April 5, 2019
Mr. Drew Walker
Kimley-Horn & Associates
111 West Jackson Boulevard, Suite 1320
Chicago, Illinois 60604
Email: drew.walker@kimley-horn.com
ECS Project No. 53-2027
RE: Environmental Services Supporting Soil Sampling and Analysis – Calumet Country Club, 2136 175th Street, Homewood, Cook County, Illinois
Dear Mr. Walker:
At your request, ECS Midwest, LLC (ECS) was retained to perform an environmental soil analysis of the soil associated with the planned construction at the subject property. It is our understanding that the proposed construction activities will result in removal and disposal of excavation soils. To evaluate disposal options for the excavated soils, ECS performed a broad screening soil sampling and analysis as described below.
1.0 SOIL SAMPLING & ANALYSIS
1.1 Soil Sampling
In order to characterize the onsite soils slated for off-site disposal, ECS collected two soil samples from two geotechnical borings advanced within the anticipated excavation area (B-2 and S-2). Note that the soil samples collected for analysis were collected from the geotechnical borings and associated depth intervals (approximately 1-4 feet bgs) with the greatest potential for possible impacts (visual, olfactory, PID readings, etc.). ECS then placed the materials into appropriate sampling containers supplied by the laboratory, and delivered the samples to Test America under standard chain-of-custody procedures. Soil sampling and analysis was conducted in general accordance with 35 III. Adm. Code 1100, Clean Construction Demolition Debris Fill Operations and Uncontaminated Soil Fill Operations.
1.2 Soil Analysis
The soil samples were analyzed for a broad range of contaminants including the following:
VOCS – Volatile Organic Compounds via Method 5035/8260B
SVOCs – Semi-Volatile Organic Compounds via Method 8270D
PCBs – Polychlorinated biphenyls via Method 8082A
Pesticides – Via Method 8081B
Priority Pollutant Metals/Cyanide– Via Method 6010B/7471B/9014
pH – Via Method 9045D
Number of Samples Analytical Parameters Soil 2 VOCs, SVOCs, Pesticides, PCBs, PP Metals/Cyanide and pH
The sample analysis was performed by Test America of University Park, Illinois. Test America is an Illinois EPA accredited analytical laboratory. The results of the soil analysis are discussed in Section 2.1.
2.0 RESULTS OF SOIL SAMPLING
2.1 Results of Soil Analysis
The soil samples were analyzed for a broad variety of target compounds in order to assist in the potential disposal of the excavated soils. The target compounds and findings are provided below:
Sample ID Analysis
Test Results
VOCs BelowMaximumAllowableConcentrations
SVOCs BelowMaximumAllowableConcentrations
Metals Above Maximum Allowable Concentrations (Cr, Tl)
B-2
PCBs BelowMaximumAllowableConcentrations
Pesticides BelowMaximumAllowableConcentrations
Cyanide BelowMaximumAllowableConcentration pH WithinAcceptableRange
VOCs BelowMaximumAllowableConcentrations
SVOCs BelowMaximumAllowableConcentrations
Metals Above Maximum Allowable Concentrations (Cr, Tl)
S-2
PCBs BelowMaximumAllowableConcentrations
Pesticides BelowMaximumAllowableConcentrations
Cyanide BelowMaximumAllowableConcentration pH WithinAcceptableRange
Bold and Highlighted indicates compounds were detected above applicable MACs
The laboratory results were compared to the numerical standards listed in 35 Ill. Adm. Code 1100, Subpart F, Maximum Allowable Concentrations of Chemical Constituents in Uncontaminated Soil Used as Fill Material at Regulated Fill Operations (MACs) for the contaminants of concern. As indicated above, chromium and thallium were detected at concentrations in excess of their applicable MACs. Based on the elevated contaminant concentrations detected, it does not appear that the on-site soils are suitable for disposal at a CCDD landfill and will have to be taken to a landfill that is licensed to accept this type of waste stream. Please note that since the soils were found to be impacted, additional analyses (specific to the appropriate landfill that can accept this type of impacted soils) may be required prior to acceptance. Additionally, it should be noted that the landfill will make the final determination on whether or not they will choose to accept the waste. Copies of the laboratory report and the laboratory accreditation information are attached.
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CalumetCountryClub–CCDDReport#53-2027 April2019
CalumetCountryClub–CCDDReport#53-2027
April2019
If you have any questions regarding our findings or opinions, please contact either of the undersigned at (847) 279-0366. Thank you for retaining ECS Midwest, LLC for this evaluation.
Respectfully Submitted, ECS MIDWEST, LLC
Jason Warren
David T. Kwasiborski, CIAQM Senior Project Manager Principal Geologist
Attachment:LaboratoryAnalyticalReport
Z:\Office 53 Environmental\CCDD\2000-2099\2027 Calumet Country Club CCDD\53-2027 Calumet Country Club CCDD.doc
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CalumetCountryClub–CCDDReport#53-2027 April2019
Attachment I Laboratory Analytical Report
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago 2417 Bond Street University Park, IL 60484
Tel: (708)534-5200
TestAmerica Job ID: 500-160490-1
Client Project/Site: Calumet Country Club CCDD - 53-2027
For:
ECS Midwest LLC 1575 Barclay Blvd. Buffalo Grove, Illinois 60089
Attn: Jason Warren
Authorized for release by: 3/29/2019 5:58:51 PM
Jim Knapp, Project Manager II (630)758-0262
jim.knapp@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Table of Contents Client: ECS Midwest LLC Project/Site: Calumet Country Club CCDD - 53-2027 TestAmerica Job ID: 500-160490-1 Page 2 of 35 TestAmerica Chicago 3/29/2019 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Project/Site: Calumet Country Club CCDD - 53-2027
Job ID: 500-160490-1
Laboratory: TestAmerica Chicago
Narrative
Comments
No additional comments.
Receipt
Case Narrative
TestAmerica Job ID: 500-160490-1
Job Narrative 500-160490-1
The samples were received on 3/25/2019 12:30 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 3.6º C.
GC/MS VOA
The laboratory control sample and laboratory control sample duplicate (LCS/ LCSD) for 478012 recovered outside control limits for the following analyte: Chloroethane. This analyte was biased high in the LCS/ LCSD and was not detected in the associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
Method(s) 8081B: The %RPD between the primary and confirmation column exceeded 40% for 4,4'-DDD and Heptachlor epoxide for the following sample: B-2 (500-160490-1). The lower has been reported and qualified in accordance with the laboratory's SOP.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Chicago Page 3 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Detection Summary
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: B-2
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1
Client Sample ID: S-2
Lab Sample ID: 500-160490-2
☼ Heptachlor epoxide RL 0.0021 mg/Kg MDL 0.00072 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA 1 J 0.0011 8081B ☼ 4,4'-DDE 0.0021 mg/Kg 0.00034 Total/NA 1 0.0012 J 8081B ☼ 4,4'-DDD 0.0021 mg/Kg 0.00040 Total/NA 1 0.0012 J 8081B ☼ 4,4'-DDT 0.0021 mg/Kg 0.0011 Total/NA 1 0.0033 8081B ☼ Antimony 2.3 mg/Kg 0.46 Total/NA 1 0.67 J 6010B ☼ Arsenic 1.2 mg/Kg 0.40 Total/NA 1 11 6010B ☼ Beryllium 0.47 mg/Kg 0.11 Total/NA 1 0.95 6010B ☼ Cadmium 0.23 mg/Kg 0.042 Total/NA 1 0.20 J B 6010B ☼ Chromium 1.2 mg/Kg 0.58 Total/NA 1 22 6010B ☼ Copper 1.2 mg/Kg 0.33 Total/NA 1 28 6010B ☼ Lead 0.59 mg/Kg 0.27 Total/NA 1 19 6010B ☼ Nickel 1.2 mg/Kg 0.34 Total/NA 1 35 6010B ☼ Selenium 1.2 mg/Kg 0.69 Total/NA 1 0.78 J 6010B ☼ Silver 0.59 mg/Kg 0.15 Total/NA 1 3.7 6010B ☼ Thallium 1.2 mg/Kg 0.59 Total/NA 1 3.1 6010B ☼ Zinc 2.3 mg/Kg 1.0 Total/NA 1 56 6010B ☼ Mercury 0.020 mg/Kg 0.0066 Total/NA 1 0.041 7471B pH 0.2 SU 0.2 Total/NA 1 8.4 9045D
☼ Antimony RL 2.3 mg/Kg MDL 0.45 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA 1 J 0.52 6010B ☼ Arsenic 1.1 mg/Kg 0.39 Total/NA 1 9.2 6010B ☼ Beryllium 0.46 mg/Kg 0.11 Total/NA 1 0.92 6010B ☼ Cadmium 0.23 mg/Kg 0.041 Total/NA 1 0.27 B 6010B ☼ Chromium 1.1 mg/Kg 0.57 Total/NA 1 23 6010B ☼ Copper 1.1 mg/Kg 0.32 Total/NA 1 29 6010B ☼ Lead 0.57 mg/Kg 0.26 Total/NA 1 17 6010B ☼ Nickel 1.1 mg/Kg 0.33 Total/NA 1 42 6010B ☼ Silver 0.57 mg/Kg 0.15 Total/NA 1 3.3 6010B ☼ Thallium 1.1 mg/Kg 0.57 Total/NA 1 2.7 6010B ☼ Zinc 2.3 mg/Kg 1.0 Total/NA 1 70 6010B ☼ Mercury 0.019 mg/Kg 0.0063 Total/NA 1 0.078 7471B pH 0.2 SU 0.2 Total/NA 1 8.8 9045D TestAmerica Chicago
Page 4 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
This Detection Summary does not include radiochemical test results.
Client: ECS Midwest LLC
Method Summary
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Method Method Description Laboratory Protocol SW846 8260B Volatile Organic Compounds (GC/MS) TAL CHI SW846 8270D Semivolatile Organic Compounds (GC/MS) TAL CHI SW846 8081B Organochlorine Pesticides (GC) TAL CHI SW846 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CHI SW846 6010B Metals (ICP) TAL CHI SW846 7471B Mercury (CVAA) TAL CHI SW846 9014 Cyanide TAL CHI SW846 9045D pH TAL CHI EPA Moisture Percent Moisture TAL CHI SW846 3050B Preparation, Metals TAL CHI SW846 3541 Automated Soxhlet Extraction TAL CHI SW846 5035 Closed System Purge and Trap TAL CHI SW846 7471B Preparation, Mercury TAL CHI SW846 9010B Cyanide, Distillation TAL CHI Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical
Third Edition, November 1986 And Its Updates. Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 TestAmerica Chicago Page 5 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Methods",
Sample Summary
TestAmerica Job ID: 500-160490-1
Lab Sample ID Client Sample ID Received Collected Matrix 500-160490-1 B-2 Solid 03/25/19 09:00 03/25/19 12:30 500-160490-2 S-2 Solid 03/25/19 09:00 03/25/19 12:30 TestAmerica Chicago Page 6 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC Project/Site: Calumet Country Club CCDD - 53-2027
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: B-2
Collected: 03/25/19 09:00
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1
Matrix: Solid Date
Percent Solids: 80.0 Date Received:
12:30 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Chloromethane ND 0.0045 0.0018 mg/Kg ☼ 03/25/19 17:17 03/28/19 15:49 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.0018 0.00079 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Vinyl chloride ND 0.0045 0.0017 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Bromomethane ND 0.0045 0.0013 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Chloroethane ND * 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,1-Dichloroethene ND 0.018 0.0078 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Acetone ND 0.0045 0.00093 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Carbon disulfide ND 0.0045 0.0018 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Methylene Chloride ND 0.0018 0.00079 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ trans-1,2-Dichloroethene ND 0.0018 0.00052 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Methyl tert-butyl ether ND 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,1-Dichloroethane ND 0.0018 0.00050 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ cis-1,2-Dichloroethene ND 0.0045 0.0020 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Methyl Ethyl Ketone ND 0.0018 0.00062 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Chloroform ND 0.0018 0.00060 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,1,1-Trichloroethane ND 0.0018 0.00052 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Carbon tetrachloride ND 0.0018 0.00045 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Benzene ND 0.0045 0.0014 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,2-Dichloroethane ND 0.0018 0.00060 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Trichloroethene ND 0.0018 0.00046 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,2-Dichloropropane ND 0.0018 0.00036 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Bromodichloromethane ND 0.0018 0.00054 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ cis-1,3-Dichloropropene ND 0.0045 0.0013 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ methyl isobutyl ketone ND 0.0018 0.00045 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Toluene ND 0.0018 0.00063 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ trans-1,3-Dichloropropene ND 0.0018 0.00076 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,1,2-Trichloroethane ND 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Tetrachloroethene ND 0.0045 0.0014 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 2-Hexanone ND 0.0018 0.00058 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Dibromochloromethane ND 0.0018 0.00066 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Chlorobenzene ND 0.0018 0.00085 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Ethylbenzene ND 0.0036 0.00057 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Xylenes, Total ND 0.0018 0.00054 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Styrene ND 0.0018 0.00052 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ Bromoform ND 0.0018 0.00057 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,1,2,2-Tetrachloroethane ND 0.0018 0.00063 mg/Kg 03/25/19 17:17 03/28/19 15:49 1 ☼ 1,3-Dichloropropene, Total ND 1,2-Dichloroethane-d4 (Surr) 95 70 - 134 03/25/19 17:17 03/28/19 15:49 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Toluene-d8 (Surr) 97 03/25/19 17:17 03/28/19 15:49 1 75 - 124 4-Bromofluorobenzene (Surr) 92 03/25/19 17:17 03/28/19 15:49 1 75 - 131 Dibromofluoromethane 95 03/25/19 17:17 03/28/19 15:49 1 75 - 126 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Phenol ND 0.20 0.088 mg/Kg ☼ 03/25/19 16:20 03/26/19 11:54 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.060 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Bis(2-chloroethyl)ether ND 0.20 0.045 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 1,3-Dichlorobenzene ND 0.20 0.051 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 1,4-Dichlorobenzene ND 0.20 0.048 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 1,2-Dichlorobenzene ND TestAmerica Chicago Page 7 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
03/25/19
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: B-2
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1
Solid Date Collected: 03/25/19 09:00
Solids: 80.0 Date Received: 03/25/19 12:30
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Percent
Matrix:
RL MDL 2-Methylphenol ND 0.20 0.064 mg/Kg ☼ 03/25/19 16:20 03/26/19 11:54 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.046 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,2'-oxybis[1-chloropropane] ND 0.080 0.049 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ N-Nitrosodi-n-propylamine ND 0.20 0.060 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Hexachloroethane ND 0.20 0.068 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2-Chlorophenol ND 0.040 0.0099 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Nitrobenzene ND 0.20 0.041 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Bis(2-chloroethoxy)methane ND 0.20 0.043 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 1,2,4-Trichlorobenzene ND 0.20 0.045 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Isophorone ND 0.40 0.15 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4-Dimethylphenol ND 0.20 0.063 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Hexachlorobutadiene ND 0.040 0.0061 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Naphthalene ND 0.40 0.094 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4-Dichlorophenol ND 0.80 0.19 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Chloroaniline ND 0.40 0.14 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4,6-Trichlorophenol ND 0.40 0.091 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4,5-Trichlorophenol ND 0.80 0.23 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Hexachlorocyclopentadiene ND 0.080 0.0073 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2-Methylnaphthalene ND 0.20 0.054 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2-Nitroaniline ND 0.20 0.044 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2-Chloronaphthalene ND 0.40 0.14 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Chloro-3-methylphenol ND 0.20 0.078 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,6-Dinitrotoluene ND 0.40 0.094 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2-Nitrophenol ND 0.40 0.12 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 3-Nitroaniline ND 0.20 0.052 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Dimethyl phthalate ND 0.80 0.70 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4-Dinitrophenol ND 0.040 0.0052 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Acenaphthylene ND 0.20 0.063 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 2,4-Dinitrotoluene ND 0.040 0.0071 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Acenaphthene ND 0.20 0.047 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Dibenzofuran ND 0.80 0.38 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Nitrophenol ND 0.040 0.0056 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Fluorene ND 0.40 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Nitroaniline ND 0.20 0.052 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Bromophenyl phenyl ether ND 0.080 0.0092 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Hexachlorobenzene ND 0.20 0.067 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Diethyl phthalate ND 0.20 0.046 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4-Chlorophenyl phenyl ether ND 0.80 0.64 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Pentachlorophenol ND 0.20 0.047 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ N-Nitrosodiphenylamine ND 0.80 0.32 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 4,6-Dinitro-2-methylphenol ND 0.040 0.0055 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Phenanthrene ND 0.040 0.0066 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Anthracene ND 0.20 0.099 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Carbazole ND 0.20 0.061 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Di-n-butyl phthalate ND 0.040 0.0074 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Fluoranthene ND 0.040 0.0079 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Pyrene ND 0.20 0.076 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Butyl benzyl phthalate ND 0.040 0.0054 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Benzo[a]anthracene ND 0.040 0.011 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Chrysene ND TestAmerica Chicago Page 8 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1
Date Collected: 03/25/19 09:00
Client Sample ID: B-2 Matrix: Solid
Solids: 80.0 Date Received: 03/25/19 12:30
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Percent
RL MDL 3,3'-Dichlorobenzidine ND 0.20 0.056 mg/Kg ☼ 03/25/19 16:20 03/26/19 11:54 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.073 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Bis(2-ethylhexyl) phthalate ND 0.20 0.065 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Di-n-octyl phthalate ND 0.040 0.0086 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Benzo[b]fluoranthene ND 0.040 0.012 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Benzo[k]fluoranthene ND 0.040 0.0077 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Benzo[a]pyrene ND 0.040 0.010 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Indeno[1,2,3-cd]pyrene ND 0.040 0.0077 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Dibenz(a,h)anthracene ND 0.040 0.013 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ Benzo[g,h,i]perylene ND 0.20 0.066 mg/Kg 03/25/19 16:20 03/26/19 11:54 1 ☼ 3 & 4 Methylphenol ND 2-Fluorophenol 91 31 - 166 03/25/19 16:20 03/26/19 11:54 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Phenol-d5 100 03/25/19 16:20 03/26/19 11:54 1 30 - 153 Nitrobenzene-d5 82 03/25/19 16:20 03/26/19 11:54 1 37 - 147 2-Fluorobiphenyl 86 03/25/19 16:20 03/26/19 11:54 1 43 - 145 2,4,6-Tribromophenol 99 03/25/19 16:20 03/26/19 11:54 1 31 - 143 Terphenyl-d14 95 03/25/19 16:20 03/26/19 11:54 1 42 - 157 Method: 8081B - Organochlorine Pesticides (GC) RL MDL alpha-BHC ND 0.0021 0.00052 mg/Kg ☼ 03/26/19 07:44 03/26/19 23:01 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.0021 0.00063 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ beta-BHC ND 0.0021 0.00064 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ delta-BHC ND 0.0021 0.00044 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ gamma-BHC (Lindane) ND 0.0021 0.00085 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Heptachlor ND 0.0021 0.00084 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Aldrin ND 0.0021 0.00072 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Heptachlor epoxide 0.0011 J 0.0021 0.00089 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endosulfan I ND 0.0021 0.00028 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Dieldrin ND 0.0021 0.00034 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ 4,4'-DDE 0.0012 J 0.0021 0.00028 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endrin ND 0.0021 0.00033 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endosulfan II ND 0.0021 0.00040 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ 4,4'-DDD 0.0012 J 0.0021 0.00037 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endosulfan sulfate ND 0.0021 0.0011 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ 4,4'-DDT 0.0033 0.010 0.00039 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Methoxychlor ND 0.0021 0.0010 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ cis-Chlordane ND 0.0021 0.00053 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ trans-Chlordane ND 0.020 0.0086 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Toxaphene ND 0.0021 0.00034 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endrin aldehyde ND 0.0021 0.00046 mg/Kg 03/26/19 07:44 03/26/19 23:01 1 ☼ Endrin ketone ND DCB Decachlorobiphenyl 93 33 - 148 03/26/19 07:44 03/26/19 23:01 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Tetrachloro-m-xylene 78 03/26/19 07:44 03/26/19 23:01 1 30 - 121
Biphenyls
RL MDL PCB-1016 ND 0.020 0.0072 mg/Kg ☼ 03/26/19 07:44 03/26/19 16:21 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica Chicago Page 9 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Method: 8082A -
Polychlorinated
(PCBs) by Gas Chromatography
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: B-2
Collected: 03/25/19 09:00
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1
Matrix: Solid Date
Percent Solids:
Date
Method: 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) RL MDL PCB-1221 ND 0.020 0.0089 mg/Kg ☼ 03/26/19 07:44 03/26/19 16:21 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.020 0.0088 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ PCB-1232 ND 0.020 0.0067 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ PCB-1242 ND 0.020 0.0080 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ PCB-1248 ND 0.020 0.0044 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ PCB-1254 ND 0.020 0.010 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ PCB-1260 ND 0.020 0.0039 mg/Kg 03/26/19 07:44 03/26/19 16:21 1 ☼ Polychlorinated biphenyls, Total ND Tetrachloro-m-xylene 67 49 - 129 03/26/19 07:44 03/26/19 16:21 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery DCB Decachlorobiphenyl 76 03/26/19 07:44 03/26/19 16:21 1 37 - 121 Method: 6010B - Metals (ICP) RL MDL Antimony 0.67 J 2.3 0.46 mg/Kg ☼ 03/26/19 16:18 03/27/19 12:11 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.2 0.40 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Arsenic 11 0.47 0.11 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Beryllium 0.95 0.23 0.042 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Cadmium 0.20 J B 1.2 0.58 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Chromium 22 1.2 0.33 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Copper 28 0.59 0.27 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Lead 19 1.2 0.34 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Nickel 35 1.2 0.69 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Selenium 0.78 J 0.59 0.15 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Silver 3.7 1.2 0.59 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Thallium 3.1 2.3 1.0 mg/Kg 03/26/19 16:18 03/27/19 12:11 1 ☼ Zinc 56 Method: 7471B - Mercury (CVAA) RL MDL Mercury 0.041 0.020 0.0066 mg/Kg ☼ 03/26/19 14:00 03/27/19 10:02 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL MDL Cyanide, Total ND 0.60 0.21 mg/Kg ☼ 03/27/19 12:10 03/27/19 14:47 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.2 0.2 SU 03/29/19 13:01 1 pH 8.4 TestAmerica Chicago Page 10 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
80.0
Received: 03/25/19 12:30
-
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: S-2
Collected: 03/25/19 09:00
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-2
Matrix: Solid Date
Percent Solids: 83.4 Date Received:
Method: 8260B
Volatile Organic Compounds (GC/MS) RL MDL Chloromethane ND 0.0044 0.0018 mg/Kg ☼ 03/25/19 17:17 03/28/19 16:15 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.0018 0.00078 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Vinyl chloride ND 0.0044 0.0017 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Bromomethane ND 0.0044 0.0013 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Chloroethane ND * 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,1-Dichloroethene ND 0.018 0.0077 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Acetone ND 0.0044 0.00092 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Carbon disulfide ND 0.0044 0.0017 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Methylene Chloride ND 0.0018 0.00078 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ trans-1,2-Dichloroethene ND 0.0018 0.00052 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Methyl tert-butyl ether ND 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,1-Dichloroethane ND 0.0018 0.00049 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ cis-1,2-Dichloroethene ND 0.0044 0.0020 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Methyl Ethyl Ketone ND 0.0018 0.00061 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Chloroform ND 0.0018 0.00059 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,1,1-Trichloroethane ND 0.0018 0.00051 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Carbon tetrachloride ND 0.0018 0.00045 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Benzene ND 0.0044 0.0014 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,2-Dichloroethane ND 0.0018 0.00060 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Trichloroethene ND 0.0018 0.00046 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,2-Dichloropropane ND 0.0018 0.00036 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Bromodichloromethane ND 0.0018 0.00053 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ cis-1,3-Dichloropropene ND 0.0044 0.0013 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ methyl isobutyl ketone ND 0.0018 0.00045 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Toluene ND 0.0018 0.00062 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ trans-1,3-Dichloropropene ND 0.0018 0.00076 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,1,2-Trichloroethane ND 0.0018 0.00060 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Tetrachloroethene ND 0.0044 0.0014 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 2-Hexanone ND 0.0018 0.00058 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Dibromochloromethane ND 0.0018 0.00065 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Chlorobenzene ND 0.0018 0.00085 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Ethylbenzene ND 0.0035 0.00057 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Xylenes, Total ND 0.0018 0.00053 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Styrene ND 0.0018 0.00052 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ Bromoform ND 0.0018 0.00057 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,1,2,2-Tetrachloroethane ND 0.0018 0.00062 mg/Kg 03/25/19 17:17 03/28/19 16:15 1 ☼ 1,3-Dichloropropene, Total ND 1,2-Dichloroethane-d4 (Surr) 96 70 - 134 03/25/19 17:17 03/28/19 16:15 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Toluene-d8 (Surr) 96 03/25/19 17:17 03/28/19 16:15 1 75 - 124 4-Bromofluorobenzene (Surr) 91 03/25/19 17:17 03/28/19 16:15 1 75 - 131 Dibromofluoromethane 94 03/25/19 17:17 03/28/19 16:15 1 75 - 126 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Phenol ND 0.20 0.088 mg/Kg ☼ 03/25/19 16:20 03/26/19 12:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.059 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Bis(2-chloroethyl)ether ND 0.20 0.045 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 1,3-Dichlorobenzene ND 0.20 0.051 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 1,4-Dichlorobenzene ND 0.20 0.047 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 1,2-Dichlorobenzene ND TestAmerica Chicago Page 11 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
03/25/19 12:30
-
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-2
Date Collected: 03/25/19 09:00
Client Sample ID: S-2 Matrix: Solid
Solids: 83.4 Date Received: 03/25/19 12:30
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Percent
RL MDL 2-Methylphenol ND 0.20 0.064 mg/Kg ☼ 03/25/19 16:20 03/26/19 12:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.046 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,2'-oxybis[1-chloropropane] ND 0.080 0.048 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ N-Nitrosodi-n-propylamine ND 0.20 0.060 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Hexachloroethane ND 0.20 0.068 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2-Chlorophenol ND 0.039 0.0099 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Nitrobenzene ND 0.20 0.040 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Bis(2-chloroethoxy)methane ND 0.20 0.043 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 1,2,4-Trichlorobenzene ND 0.20 0.045 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Isophorone ND 0.39 0.15 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4-Dimethylphenol ND 0.20 0.062 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Hexachlorobutadiene ND 0.039 0.0061 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Naphthalene ND 0.39 0.094 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4-Dichlorophenol ND 0.80 0.19 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Chloroaniline ND 0.39 0.14 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4,6-Trichlorophenol ND 0.39 0.090 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4,5-Trichlorophenol ND 0.80 0.23 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Hexachlorocyclopentadiene ND 0.080 0.0073 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2-Methylnaphthalene ND 0.20 0.053 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2-Nitroaniline ND 0.20 0.044 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2-Chloronaphthalene ND 0.39 0.13 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Chloro-3-methylphenol ND 0.20 0.078 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,6-Dinitrotoluene ND 0.39 0.094 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2-Nitrophenol ND 0.39 0.12 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 3-Nitroaniline ND 0.20 0.052 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Dimethyl phthalate ND 0.80 0.70 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4-Dinitrophenol ND 0.039 0.0052 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Acenaphthylene ND 0.20 0.063 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 2,4-Dinitrotoluene ND 0.039 0.0071 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Acenaphthene ND 0.20 0.046 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Dibenzofuran ND 0.80 0.38 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Nitrophenol ND 0.039 0.0056 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Fluorene ND 0.39 0.17 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Nitroaniline ND 0.20 0.052 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Bromophenyl phenyl ether ND 0.080 0.0092 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Hexachlorobenzene ND 0.20 0.067 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Diethyl phthalate ND 0.20 0.046 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4-Chlorophenyl phenyl ether ND 0.80 0.64 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Pentachlorophenol ND 0.20 0.047 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ N-Nitrosodiphenylamine ND 0.80 0.32 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 4,6-Dinitro-2-methylphenol ND 0.039 0.0055 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Phenanthrene ND 0.039 0.0066 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Anthracene ND 0.20 0.099 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Carbazole ND 0.20 0.060 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Di-n-butyl phthalate ND 0.039 0.0074 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Fluoranthene ND 0.039 0.0079 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Pyrene ND 0.20 0.075 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Butyl benzyl phthalate ND 0.039 0.0053 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Benzo[a]anthracene ND 0.039 0.011 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Chrysene ND TestAmerica Chicago Page 12 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-2
Date Collected: 03/25/19 09:00
Client Sample ID: S-2 Matrix: Solid
Date Received: 03/25/19 12:30
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Solids: 83.4
Percent
RL MDL 3,3'-Dichlorobenzidine ND 0.20 0.055 mg/Kg ☼ 03/25/19 16:20 03/26/19 12:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.20 0.072 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Bis(2-ethylhexyl) phthalate ND 0.20 0.065 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Di-n-octyl phthalate ND 0.039 0.0086 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Benzo[b]fluoranthene ND 0.039 0.012 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Benzo[k]fluoranthene ND 0.039 0.0077 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Benzo[a]pyrene ND 0.039 0.010 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Indeno[1,2,3-cd]pyrene ND 0.039 0.0077 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Dibenz(a,h)anthracene ND 0.039 0.013 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ Benzo[g,h,i]perylene ND 0.20 0.066 mg/Kg 03/25/19 16:20 03/26/19 12:18 1 ☼ 3 & 4 Methylphenol ND 2-Fluorophenol 102 31 - 166 03/25/19 16:20 03/26/19 12:18 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Phenol-d5 103 03/25/19 16:20 03/26/19 12:18 1 30 - 153 Nitrobenzene-d5 90 03/25/19 16:20 03/26/19 12:18 1 37 - 147 2-Fluorobiphenyl 91 03/25/19 16:20 03/26/19 12:18 1 43 - 145 2,4,6-Tribromophenol 97 03/25/19 16:20 03/26/19 12:18 1 31 - 143 Terphenyl-d14 102 03/25/19 16:20 03/26/19 12:18 1 42 - 157 Method: 8081B - Organochlorine Pesticides (GC) RL MDL alpha-BHC ND 0.0020 0.00050 mg/Kg ☼ 03/26/19 07:44 03/26/19 23:21 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.0020 0.00062 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ beta-BHC ND 0.0020 0.00063 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ delta-BHC ND 0.0020 0.00043 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ gamma-BHC (Lindane) ND 0.0020 0.00083 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Heptachlor ND 0.0020 0.00083 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Aldrin ND 0.0020 0.00071 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Heptachlor epoxide ND 0.0020 0.00087 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endosulfan I ND 0.0020 0.00027 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Dieldrin ND 0.0020 0.00033 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ 4,4'-DDE ND 0.0020 0.00028 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endrin ND 0.0020 0.00032 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endosulfan II ND 0.0020 0.00040 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ 4,4'-DDD ND 0.0020 0.00036 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endosulfan sulfate ND 0.0020 0.0010 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ 4,4'-DDT ND 0.0099 0.00039 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Methoxychlor ND 0.0020 0.0010 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ cis-Chlordane ND 0.0020 0.00052 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ trans-Chlordane ND 0.020 0.0084 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Toxaphene ND 0.0020 0.00033 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endrin aldehyde ND 0.0020 0.00045 mg/Kg 03/26/19 07:44 03/26/19 23:21 1 ☼ Endrin ketone ND DCB Decachlorobiphenyl 84 33 - 148 03/26/19 07:44 03/26/19 23:21 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Tetrachloro-m-xylene 75 03/26/19 07:44 03/26/19 23:21 1 30 - 121
RL MDL PCB-1016 ND 0.020 0.0070 mg/Kg ☼ 03/26/19 07:44 03/26/19 16:41 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier TestAmerica Chicago Page 13 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Method:
Client: ECS Midwest LLC
Client Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: S-2
Collected: 03/25/19 09:00
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-2
Matrix: Solid Date
Percent Solids:
Date
Method: 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) RL MDL PCB-1221 ND 0.020 0.0087 mg/Kg ☼ 03/26/19 07:44 03/26/19 16:41 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.020 0.0087 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ PCB-1232 ND 0.020 0.0065 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ PCB-1242 ND 0.020 0.0078 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ PCB-1248 ND 0.020 0.0043 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ PCB-1254 ND 0.020 0.0098 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ PCB-1260 ND 0.020 0.0038 mg/Kg 03/26/19 07:44 03/26/19 16:41 1 ☼ Polychlorinated biphenyls, Total ND Tetrachloro-m-xylene 70 49 - 129 03/26/19 07:44 03/26/19 16:41 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery DCB Decachlorobiphenyl 80 03/26/19 07:44 03/26/19 16:41 1 37 - 121 Method: 6010B - Metals (ICP) RL MDL Antimony 0.52 J 2.3 0.45 mg/Kg ☼ 03/26/19 16:18 03/27/19 12:31 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.1 0.39 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Arsenic 9.2 0.46 0.11 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Beryllium 0.92 0.23 0.041 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Cadmium 0.27 B 1.1 0.57 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Chromium 23 1.1 0.32 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Copper 29 0.57 0.26 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Lead 17 1.1 0.33 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Nickel 42 1.1 0.67 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Selenium ND 0.57 0.15 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Silver 3.3 1.1 0.57 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Thallium 2.7 2.3 1.0 mg/Kg 03/26/19 16:18 03/27/19 12:31 1 ☼ Zinc 70 Method: 7471B - Mercury (CVAA) RL MDL Mercury 0.078 0.019 0.0063 mg/Kg ☼ 03/26/19 14:00 03/27/19 10:14 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL MDL Cyanide, Total ND 0.58 0.20 mg/Kg ☼ 03/27/19 12:10 03/27/19 14:48 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.2 0.2 SU 03/29/19 13:08 1 pH 8.8 TestAmerica Chicago Page 14 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
83.4
Received: 03/25/19 12:30
-
Client: ECS Midwest LLC
Definitions/Glossary
Project/Site: Calumet Country Club CCDD - 53-2027
Qualifiers
TestAmerica Job ID: 500-160490-1
GC/MS VOA Qualifier Description
Qualifier
* LCS or LCSD is outside acceptance limits.
GC Semi VOA
Qualifier
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
B Compound was found in the blank and sample.
Glossary
Abbreviation
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Chicago Page 15 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Association Summary
Project/Site: Calumet Country Club CCDD - 53-2027
GC/MS VOA
Prep Batch: 477800
Batch: 478012
GC/MS Semi VOA
Batch: 477587
Batch: 477635
GC Semi VOA
Batch: 477625
Batch: 477658
Analysis Batch: 477741
TestAmerica Job ID: 500-160490-1
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035 500-160490-1 B-2 Total/NA Solid 5035 500-160490-2 S-2 Total/NA Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 477800 500-160490-1 B-2 Total/NA Solid 8260B 477800 500-160490-2 S-2 Total/NA Solid 8260B MB 500-478012/8 Method Blank Total/NA Solid 8260B LCS 500-478012/6 Lab Control Sample Total/NA Solid 8260B LCSD 500-478012/9 Lab Control Sample Dup Total/NA
Prep
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3541 500-160490-1 B-2 Total/NA Solid 3541 500-160490-2 S-2 Total/NA Solid 3541 MB 500-477587/1-A Method Blank Total/NA Solid 3541 LCS 500-477587/2-A Lab Control Sample Total/NA Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270D 477587 500-160490-1 B-2 Total/NA Solid 8270D 477587 500-160490-2 S-2 Total/NA Solid 8270D 477587 MB 500-477587/1-A Method Blank Total/NA Solid 8270D 477587 LCS 500-477587/2-A Lab Control Sample Total/NA
Prep
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3541 500-160490-1 B-2 Total/NA Solid 3541 500-160490-2 S-2 Total/NA Solid 3541 MB 500-477625/1-A Method Blank Total/NA Solid 3541 LCS 500-477625/2-A Lab Control Sample Total/NA Solid 3541 LCS 500-477625/3-A Lab Control Sample Total/NA Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8082A 477625 500-160490-1 B-2 Total/NA Solid 8082A 477625 500-160490-2 S-2 Total/NA Solid 8082A 477625 MB 500-477625/1-A Method Blank Total/NA Solid 8082A 477625 LCS 500-477625/3-A Lab Control Sample Total/NA
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8081B 477625 500-160490-1 B-2 Total/NA Solid 8081B 477625 500-160490-2 S-2 Total/NA Solid 8081B 477625 MB 500-477625/1-A Method Blank Total/NA Solid 8081B 477625 LCS 500-477625/2-A Lab Control Sample Total/NA TestAmerica Chicago Page 16 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Association Summary
Project/Site: Calumet Country Club CCDD - 53-2027
Metals
Prep Batch: 477684
Batch: 477754
Analysis Batch: 477884
Batch: 477904
General Chemistry
Analysis Batch: 477605
Prep Batch: 477872
TestAmerica Job ID: 500-160490-1
Batch: 477933
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 500-160490-1 B-2 Total/NA Solid 7471B 500-160490-2 S-2 Total/NA Solid 7471B MB 500-477684/12-A Method Blank Total/NA Solid 7471B LCS 500-477684/13-A Lab Control Sample Total/NA Solid 7471B 500-160490-1 MS B-2 Total/NA Solid 7471B 500-160490-1 MSD B-2 Total/NA Solid 7471B 500-160490-1 DU B-2 Total/NA Prep
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3050B 500-160490-1 B-2 Total/NA Solid 3050B 500-160490-2 S-2 Total/NA Solid 3050B MB 500-477754/1-A Method Blank Total/NA Solid 3050B LCS 500-477754/2-A Lab Control Sample Total/NA
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 477684 500-160490-1 B-2 Total/NA Solid 7471B 477684 500-160490-2 S-2 Total/NA Solid 7471B 477684 MB 500-477684/12-A Method Blank Total/NA Solid 7471B 477684 LCS 500-477684/13-A Lab Control Sample Total/NA Solid 7471B 477684 500-160490-1 MS B-2 Total/NA Solid 7471B 477684 500-160490-1 MSD B-2 Total/NA Solid 7471B 477684 500-160490-1 DU B-2 Total/NA
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010B 477754 500-160490-1 B-2 Total/NA Solid 6010B 477754 500-160490-2 S-2 Total/NA Solid 6010B 477754 MB 500-477754/1-A Method Blank Total/NA Solid 6010B 477754 LCS 500-477754/2-A Lab Control Sample Total/NA
Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 500-160490-1 B-2 Total/NA Solid Moisture 500-160490-2 S-2 Total/NA
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 9010B 500-160490-1 B-2 Total/NA Solid 9010B 500-160490-2 S-2 Total/NA Solid 9010B MB 500-477872/1-A Method Blank Total/NA Solid 9010B LCS 500-477872/2-A Lab Control Sample Total/NA Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 9014 477872 500-160490-1 B-2 Total/NA Solid 9014 477872 500-160490-2 S-2 Total/NA TestAmerica Chicago Page 17 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Association Summary
Project/Site: Calumet Country Club CCDD - 53-2027
General Chemistry (Continued)
Analysis Batch: 477933 (Continued)
TestAmerica Job ID: 500-160490-1
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 9014 477872 MB 500-477872/1-A Method Blank Total/NA Solid 9014 477872 LCS 500-477872/2-A Lab Control Sample Total/NA Analysis
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 9045D 500-160490-1 B-2 Total/NA Solid 9045D 500-160490-2 S-2 Total/NA TestAmerica Chicago Page 18 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Batch: 478405
Client: ECS Midwest LLC
Surrogate Summary
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8260B - Volatile Organic Compounds (GC/MS)
TestAmerica Job ID: 500-160490-1
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Method: 8081B - Organochlorine Pesticides (GC)
Prep Type:
Matrix:
Lab Sample ID Client Sample ID (70-134) (75-124) (75-131) (75-126) DCA TOL BFB DBFM 95 97 92 95 500-160490-1 Percent Surrogate Recovery (Acceptance Limits) B-2 96 96 91 94 500-160490-2 S-2 88 94 90 94 LCS 500-478012/6 Lab Control Sample 89 93 90 94 LCSD 500-478012/9 Lab Control Sample Dup 88 97 90 90 MB 500-478012/8 Method Blank Surrogate Legend DCA = 1,2-Dichloroethane-d4 (Surr) TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene (Surr) DBFM = Dibromofluoromethane
Total/NA
Solid
Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (31-166) (30-153) (37-147) (43-145) (31-143) (42-157) 2FP PHL NBZ FBP TBP TPHL 91 100 82 86 99 95 500-160490-1 Percent Surrogate Recovery (Acceptance Limits) B-2 102 103 90 97 91 102 500-160490-2 S-2 109 114 99 113 97 99 LCS 500-477587/2-A Lab Control Sample 105 103 92 94 95 104 MB 500-477587/1-A Method Blank Surrogate Legend 2FP = 2-Fluorophenol PHL = Phenol-d5 NBZ = Nitrobenzene-d5 FBP =
2-Fluorobiphenyl TBP = 2,4,6-Tribromophenol TPHL = Terphenyl-d14
Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (33-148) (30-121) DCBP1 TCX1 93 78 500-160490-1 Percent Surrogate Recovery (Acceptance Limits) B-2 84 75 500-160490-2 S-2 103 92 LCS 500-477625/2-A Lab Control Sample 102 90 MB 500-477625/1-A Method Blank Surrogate Legend DCBP = DCB Decachlorobiphenyl TCX = Tetrachloro-m-xylene TestAmerica Chicago Page 19 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Surrogate Summary
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Prep
Matrix: Solid Lab Sample ID Client Sample ID (49-129) (37-121) TCX1 DCBP1 67 76 500-160490-1 Percent Surrogate Recovery (Acceptance Limits) B-2 70 80 500-160490-2 S-2 78 79 LCS 500-477625/3-A Lab Control Sample 91 89 MB 500-477625/1-A Method Blank Surrogate Legend TCX = Tetrachloro-m-xylene DCBP = DCB Decachlorobiphenyl TestAmerica Chicago Page 20 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Type: Total/NA
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8260B - Volatile Organic Compounds (GC/MS)
ID: MB 500-478012/8
478012
TestAmerica Job ID: 500-160490-1
Client Sample ID:
Lab
Matrix: Solid Prep Type: Total/NA Analysis
RL MDL Chloromethane ND 0.0050 0.0020 mg/Kg 03/28/19 11:35 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.00089 0.0020 mg/Kg 03/28/19 11:35 1 Vinyl chloride ND 0.0019 0.0050 mg/Kg 03/28/19 11:35 1 Bromomethane ND 0.0015 0.0050 mg/Kg 03/28/19 11:35 1 Chloroethane ND 0.00069 0.0020 mg/Kg 03/28/19 11:35 1 1,1-Dichloroethene ND 0.0087 0.020 mg/Kg 03/28/19 11:35 1 Acetone ND 0.0010 0.0050 mg/Kg 03/28/19 11:35 1 Carbon disulfide ND 0.0020 0.0050 mg/Kg 03/28/19 11:35 1 Methylene Chloride ND 0.00089 0.0020 mg/Kg 03/28/19 11:35 1 trans-1,2-Dichloroethene ND 0.00059 0.0020 mg/Kg 03/28/19 11:35 1 Methyl tert-butyl ether ND 0.00069 0.0020 mg/Kg 03/28/19 11:35 1 1,1-Dichloroethane ND 0.00056 0.0020 mg/Kg 03/28/19 11:35 1 cis-1,2-Dichloroethene ND 0.0022 0.0050 mg/Kg 03/28/19 11:35 1 Methyl Ethyl Ketone ND 0.00069 0.0020 mg/Kg 03/28/19 11:35 1 Chloroform ND 0.00067 0.0020 mg/Kg 03/28/19 11:35 1 1,1,1-Trichloroethane ND 0.00058 0.0020 mg/Kg 03/28/19 11:35 1 Carbon tetrachloride ND 0.00051 0.0020 mg/Kg 03/28/19 11:35 1 Benzene ND 0.0016 0.0050 mg/Kg 03/28/19 11:35 1 1,2-Dichloroethane ND 0.00068 0.0020 mg/Kg 03/28/19 11:35 1 Trichloroethene ND 0.00052 0.0020 mg/Kg 03/28/19 11:35 1 1,2-Dichloropropane ND 0.00041 0.0020 mg/Kg 03/28/19 11:35 1 Bromodichloromethane ND 0.00060 0.0020 mg/Kg 03/28/19 11:35 1 cis-1,3-Dichloropropene ND 0.0015 0.0050 mg/Kg 03/28/19 11:35 1 methyl isobutyl ketone ND 0.00051 0.0020 mg/Kg 03/28/19 11:35 1 Toluene ND 0.00070 0.0020 mg/Kg 03/28/19 11:35 1 trans-1,3-Dichloropropene ND 0.00086 0.0020 mg/Kg 03/28/19 11:35 1 1,1,2-Trichloroethane ND 0.00068 0.0020 mg/Kg 03/28/19 11:35 1 Tetrachloroethene ND 0.0016 0.0050 mg/Kg 03/28/19 11:35 1 2-Hexanone ND 0.00065 0.0020 mg/Kg 03/28/19 11:35 1 Dibromochloromethane ND 0.00074 0.0020 mg/Kg 03/28/19 11:35 1 Chlorobenzene ND 0.00096 0.0020 mg/Kg 03/28/19 11:35 1 Ethylbenzene ND 0.00064 0.0040 mg/Kg 03/28/19 11:35 1 Xylenes, Total ND 0.00060 0.0020 mg/Kg 03/28/19 11:35 1 Styrene ND 0.00058 0.0020 mg/Kg 03/28/19 11:35 1 Bromoform ND 0.00064 0.0020 mg/Kg 03/28/19 11:35 1 1,1,2,2-Tetrachloroethane ND 0.00070 0.0020 mg/Kg 03/28/19 11:35 1 1,3-Dichloropropene, Total 1,2-Dichloroethane-d4 (Surr) 88 70 - 134 03/28/19 11:35 1 MB MB Surrogate Dil Fac Prepared Analyzed Qualifier Limits %Recovery 97 03/28/19 11:35 1 Toluene-d8 (Surr) 75 - 124 90 03/28/19 11:35 1 4-Bromofluorobenzene (Surr) 75 - 131 90 03/28/19 11:35 1 Dibromofluoromethane 75 - 126 TestAmerica Chicago Page 21 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Method Blank
Sample
Batch:
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
LCS 500-478012/6
Lab Sample ID: LCSD 500-478012/9
Batch: 478012
TestAmerica Job ID: 500-160490-1
Client Sample ID: Lab Control Sample Dup
Client Sample ID: Lab Control Sample Lab Sample ID:
Matrix: Solid Prep Type: Total/NA Analysis
Chloromethane 0.0500 0.0498 mg/Kg 100 70 - 125 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Vinyl chloride 0.0500 0.0476 mg/Kg 95 70 - 125 Bromomethane 0.0500 0.0537 mg/Kg 107 70 - 130 Chloroethane 0.0500 0.0639 * mg/Kg 128 75 - 125 1,1-Dichloroethene 0.0500 0.0449 mg/Kg 90 70 - 120 Acetone 0.0500 0.0510 mg/Kg 102 40 - 150 Carbon disulfide 0.0500 0.0491 mg/Kg 98 70 - 129 Methylene Chloride 0.0500 0.0426 mg/Kg 85 70 - 126 trans-1,2-Dichloroethene 0.0500 0.0464 mg/Kg 93 70 - 125 Methyl tert-butyl ether 0.0500 0.0436 mg/Kg 87 50 - 140 1,1-Dichloroethane 0.0500 0.0451 mg/Kg 90 70 - 125 cis-1,2-Dichloroethene 0.0500 0.0454 mg/Kg 91 70 - 125 Methyl Ethyl Ketone 0.0500 0.0472 mg/Kg 94 47 - 138 Chloroform 0.0500 0.0436 mg/Kg 87 57 - 135 1,1,1-Trichloroethane 0.0500 0.0442 mg/Kg 88 70 - 128 Carbon tetrachloride 0.0500 0.0440 mg/Kg 88 75 - 125 Benzene 0.0500 0.0441 mg/Kg 88 70 - 125 1,2-Dichloroethane 0.0500 0.0425 mg/Kg 85 70 - 130 Trichloroethene 0.0500 0.0467 mg/Kg 93 70 - 125 1,2-Dichloropropane 0.0500 0.0432 mg/Kg 86 70 - 125 Bromodichloromethane 0.0500 0.0417 mg/Kg 83 67 - 129 cis-1,3-Dichloropropene 0.0500 0.0411 mg/Kg 82 70 - 125 methyl isobutyl ketone 0.0500 0.0511 mg/Kg 102 50 - 148 Toluene 0.0500 0.0441 mg/Kg 88 70 - 125 trans-1,3-Dichloropropene 0.0500 0.0406 mg/Kg 81 70 - 125 1,1,2-Trichloroethane 0.0500 0.0439 mg/Kg 88 70 - 125 Tetrachloroethene 0.0500 0.0476 mg/Kg 95 70 - 124 2-Hexanone 0.0500 0.0540 mg/Kg 108 48 - 146 Dibromochloromethane 0.0500 0.0430 mg/Kg 86 69 - 125 Chlorobenzene 0.0500 0.0452 mg/Kg 90 50 - 150 Ethylbenzene 0.0500 0.0443 mg/Kg 89 61 - 136 Xylenes, Total 0.100 0.0860 mg/Kg 86 53 - 147 Styrene 0.0500 0.0434 mg/Kg 87 70 - 125 Bromoform 0.0500 0.0438 mg/Kg 88 68 - 136 1,1,2,2-Tetrachloroethane 0.0500 0.0438 mg/Kg 88 70 - 122 1,2-Dichloroethane-d4 (Surr) 70 - 134 Surrogate 88 LCS LCS Qualifier Limits %Recovery 94 Toluene-d8 (Surr) 75 - 124 90 4-Bromofluorobenzene (Surr) 75 - 131 94 Dibromofluoromethane 75 - 126
Batch: 478012
Matrix: Solid Prep
Analysis
Chloromethane 0.0500 0.0541 mg/Kg 108 70 - 125 8 30 Analyte LCSD LCSD D Unit Result Qualifier %Rec Spike Added %Rec. Limits Limit RPD RPD TestAmerica Chicago Page 22 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Type: Total/NA
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
500-478012/9
TestAmerica Job ID: 500-160490-1
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD
Matrix: Solid Prep Type: Total/NA Analysis Batch: 478012 Vinyl chloride 0.0500 0.0504 mg/Kg 101 70 - 125 6 30 Analyte LCSD LCSD D Unit Result Qualifier %Rec Spike Added %Rec. Limits Limit RPD RPD Bromomethane 0.0500 0.0582 mg/Kg 116 70 - 130 8 30 Chloroethane 0.0500 0.0677 * mg/Kg 135 75 - 125 6 30 1,1-Dichloroethene 0.0500 0.0450 mg/Kg 90 70 - 120 0 30 Acetone 0.0500 0.0536 mg/Kg 107 40 - 150 5 30 Carbon disulfide 0.0500 0.0498 mg/Kg 100 70 - 129 2 30 Methylene Chloride 0.0500 0.0433 mg/Kg 87 70 - 126 2 30 trans-1,2-Dichloroethene 0.0500 0.0456 mg/Kg 91 70 - 125 2 30 Methyl tert-butyl ether 0.0500 0.0440 mg/Kg 88 50 - 140 1 30 1,1-Dichloroethane 0.0500 0.0447 mg/Kg 89 70 - 125 1 30 cis-1,2-Dichloroethene 0.0500 0.0451 mg/Kg 90 70 - 125 1 30 Methyl Ethyl Ketone 0.0500 0.0570 mg/Kg 114 47 - 138 19 30 Chloroform 0.0500 0.0434 mg/Kg 87 57 - 135 0 30 1,1,1-Trichloroethane 0.0500 0.0425 mg/Kg 85 70 - 128 4 30 Carbon tetrachloride 0.0500 0.0426 mg/Kg 85 75 - 125 3 30 Benzene 0.0500 0.0440 mg/Kg 88 70 - 125 0 30 1,2-Dichloroethane 0.0500 0.0435 mg/Kg 87 70 - 130 2 30 Trichloroethene 0.0500 0.0454 mg/Kg 91 70 - 125 3 30 1,2-Dichloropropane 0.0500 0.0436 mg/Kg 87 70 - 125 1 30 Bromodichloromethane 0.0500 0.0419 mg/Kg 84 67 - 129 0 30 cis-1,3-Dichloropropene 0.0500 0.0402 mg/Kg 80 70 - 125 2 30 methyl isobutyl ketone 0.0500 0.0546 mg/Kg 109 50 - 148 7 30 Toluene 0.0500 0.0427 mg/Kg 85 70 - 125 3 30 trans-1,3-Dichloropropene 0.0500 0.0403 mg/Kg 81 70 - 125 1 30 1,1,2-Trichloroethane 0.0500 0.0435 mg/Kg 87 70 - 125 1 30 Tetrachloroethene 0.0500 0.0452 mg/Kg 90 70 - 124 5 30 2-Hexanone 0.0500 0.0557 mg/Kg 111 48 - 146 3 30 Dibromochloromethane 0.0500 0.0414 mg/Kg 83 69 - 125 4 30 Chlorobenzene 0.0500 0.0439 mg/Kg 88 50 - 150 3 30 Ethylbenzene 0.0500 0.0432 mg/Kg 86 61 - 136 3 30 Xylenes, Total 0.100 0.0824 mg/Kg 82 53 - 147 4 30 Styrene 0.0500 0.0422 mg/Kg 84 70 - 125 3 30 Bromoform 0.0500 0.0413 mg/Kg 83 68 - 136 6 30 1,1,2,2-Tetrachloroethane 0.0500 0.0434 mg/Kg 87 70 - 122 1 30 1,2-Dichloroethane-d4 (Surr) 70 - 134 Surrogate 89 LCSD LCSD Qualifier Limits %Recovery 93 Toluene-d8 (Surr) 75 - 124 90 4-Bromofluorobenzene (Surr) 75 - 131 94 Dibromofluoromethane 75 - 126 TestAmerica Chicago Page 23 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
MB 500-477587/1-A
TestAmerica Job ID: 500-160490-1
Client Sample ID: Method Blank Lab Sample ID:
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477635 Prep Batch: 477587 RL MDL Phenol ND 0.17 0.074 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.050 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Bis(2-chloroethyl)ether ND 0.037 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 1,3-Dichlorobenzene ND 0.043 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 1,4-Dichlorobenzene ND 0.040 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 1,2-Dichlorobenzene ND 0.053 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Methylphenol ND 0.039 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,2'-oxybis[1-chloropropane] ND 0.041 0.067 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 N-Nitrosodi-n-propylamine ND 0.051 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Hexachloroethane ND 0.057 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Chlorophenol ND 0.0083 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Nitrobenzene ND 0.034 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Bis(2-chloroethoxy)methane ND 0.036 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 1,2,4-Trichlorobenzene ND 0.037 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Isophorone ND 0.13 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4-Dimethylphenol ND 0.052 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Hexachlorobutadiene ND 0.0051 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Naphthalene ND 0.079 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4-Dichlorophenol ND 0.16 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Chloroaniline ND 0.11 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4,6-Trichlorophenol ND 0.076 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4,5-Trichlorophenol ND 0.19 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Hexachlorocyclopentadiene ND 0.0061 0.067 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Methylnaphthalene ND 0.045 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Nitroaniline ND 0.037 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Chloronaphthalene ND 0.11 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Chloro-3-methylphenol ND 0.065 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,6-Dinitrotoluene ND 0.079 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2-Nitrophenol ND 0.10 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 3-Nitroaniline ND 0.043 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Dimethyl phthalate ND 0.59 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4-Dinitrophenol ND 0.0044 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Acenaphthylene ND 0.053 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 2,4-Dinitrotoluene ND 0.0060 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Acenaphthene ND 0.039 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Dibenzofuran ND 0.32 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Nitrophenol ND 0.0047 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Fluorene ND 0.14 0.33 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Nitroaniline ND 0.044 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Bromophenyl phenyl ether ND 0.0077 0.067 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Hexachlorobenzene ND 0.056 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Diethyl phthalate ND 0.039 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4-Chlorophenyl phenyl ether ND 0.53 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Pentachlorophenol ND 0.039 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 N-Nitrosodiphenylamine ND 0.27 0.67 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 4,6-Dinitro-2-methylphenol ND 0.0046 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Phenanthrene ND 0.0056 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Anthracene ND 0.083 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Carbazole TestAmerica Chicago Page 24 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
MB 500-477587/1-A
TestAmerica Job ID: 500-160490-1
Client Sample ID: Method Blank Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477635 Prep Batch: 477587 RL MDL Di-n-butyl phthalate ND 0.17 0.051 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.0062 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Fluoranthene ND 0.0066 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Pyrene ND 0.063 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Butyl benzyl phthalate ND 0.0045 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Benzo[a]anthracene ND 0.0091 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Chrysene ND 0.047 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 3,3'-Dichlorobenzidine ND 0.061 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Bis(2-ethylhexyl) phthalate ND 0.054 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Di-n-octyl phthalate ND 0.0072 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Benzo[b]fluoranthene ND 0.0098 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Benzo[k]fluoranthene ND 0.0064 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Benzo[a]pyrene ND 0.0086 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Indeno[1,2,3-cd]pyrene ND 0.0064 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Dibenz(a,h)anthracene ND 0.011 0.033 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 Benzo[g,h,i]perylene ND 0.055 0.17 mg/Kg 03/25/19 16:20 03/26/19 11:30 1 3 & 4 Methylphenol 2-Fluorophenol 105 31 - 166 03/26/19 11:30 1 MB MB Surrogate 03/25/19 16:20 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 103 03/25/19 16:20 03/26/19 11:30 1 Phenol-d5 30 - 153 92 03/25/19 16:20 03/26/19 11:30 1 Nitrobenzene-d5 37 - 147 95 03/25/19 16:20 03/26/19 11:30 1 2-Fluorobiphenyl 43 - 145 94 03/25/19 16:20 03/26/19 11:30 1 2,4,6-Tribromophenol 31 - 143 104 03/25/19 16:20 03/26/19 11:30 1 Terphenyl-d14 42 - 157 Client Sample ID: Lab Control Sample Lab Sample ID: LCS 500-477587/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 477635 Prep Batch: 477587 Phenol 1.33 1.52 mg/Kg 114 56 - 122 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Bis(2-chloroethyl)ether 1.33 1.25 mg/Kg 94 55 - 111 1,3-Dichlorobenzene 1.33 1.30 mg/Kg 97 65 - 124 1,4-Dichlorobenzene 1.33 1.31 mg/Kg 98 61 - 110 1,2-Dichlorobenzene 1.33 1.32 mg/Kg 99 62 - 110 2-Methylphenol 1.33 1.35 mg/Kg 101 60 - 120 2,2'-oxybis[1-chloropropane] 1.33 1.03 mg/Kg 77 40 - 124 N-Nitrosodi-n-propylamine 1.33 1.31 mg/Kg 99 56 - 118 Hexachloroethane 1.33 1.23 mg/Kg 93 60 - 114 2-Chlorophenol 1.33 1.39 mg/Kg 104 64 - 110 Nitrobenzene 1.33 1.30 mg/Kg 97 60 - 116 Bis(2-chloroethoxy)methane 1.33 1.36 mg/Kg 102 60 - 112 1,2,4-Trichlorobenzene 1.33 1.32 mg/Kg 99 66 - 117 Isophorone 1.33 1.28 mg/Kg 96 55 - 110 2,4-Dimethylphenol 1.33 1.31 mg/Kg 99 60 - 110 Hexachlorobutadiene 1.33 1.27 mg/Kg 95 56 - 120 Naphthalene 1.33 1.35 mg/Kg 102 63 - 110 2,4-Dichlorophenol 1.33 1.36 mg/Kg 102 58 - 120 TestAmerica Chicago Page 25 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
ID:
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
LCS 500-477587/2-A
TestAmerica Job ID: 500-160490-1
Client Sample ID: Lab Control Sample Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477635 Prep Batch: 477587 4-Chloroaniline 1.33 1.32 mg/Kg 99 30 - 150 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits 2,4,6-Trichlorophenol 1.33 1.32 mg/Kg 99 57 - 120 2,4,5-Trichlorophenol 1.33 1.29 mg/Kg 97 50 - 120 Hexachlorocyclopentadiene 1.33 1.53 mg/Kg 115 10 - 133 2-Methylnaphthalene 1.33 1.40 mg/Kg 105 69 - 112 2-Nitroaniline 1.33 1.20 mg/Kg 90 57 - 124 2-Chloronaphthalene 1.33 1.27 mg/Kg 95 69 - 114 4-Chloro-3-methylphenol 1.33 1.31 mg/Kg 99 65 - 122 2,6-Dinitrotoluene 1.33 1.34 mg/Kg 101 70 - 123 2-Nitrophenol 1.33 1.36 mg/Kg 102 60 - 120 3-Nitroaniline 1.33 1.14 mg/Kg 85 40 - 122 Dimethyl phthalate 1.33 1.25 mg/Kg 94 69 - 116 2,4-Dinitrophenol 2.67 0.747 mg/Kg 28 10 - 100 Acenaphthylene 1.33 1.29 mg/Kg 96 68 - 120 2,4-Dinitrotoluene 1.33 1.31 mg/Kg 98 69 - 124 Acenaphthene 1.33 1.28 mg/Kg 96 65 - 124 Dibenzofuran 1.33 1.28 mg/Kg 96 66 - 115 4-Nitrophenol 2.67 2.45 mg/Kg 92 30 - 122 Fluorene 1.33 1.30 mg/Kg 97 62 - 120 4-Nitroaniline 1.33 1.24 mg/Kg 93 60 - 160 4-Bromophenyl phenyl ether 1.33 1.30 mg/Kg 98 68 - 118 Hexachlorobenzene 1.33 1.42 mg/Kg 106 63 - 124 Diethyl phthalate 1.33 1.20 mg/Kg 90 58 - 120 4-Chlorophenyl phenyl ether 1.33 1.23 mg/Kg 92 62 - 119 Pentachlorophenol 2.67 2.46 mg/Kg 92 13 - 112 N-Nitrosodiphenylamine 1.33 1.35 mg/Kg 101 65 - 112 4,6-Dinitro-2-methylphenol 2.67 1.22 mg/Kg 46 10 - 110 Phenanthrene 1.33 1.33 mg/Kg 100 62 - 120 Anthracene 1.33 1.35 mg/Kg 101 70 - 114 Carbazole 1.33 1.46 mg/Kg 110 65 - 142 Di-n-butyl phthalate 1.33 1.24 mg/Kg 93 65 - 120 Fluoranthene 1.33 1.33 mg/Kg 100 62 - 120 Pyrene 1.33 1.32 mg/Kg 99 61 - 128 Butyl benzyl phthalate 1.33 1.20 mg/Kg 90 71 - 129 Benzo[a]anthracene 1.33 1.22 mg/Kg 92 67 - 122 Chrysene 1.33 1.34 mg/Kg 101 63 - 120 3,3'-Dichlorobenzidine 1.33 1.13 mg/Kg 85 35 - 128 Bis(2-ethylhexyl) phthalate 1.33 1.22 mg/Kg 92 72 - 131 Di-n-octyl phthalate 1.33 1.21 mg/Kg 91 68 - 134 Benzo[b]fluoranthene 1.33 1.49 mg/Kg 112 69 - 129 Benzo[k]fluoranthene 1.33 1.23 mg/Kg 93 68 - 127 Benzo[a]pyrene 1.33 1.40 mg/Kg 105 65 - 133 Indeno[1,2,3-cd]pyrene 1.33 1.37 mg/Kg 103 68 - 130 Dibenz(a,h)anthracene 1.33 1.39 mg/Kg 104 64 - 131 Benzo[g,h,i]perylene 1.33 1.39 mg/Kg 104 72 - 131 3 & 4 Methylphenol 1.33 1.42 mg/Kg 106 57 - 120 TestAmerica Chicago Page 26 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
ID:
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample
Sample ID: LCS 500-477587/2-A
Method: 8081B - Organochlorine Pesticides (GC) Client Sample ID: Method Blank
ID: MB 500-477625/1-A
Lab Sample ID: LCS 500-477625/2-A
Matrix: Solid
Analysis Batch: 477741
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Batch: 477625
Lab
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477635 Prep Batch: 477587 2-Fluorophenol 31 - 166 Surrogate 109 LCS LCS Qualifier Limits %Recovery 114 Phenol-d5 30 - 153 99 Nitrobenzene-d5 37 - 147 97 2-Fluorobiphenyl 43 - 145 113 2,4,6-Tribromophenol 31 - 143 99 Terphenyl-d14 42 - 157
Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477741 Prep Batch: 477625 RL MDL alpha-BHC ND 0.0017 0.00042 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.00052 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 beta-BHC 0.000611 J 0.00053 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 delta-BHC ND 0.00036 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 gamma-BHC (Lindane) ND 0.00070 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Heptachlor ND 0.00069 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Aldrin ND 0.00059 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Heptachlor epoxide ND 0.00073 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endosulfan I ND 0.00023 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Dieldrin ND 0.00028 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 4,4'-DDE ND 0.00023 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endrin ND 0.00027 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endosulfan II ND 0.00033 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 4,4'-DDD ND 0.00031 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endosulfan sulfate ND 0.00088 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 4,4'-DDT ND 0.00032 0.0083 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Methoxychlor ND 0.00085 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 cis-Chlordane ND 0.00044 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 trans-Chlordane ND 0.0070 0.017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Toxaphene ND 0.00028 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endrin aldehyde ND 0.00038 0.0017 mg/Kg 03/26/19 07:44 03/26/19 17:55 1 Endrin ketone DCB Decachlorobiphenyl 102 33 - 148 03/26/19 17:55 1 MB MB Surrogate 03/26/19 07:44 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 90 03/26/19 07:44 03/26/19 17:55 1 Tetrachloro-m-xylene 30 - 121
Prep
alpha-BHC 0.0133 0.0135 mg/Kg 101 50 - 123 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits beta-BHC 0.0133 0.0126 mg/Kg 95 44 - 140 TestAmerica Chicago Page 27 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
TestAmerica Job ID: 500-160490-1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method Blank Lab Sample ID: MB 500-477625/1-A
Client Sample ID: Lab Control Sample Lab Sample ID: LCS
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477741 Prep Batch: 477625 delta-BHC 0.0133 0.0145 mg/Kg 108 57 - 125 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits gamma-BHC (Lindane) 0.0133 0.0134 mg/Kg 100 50 - 122 Heptachlor 0.0133 0.0150 mg/Kg 113 53 - 129 Aldrin 0.0133 0.0139 mg/Kg 104 52 - 122 Heptachlor epoxide 0.0133 0.0133 mg/Kg 100 50 - 139 Endosulfan I 0.0133 0.00942 mg/Kg 71 30 - 120 Dieldrin 0.0133 0.0138 mg/Kg 103 51 - 133 4,4'-DDE 0.0133 0.0138 mg/Kg 104 50 - 130 Endrin 0.0133 0.0141 mg/Kg 106 43 - 144 Endosulfan II 0.0133 0.0102 mg/Kg 76 30 - 120 4,4'-DDD 0.0133 0.0146 mg/Kg 109 47 - 137 Endosulfan sulfate 0.0133 0.0149 mg/Kg 112 42 - 150 4,4'-DDT 0.0133 0.0153 mg/Kg 115 46 - 143 Methoxychlor 0.0133 0.0154 mg/Kg 115 45 - 144 cis-Chlordane 0.0133 0.0131 mg/Kg 99 52 - 129 trans-Chlordane 0.0133 0.0125 mg/Kg 94 52 - 132 Endrin aldehyde 0.0133 0.0143 mg/Kg 108 39 - 131 Endrin ketone 0.0133 0.0143 mg/Kg 108 51 - 135 DCB Decachlorobiphenyl 33 - 148 Surrogate 103 LCS LCS Qualifier Limits %Recovery 92 Tetrachloro-m-xylene 30 - 121
500-477625/2-A
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477658 Prep Batch: 477625 RL MDL PCB-1016 ND 0.017 0.0059 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.0073 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1221 ND 0.0073 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1232 ND 0.0055 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1242 ND 0.0066 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1248 ND 0.0036 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1254 ND 0.0082 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 PCB-1260 ND 0.0032 0.017 mg/Kg 03/26/19 07:44 03/26/19 14:40 1 Polychlorinated biphenyls, Total Tetrachloro-m-xylene 91 49 - 129 03/26/19 14:40 1 MB MB Surrogate 03/26/19 07:44 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 89 03/26/19 07:44 03/26/19 14:40 1 DCB Decachlorobiphenyl 37 - 121 TestAmerica Chicago Page 28 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
TestAmerica Job ID: 500-160490-1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
ID: LCS 500-477625/3-A
Method: 6010B - Metals (ICP)
MB 500-477754/1-A
Client Sample
Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477658 Prep Batch: 477625 PCB-1016 0.167 0.129 mg/Kg 77 57 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits PCB-1260 0.167 0.127 mg/Kg 76 61 - 125 Tetrachloro-m-xylene 49 - 129 Surrogate 78 LCS LCS Qualifier Limits %Recovery 79 DCB Decachlorobiphenyl 37 - 121
ID: Lab Control Sample
Client Sample
Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477904 Prep Batch: 477754 RL MDL Antimony ND 2.0 0.39 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier ND 0.34 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Arsenic ND 0.093 0.40 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Beryllium 0.0781 J 0.036 0.20 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Cadmium ND 0.50 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Chromium ND 0.28 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Copper ND 0.23 0.50 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Lead ND 0.29 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Nickel ND 0.59 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Selenium ND 0.13 0.50 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Silver ND 0.50 1.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Thallium ND 0.88 2.0 mg/Kg 03/26/19 16:18 03/27/19 09:52 1 Zinc Client Sample ID: Lab Control Sample Lab Sample ID: LCS 500-477754/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 477904 Prep Batch: 477754 Antimony 50.0 45.1 mg/Kg 90 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Arsenic 10.0 8.99 mg/Kg 90 80 - 120 Beryllium 5.00 4.73 mg/Kg 95 80 - 120 Cadmium 5.00 4.65 mg/Kg 93 80 - 120 Chromium 20.0 18.6 mg/Kg 93 80 - 120 Copper 25.0 24.6 mg/Kg 98 80 - 120 Lead 10.0 9.51 mg/Kg 95 80 - 120 Nickel 50.0 47.6 mg/Kg 95 80 - 120 Selenium 10.0 8.45 mg/Kg 85 80 - 120 Silver 5.00 4.60 mg/Kg 92 80 - 120 Thallium 10.0 9.58 mg/Kg 96 80 - 120 Zinc 50.0 46.0 mg/Kg 92 80 - 120 TestAmerica Chicago Page 29 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
ID: Method Blank
ID:
Client: ECS Midwest LLC
QC Sample Results
Project/Site: Calumet Country Club CCDD - 53-2027
Method: 7471B - Mercury (CVAA)
MB 500-477684/12-A
Method: 9014 - Cyanide
ID: MB 500-477872/1-A
Sample ID: LCS 500-477872/2-A
TestAmerica Job ID: 500-160490-1
Client Sample ID:
Lab Sample ID:
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477884 Prep Batch: 477684 RL MDL Mercury ND 0.017 0.0056 mg/Kg 03/26/19 14:00 03/27/19 09:49 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 500-477684/13-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 477884 Prep Batch: 477684 Mercury 0.167 0.182 mg/Kg 109 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: B-2 Lab Sample ID: 500-160490-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 477884 Prep Batch: 477684 Mercury 0.041 0.100 0.149 mg/Kg 108 75 - 125 ☼ Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: B-2 Lab Sample ID: 500-160490-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 477884 Prep Batch: 477684 Mercury 0.041 0.0997 0.155 mg/Kg 114 75 - 125 4 20 ☼ Analyte MSD MSD D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Limit RPD RPD Client Sample ID: B-2 Lab Sample ID: 500-160490-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 477884 Prep Batch: 477684 Mercury 0.041 0.0401 mg/Kg 2 20 ☼ Analyte DU DU D Unit Result Qualifier Sample Result Sample Qualifier Limit RPD RPD
Method Blank
Client Sample ID:
Lab Sample
Matrix: Solid Prep Type: Total/NA Analysis Batch: 477933 Prep Batch: 477872 RL MDL Cyanide, Total ND 0.50 0.17 mg/Kg 03/27/19 12:10 03/27/19 14:39 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab
Matrix:
Prep Type: Total/NA Analysis Batch:
Prep Batch: 477872 Cyanide, Total 5.00 4.83 mg/Kg 97 85 - 115 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits TestAmerica Chicago Page 30 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Method Blank
Solid
477933
Client: ECS Midwest LLC
Project/Site: Calumet Country Club CCDD - 53-2027
Lab Chronicle
TestAmerica Job ID: 500-160490-1
Lab Sample ID: 500-160490-1 Matrix: Solid Date Collected: 03/25/19 09:00 Date Received: 03/25/19 12:30 Analysis 9045D SMO 1 478405 TAL CHI Type Batch Batch Method Prep Type Lab Analyst Run Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/29/19 13:01 03/29/19 13:08 (Start) (End) Analysis Moisture 1 477605 03/26/19 06:42 LWN TAL CHI Total/NA Client Sample ID: B-2 Lab Sample ID: 500-160490-1 Matrix: Solid Date Collected: 03/25/19 09:00 Percent Solids: 80.0 Date Received: 03/25/19 12:30 Prep 5035 03/25/19 17:17 WRE 477800 TAL CHI Type Batch Batch Method Prep Type Lab Analyst Run Prepared or Analyzed Batch Number Dilution Factor Total/NA Analysis 8260B 1 478012 03/28/19 15:49 PMF TAL CHI Total/NA Prep 3541 477587 03/25/19 16:20 NRJ TAL CHI Total/NA Analysis 8270D 1 477635 03/26/19 11:54 STW TAL CHI Total/NA Prep 3541 477625 03/26/19 07:44 DX TAL CHI Total/NA Analysis 8081B 1 477741 03/26/19 23:01 S1S TAL CHI Total/NA Prep 3541 477625 03/26/19 07:44 DX TAL CHI Total/NA Analysis 8082A 1 477658 03/26/19 16:21 BJH TAL CHI Total/NA Prep 3050B 477754 03/26/19 16:18 BDE TAL CHI Total/NA Analysis 6010B 1 477904 03/27/19 12:11 EEN TAL CHI Total/NA Prep 7471B 477684 03/26/19 14:00 MJG TAL CHI Total/NA Analysis 7471B 1 477884 03/27/19 10:02 MJG TAL CHI Total/NA Prep 9010B 477872 03/27/19 12:10 MS TAL CHI Total/NA Analysis 9014 1 477933 MS TAL CHI Total/NA 03/27/19 14:47 03/27/19 14:48 (Start) (End) Client Sample ID: S-2 Lab Sample ID: 500-160490-2 Matrix: Solid Date Collected: 03/25/19 09:00 Date Received: 03/25/19 12:30 Analysis 9045D SMO 1 478405 TAL CHI Type Batch Batch Method Prep Type Lab Analyst Run Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/29/19 13:08 03/29/19 13:14 (Start) (End) Analysis Moisture 1 477605 03/26/19 06:42 LWN TAL CHI Total/NA Client Sample ID: S-2 Lab Sample ID: 500-160490-2 Matrix: Solid Date Collected: 03/25/19 09:00 Percent Solids: 83.4 Date Received: 03/25/19 12:30 Prep 5035 03/25/19 17:17 WRE 477800 TAL CHI Type Batch Batch Method Prep Type Lab Analyst Run Prepared or Analyzed Batch Number Dilution Factor Total/NA TestAmerica Chicago Page 31 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client Sample ID: B-2
Client: ECS Midwest LLC
Project/Site: Calumet Country Club CCDD - 53-2027
Client Sample ID: S-2
Lab Chronicle
TestAmerica
Job ID: 500-160490-1
Lab
Matrix: Solid Date Collected:
09:00 Percent Solids: 83.4 Date Received: 03/25/19 12:30 Analysis 8260B 03/28/19 16:15 PMF 1 478012 TAL CHI Type Batch Batch Method Prep Type Lab Analyst Run Prepared or Analyzed Batch Number Dilution Factor Total/NA Prep 3541 477587 03/25/19 16:20 NRJ TAL CHI Total/NA Analysis 8270D 1 477635 03/26/19 12:18 STW TAL CHI Total/NA Prep 3541 477625 03/26/19 07:44 DX TAL CHI Total/NA Analysis 8081B 1 477741 03/26/19 23:21 S1S TAL CHI Total/NA Prep 3541 477625 03/26/19 07:44 DX TAL CHI Total/NA Analysis 8082A 1 477658 03/26/19 16:41 BJH TAL CHI Total/NA Prep 3050B 477754 03/26/19 16:18 BDE TAL CHI Total/NA Analysis 6010B 1 477904 03/27/19 12:31 EEN TAL CHI Total/NA Prep 7471B 477684 03/26/19 14:00 MJG TAL CHI Total/NA Analysis 7471B 1 477884 03/27/19 10:14 MJG TAL CHI Total/NA Prep 9010B 477872 03/27/19 12:10 MS TAL CHI Total/NA Analysis 9014 1 477933 MS TAL CHI Total/NA 03/27/19 14:48 03/27/19 14:48 (Start) (End) Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 TestAmerica Chicago Page 32 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Sample ID: 500-160490-2
03/25/19
Client: ECS Midwest LLC
Accreditation/Certification Summary
Project/Site: Calumet Country Club CCDD - 53-2027
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
TestAmerica Job ID: 500-160490-1
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.
Authority Program EPA Region Identification Number Expiration Date Illinois 100201 5 NELAP 04-30-19
Analysis Method Prep Method Matrix Analyte 8082A 3541 Solid Polychlorinated biphenyls, Total 8260B 5035 Solid 1,3-Dichloropropene, Total Moisture Solid Percent Moisture Moisture Solid Percent Solids TestAmerica Chicago Page 33 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Page 34 of 35 3/29/2019 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Client: ECS Midwest LLC
Login Number: 160490
List Number: 1
Creator: Scott, Sherri L
Question
Login Sample Receipt Checklist
Job Number: 500-160490-1
List Source: TestAmerica Chicago
Radioactivity wasn't checked or is </= background as measured by a survey meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate HTs) True
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
Containers requiring zero headspace have no headspace or bubble is <6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Answer Comment
True
True
True
True
True
True
True
3.6 True
True
True
True
True
True
True
True
True
True
True
N/A
True
True
N/A
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