고온고압반응기 - 일신오토클레이브

Page 1

HIGH PRESSURE REACTOR 고온·고압의 환경에서 화학합성, 분해,승화 및 추출 등의 많은 연구를 수행할 수 있는 연구용 반응기입니다. 온도, 압력, 용량 선정이 가능하며, 반응조건에 따라 다양한 옵션선택이 가능합니다.

Hydrothermal Synthesis of Zeolite (ZSM-5)

Hydrothermal Synthesis of ZrO2 Nanoparticles NH4OH Solution

SIO2 A12O2 H20 MOH(F)

Mordenite(MOR)

Rho(RHO)

H S

SI-O, AI-O bounds

UZM-5(UFI)

BET Surface Area

XRD (Crystal Structure)

Intensity (arb.unit)

Desorption 150 0.60

100

Pore Volume (cm3g-1nm-1)

Volume Adsorbed (cm3g-1,STP)

SEM (Size & Morphology)

TEM (Size & Morphology)

Adsorption

200

50

0.45 0.30 0.15 0.00

0 0.0

0.2

0.4

1

10 Pore Width / nm

0.6

0.8

100

1.0

M

OH

OR

OH

+

+

+

HOH

OH

M

M

OR

20

30

40

50

60

70

80

90

2 Theta (degree)

Ref. Journal of Colloid and Interface Science 350 (2010) 290–294

Hydrothermal Synthesis of Amorphous SiO2 M

10

BET Surface Area: 186 m2∙g-1

P/P0

M

Zirconia Nanoparticles

SSZ-13, SAPO-34(CHA)

Hydrolysis Reesterification Water Condensation Hydrolysis Alcohol Condensation Alcoholysis

M

OH

+

Hydrothermal Synthesis of MnO2 Nanorod

ROH Mn(CH3COOH)2 M Solution

KMnO4 Solution

M

O

M

+

HOH

M

O

M

+

ROH

Hydrothermal

Cal. 300-500 ℃ for 2h Amorphous SiO2

AFM (Size & Morphology)

XRD (Crystal Structure) XRD (Crystal Structure)

Intesity (arb.unit)

Intensity (arb.unit)

SEM (Size & Morphology)

10

20

30

40

50

60

70

80

10

90

20

30

40

50

60

2 Theta (degree)

2 Theta (degree)

Magnedrive Seal type (O-ring/gasket) (ℓ) 용량

Liner

) 온도(℃

Pressure Vessel

Port(Inlet/Outlet) 압력(kg/㎠)

우. 305-510

Thermocouple

대전광역시 유성구 테크노2로 255 (대덕 테크노밸리) Tel: 042.931-6100 Fax: 042.931-6103 Homepage: www.suflux.com E-mail: webmaster@suflux.com


Turn static files into dynamic content formats.

Create a flipbook
Issuu converts static files into: digital portfolios, online yearbooks, online catalogs, digital photo albums and more. Sign up and create your flipbook.