethanol 96 160 ppm< LOQ
Cumene 42 70 ppm< LOQ
Cyclohexane 2278 3880 ppm< LOQ
Ethyl acetate 1400 5000 ppm< LOQ
Ethyl ether 1400 5000 ppm< LOQ
Ethylene glycol 558 620 ppm< LOQ
Ethylene oxide 30 50 ppm< LOQ
Heptane 1400 5000 ppm< LOQ
Isopropyl acetate 1400 5000 ppm< LOQ
Tetrahydrofuran 432 720 ppm< LOQ
Ethanol 1400 NA ppm7 < LOQ
N,N-Dimethylacetamide NA NATIC Water NA NATIC
Certificate
Date Sampled: 09/20/21 09:00
Date Accepted: 09/20/21
Batch ID: Batch Size:
Sampling Method/SOP: SOP.T.20.010
Date/Time Extracted: 09/21/21 14:18
Date/Time Analyzed: 09/22/21 11:17 Analysis Method/SOP: SOP.T.40.031
3 - Total butanes are calculated as sum of n-butanes (CAS# 106-97-8) and iso-butane (CAS# 75-28-5)
4 - Total hexanes are calculated as sum of n-hexane (CAS# 110-54-3), 2-methylpentane (CAS# 107-83-5), 3-methylpentane (CAS# 96-14-0), 2,2-dimethylbutane (CAS# 75-83-2), 2,3-dimethylbutane (CAS# 79-29-8)
5 - Total pentanes are calculated as sum of n-pentane (CAS# 109-66-0), iso-pentane (CAS# 78-78-4), and neo-pentane (CAS# 463-82-1)
6 - Total xylenes are calculated as 1,2-dimethylbenzene (CAS# 95-47-6), 1,3-dimethylbenzene (CAS# 106-42-3), and 1-4-dimethylbenzene (CAS# 106-42-3)
7 - Ethanol is not regulated under OAR-333-007-0410.
TIC - Tentatively Identified Compound not regulated under OAR-333-007-0410
Results above the action level fail Oregon state testing requirements and will be highlighted RED LOQ=Limit of Quantitation; PPM=Parts per million; ND=Not detected; NT=Not tested; AC=Above calibration range. PASS/FAIL status based on OAR 333-007.
Kawai Medeiros Manager -of Analysis EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com A4664-01
Matrix: Extract/Concentrate
Sample ID: P210847-01 PREE Labs METRC Batch #:
010-10087092BDA
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 1 of 3
Laboratory
9/22/2021
LOQ
Quality Control
Limits
Analyte Recovery LimitsLOQResult
Butanes < LOQ250 (ppm) < LOQ n-Butane < LOQ250 (ppm) < LOQ iso-Butane < LOQ250 (ppm) < LOQ Hexanes < LOQ174 (ppm) < LOQ n-Hexane < LOQ174 (ppm) < LOQ 2-Methylpentane < LOQ174 (ppm) < LOQ 3-Methylpentane < LOQ174 (ppm) < LOQ 2,2-Dimethylbutane < LOQ174 (ppm) < LOQ 2,3-Dimethylbutane < LOQ174 (ppm) < LOQ Pentanes < LOQ1400 (ppm) < LOQ n-Pentane < LOQ1400 (ppm) < LOQ iso-Pentane < LOQ1400 (ppm) < LOQ Neopentane < LOQ250 (ppm) < LOQ Xylenes < LOQ1302 (ppm) < LOQ
1,2-Dimethylbenzene< LOQ1302 (ppm) < LOQ 1,3-Dimethylbenzene< LOQ1302 (ppm) < LOQ 1,4-Dimethylbenzene< LOQ1302 (ppm) < LOQ Xylenes MP < LOQ1302 (ppm) < LOQ
Ethyl benzene < LOQ1302 (ppm) < LOQ 2-Propanol (IPA) < LOQ1400 (ppm) < LOQ
Acetone < LOQ1400 (ppm) < LOQ Acetonitrile < LOQ246 (ppm) < LOQ
Benzene < LOQ1.2 (ppm) < LOQ Methanol < LOQ1000 (ppm) < LOQ
Propane < LOQ250 (ppm) < LOQ Toluene < LOQ534 (ppm) < LOQ
Dichloromethane < LOQ360 (ppm) < LOQ 1,4-Dioxane < LOQ228 (ppm) < LOQ
2-Butanol < LOQ1400 (ppm) < LOQ 2-Ethoxyethanol < LOQ96 (ppm) < LOQ
Cumene < LOQ42 (ppm) < LOQ Cyclohexane < LOQ2278 (ppm) < LOQ
Ethyl acetate < LOQ1400 (ppm) < LOQ Ethyl ether < LOQ1400 (ppm) < LOQ
Ethylene glycol < LOQ558 (ppm) < LOQ Ethylene oxide < LOQ30 (ppm) < LOQ
Heptane < LOQ1400 (ppm) < LOQ Isopropyl acetate < LOQ1400 (ppm) < LOQ
Tetrahydrofuran < LOQ432 (ppm) < LOQ Ethanol < LOQ1400 (ppm) < LOQ
LCS(P21I072-BS1)
Analyzed: 09/22/21 11:17Extracted: 09/21/21 14:18
% Recovery LOQAnalyte Recovery Limits
Analyte Recovery LimitsLOQ% Recovery
Butanes 67.4 (ppm) 0-200 n-Butane 75.5 (ppm) 50-150 iso-Butane 59.3 (ppm) 50-150 Hexanes 101 (ppm) 0-200 n-Hexane 104 (ppm) 70-130 2-Methylpentane 104 (ppm) 70-130
3-Methylpentane 103 (ppm) 70-130 2,2-Dimethylbutane 105 (ppm) 70-130 2,3-Dimethylbutane 95.9 (ppm) 70-130 Pentanes 111 (ppm) 0-200 n-Pentane 96.9 (ppm) 70-130 iso-Pentane 88.6 (ppm) 70-130 Neopentane 78.8 (ppm) 50-150 Xylenes 97.6 (ppm) 0-200
1,2-Dimethylbenzene 96.4 (ppm) 70-130 1,3-Dimethylbenzene 99.3 (ppm) 70-130 1,4-Dimethylbenzene 99.5 (ppm) 70-130 Xylenes MP 97.5 (ppm) 0-200 Ethyl benzene 99.0 (ppm) 70-130 2-Propanol (IPA) 106 (ppm) 70-130
Acetone 100 (ppm) 70-130 Acetonitrile 98.1 (ppm) 70-130
Benzene 111 (ppm) 70-130 Methanol 113 (ppm) 70-130
Propane 56.2 (ppm) 50-150 Toluene 100 (ppm) 70-130
Dichloromethane 116 (ppm) 70-130 1,4-Dioxane 102 (ppm) 70-130
Kawai Medeiros Laboratory Manager - 9/22/2021Certificate of Analysis EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com
Batch: P21I072 - SOP.T.40.031 Solvents Blank(P21I072-BLK1) Result
Analyte Recovery
Analyzed: 09/22/21 11:17Extracted: 09/21/21 14:18
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 2 of 3
Quality Control
Batch: P21I072 - SOP.T.40.031 Solvents (Continued) LCS(P21I072-BS1)
Extracted: 09/21/21 14:18
% Recovery LOQAnalyte Recovery Limits
Certificate of Analysis
Analyzed: 09/22/21 11:17
Analyte Recovery LimitsLOQ% Recovery
2-Butanol 104 (ppm) 70-130 2-Ethoxyethanol 101 (ppm) 70-130
Cumene 104 (ppm) 50-150 Cyclohexane 109 (ppm) 70-130
Ethyl acetate 99.9 (ppm) 70-130 Ethyl ether 110 (ppm) 70-130
Ethylene glycol 83.9 (ppm) 70-130 Ethylene oxide 93.4 (ppm) 50-150
Heptane 107 (ppm) 70-130 Isopropyl acetate 103 (ppm) 70-130
Tetrahydrofuran 97.1 (ppm) 70-130
Kawai MedeirosManager - 9/22/2021
EVIO Labs Portland 14775 SW 74th Ave, Tigard, OR 97224 503-954-2562 / OLCC 010-10046111391 / www.EVIOLabs.com
This report shall not be reproduced, unless in its entirety, without written approval from EVIO Labs, Inc. Test results are confidential unless explicitly waived otherwise. All QC samples meet acceptance criteria of the method; data available upon request. The results relate only to the material or product analyzed for the sample included on this report. Page 3 of 3
Laboratory